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Tytuł:
Comparison of the free volume sizes and shapes determined from crystallographic and PALS data
Autorzy:
Tydda, M.
Jasińska, B.
Powiązania:
https://bibliotekanauki.pl/articles/146378.pdf
Data publikacji:
2015
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
benzenediols
free volume
molecular crystals olanzapine
positron annihilation
positronium
positronium diffusion coefficient
Opis:
Two different classes of molecular crystals were investigated. The first group was benzenediols, which are characterized by the same chemical composition but a different organization of their crystallographic structures; all of the compounds from this group have only one kind of free volumes. The second class was represented by olanzapine, which has more complex chemical composition and two kinds of free volumes in the structure. The o-Ps lifetime values determined from positron annihilation lifetime spectroscopy (PALS) measurements agree quite well with those calculated for sizes found from crystallographic data for benzenediols (agreement within 10% of the lifetime values). For olanzapine, a good agreement is observed in the case of cuboidal free volumes, while for the other kind of void, the agreement is less satisfactory. Positronium diffusion coefficient determined from o-Ps redistribution in olanzapine agrees with these found for polymers.
Źródło:
Nukleonika; 2015, 60, No. 4, part 1; 771-775
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Some remarks on positron/positronium diffusion models
Autorzy:
Świątkowski, W.
Powiązania:
https://bibliotekanauki.pl/articles/148428.pdf
Data publikacji:
2003
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
diffusion
diffusion length
positron
positronium
Opis:
Positrons thermalized near the sample boundary (as well as Ps atoms formed in the sample) can reach the boundary as a result of diffusive movement. Observations of such effects as positron reemission or positron surface trapping as well as positronium emission allow one to calculate respective diffusion lengths. From the presented analysis it follows that some models used in such calculations give quite wrong results.
Źródło:
Nukleonika; 2003, 48, 3; 141-144
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Searches for discrete symmetries violation in ortho-positronium decay using the J-PET detector
Autorzy:
Kamińska, D.
Gajos, A.
Czerwiński, E.
Bednarski, T.
Białas, P.
Gorgol, M.
Jasińska, B.
Kapłon, Ł.
Korcyl, G.
Kowalski, P.
Kozik, T.
Krzemień, W.
Kubicz, E.
Niedźwiecki, S.
Pałka, M.
Raczyński, L.
Rudy, Z.
Rundel, O.
Sharma, N. G.
Silarski, M.
Słomski, A.
Strzelecki, A.
Wieczorek, A.
Wiślicki, W.
Zieliński, M.
Zgardzińska, B.
Moskal, P.
Powiązania:
https://bibliotekanauki.pl/articles/147408.pdf
Data publikacji:
2015
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
discrete symmetries
J-PET
ortho-positronium
Opis:
In this paper, we present prospects for using the Jagiellonian positron emission tomograph (J-PET) detector to search for discrete symmetries violations in a purely leptonic system of the positronium atom. We discuss tests of CP and CPT symmetries by means of ortho-positronium decays into three photons. No zero expectation values for chosen correlations between ortho-positronium spin and momentum vectors of photons would imply the existence of physics phenomena beyond the standard model. Previous measurements resulted in violation amplitude parameters for CP and CPT symmetries consistent with zero, with an uncertainty of about 10−3. The J-PET detector allows to determine those values with better precision, thanks to the unique time and angular resolution combined with a high geometrical acceptance. Achieving the aforementioned is possible because of the application of polymer scintillators instead of crystals as detectors of annihilation quanta.
Źródło:
Nukleonika; 2015, 60, No. 4, part 1; 729-732
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Positrons in naphthalene : critical remarks on the relation between o-Ps lifetime and void size
Autorzy:
Goworek, T.
Zgardzińska, B.
Wawryszczuk, J.
Powiązania:
https://bibliotekanauki.pl/articles/148003.pdf
Data publikacji:
2013
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
high pressure
naphthalene
positronium quenching
free volume
Opis:
Lowering the temperature or applying high pressure leads to elimination of positronium component in the e+ lifetime spectrum in solid naphthalene. Disappearance of positronium means reaching the free volume size limit at which there is no energy level in the potential well. It allows to estimate that size, which is found inconsistent with predictions of the popular Tao-Eldrup model. The range of applicability of that model is discussed. The dependence of the free e+ decay constant on pressure indicates that positronium is formed not only in the blob processes, but during the whole free positron life. The lifetime of free positrons begins to rise with temperature earlier than Ps intensity.
Źródło:
Nukleonika; 2013, 58, 1; 183-187
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
PALS investigations of free volumes thermal expansion of J-PET plastic scintillator synthesized in polystyrene matrix
Autorzy:
Wieczorek, A.
Zgardzińska, B.
Jasińska, B.
Gorgol, M.
Bednarski, T.
Białas, P.
Czerwiński, E.
Gajos, A.
Kamińska, D.
Kapłon, Ł.
Kochanowski, A.
Korcyl, G.
Kowalski, P.
Kozik, T.
Krzemień, W.
Kubicz, E.
Niedźwiecki, S.
Pałka, M.
Raczyński, L.
Rudy, Z.
Rundel, O.
Sharma, N. G.
Silarski, M.
Silarski, A.
Strzelecki, A.
Wiślicki, W.
Zieliński, M.
Moskal, P.
Powiązania:
https://bibliotekanauki.pl/articles/147132.pdf
Data publikacji:
2015
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
free volume
positron annihilation
polystyrene
positronium
scintillator
Opis:
The polystyrene doped with 2,5-diphenyloxazole as a primary fluor and 2-(4-styrylphenyl)benzoxazole as a wavelength shifter prepared as a plastic scintillator was investigated using positronium probe in wide range of temperatures from 123 to 423 K. Three structural transitions at 260, 283, and 370 K were found in the material. In the o-Ps intensity dependence on temperature, the significant hysteresis is observed. Heated to 370 K, the material exhibits the o-Ps intensity variations in time.
Źródło:
Nukleonika; 2015, 60, No. 4, part 1; 777-781
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Human tissue investigations using PALS technique - free radicals influence
Autorzy:
Jasińska, B.
Zgardzińska, B.
Chołubek, G.
Pietrow, M.
Gorgol, M.
Wiktor, K.
Wysogląd, K.
Białas, P.
Curceanu, C.
Czerwiński, E.
Dulski, K.
Gajos, A.
Głowacz, B.
Hiesmayr, B.
Jodłowska-Jędrych, B.
Kamińska, D.
Korcyl, G.
Kowalski, P.
Kozik, T.
Krawczyk, N.
Krzemień, W.
Kubicz, E.
Mohammed, Muhsin
Pawlik-Niedźwiecka, M.
Niedźwiecki, S.
Pałka, M.
Raczyński, L.
Rudy, Z.
Sharma, N.
Sharma, S.
Shopa, R.
Silarski, M.
Skurzok, M.
Wieczorek, A.
Wiktor, H.
Wiślicki, W.
Zieliński, M.
Moskal, P.
Powiązania:
https://bibliotekanauki.pl/articles/1057941.pdf
Data publikacji:
2017-11
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
positron annihilation
positronium
free radicals
tissues
uterine leiomyomas
Opis:
The positron annihilation lifetime spectroscopy was applied to the samples of the human uterine leiomyomas and the normal myometrium tissues taken from the selected place of the uterus during a surgery. The method indicated differences in values of the measured positron annihilation lifetime spectroscopy parameters (lifetimes and intensities) between healthy and diseased tissue samples. The additional measurements were performed either in darkness or in presence of visible light which influenced the free radicals present in both kind of tissues and, as a result, made changes in free annihilation and o-Ps decay lifetime and intensity values.
Źródło:
Acta Physica Polonica A; 2017, 132, 5; 1556-1558
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Biodegradable polyester blend and copolyesters studied by positron annihilation and other methods
Autorzy:
Dębowska, M.
Rudzińska-Girulska, J.
Serwadczak, M.
Kiersnowski, A.
Pigłowski, J.
Powiązania:
https://bibliotekanauki.pl/articles/146301.pdf
Data publikacji:
2010
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
mixing of polymers
polyesters
transesterification
positron annihilation
positronium
free volume
Opis:
Two polyesters, i.e. an aromatic one: poly(butylene terephthalate) – PBT and an aliphatic one: poly(ĺ- -caprolactone) – PCL were mixed in melt to obtain a biodegradable product. DSC, 1H NMR, SEM, WAXS, SAXS, BOD and PALS measurements were performed to study the homopolymers as well as their physical blend and copolyesters. The latter were obtained due to the transesterification reaction. Ortho-positronium (o-Ps) annihilation lifetimes were used to create the distributions of free volume. The progressive changes in probability density function of free volume, i.e. increase in large free volume holes contribution to the total free volume, appearing when going from the homopolymers to the blend and then to the copolyesters reflect the influence of: the addition of aliphatic polyester, the weight fraction of it in the composition and transesterification. The higher contribution of larger free volume holes corresponds well with the reduced crystallinity of compositions revealed in X-ray diffraction and the worsening of the regularity of structure of the macromolecules involved in formation of crystals, deduced from the 1H NMR.
Źródło:
Nukleonika; 2010, 55, 1; 57-64
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Study on the effect of atmospheric gases adsorbed in MnFe2O4/MCM-41 nanocomposite on ortho-positronium annihilation
Autorzy:
Wiertel, M.
Surowiec, Z.
Budzyński, M.
Gac, W.
Powiązania:
https://bibliotekanauki.pl/articles/146949.pdf
Data publikacji:
2015
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
manganese ferrite
MCM-41 silica
nanocomposite
o-Ps quenching
positronium annihilation
Opis:
In this paper, results of positron annihilation lifetime spectroscopy (PALS) studies of MnFe2O4/MCM- -41 nanocomposites in N2 and O2 atmosphere have been presented. In particular, the influence of manganese ferrite loading and gas filling on pick-off ortho-positronium (o-Ps) annihilation processes in the investigated samples was a point of interest. Disappearance of the longest-lived o-Ps component with τ5 present in the PAL spectrum of initial MCM-41 mesoporous material in the PAL spectra of MnFe2O4-impregnated MCM-41 measured in vacuum is a result of either a strong chemical o-Ps quenching or the Ps inhibition effects. The intensity I4 of the medium-lived component initially increases, reaching a maximum value for the sample with minimum manganese ferrite content, and then decreases monotonically. Analogous dependence for the intensity I3 of the shortest-lived component shows a maximum at higher MnFe2O4 content. Filling of open pores present in the studied nanocomposites by N2 or O2 at ambient pressure causes partial reappearance of the τ4 and τ5 components, except a sample with maximum ferrite content. The lifetimes of these components measured in O2 are shortened in comparison to that observed in N2 because of paramagnetic quenching. Anti-inhibition and anti-quenching effects of atmospheric gases observed in the MnFe2O4/MCM-41 samples are a result of neutralization of some surface active centers acting as inhibitors and weakening of pick-off annihilation mechanism, respectively.
Źródło:
Nukleonika; 2015, 60, No. 4, part 1; 783-787
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Ortho-positronium migration in mesopores of MCM-41, MSF and SBA-3
Autorzy:
Zaleski, R.
Błażewicz, A.
Kierys, A.
Powiązania:
https://bibliotekanauki.pl/articles/147955.pdf
Data publikacji:
2013
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
nitrogen adsorption/desorption
porous materials
positron annihilation lifetime spectroscopy (PALS)
positronium migration
Opis:
Three materials: MCM-41, MSF and SBA-3 with a very similar pore diameter but different lengths of cylindrical pores were investigated using the nitrogen sorption method and positron annihilation lifetime spectroscopy. The size of primary pores and interparticle spaces obtained by both methods is similar. However, volume ratios between the discussed kinds of pores found by the above-mentioned methods differ significantly. Such discrepancy is the result of both ortho-positronium migration and the inaccessibility of the pores for nitrogen. Comparing the results of nitrogen sorption and positron annihilation lifetime spectroscopy allows us to estimate that connectivity between the primary pores and the interparticle spaces is the highest in MCM-41 and lowest in SBA-3.
Źródło:
Nukleonika; 2013, 58, 1; 235-240
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
New Porosimetric Method Based on the 3γ Annihilation Rate. Applications to Materials Science and Medical Imaging
Autorzy:
Jasińska, B.
Zgardzińska, B.
Powiązania:
https://bibliotekanauki.pl/articles/1033228.pdf
Data publikacji:
2017-11
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
positron annihilation
positronium
3γ annihilation
porosity
positron emission tomography
medical imaging
Opis:
A new parameter δ based on 3γ annihilation is proposed. It describes the porosity of the materials containing small intermolecular voids below 1 nm. It can be applied to material investigation to compare changes in the material porosity depending on temperature or pressure as well as to study of ageing or manufacturing processes. Particularly it is dedicated to prepare the new imaging method and can be used during positron emission tomography diagnosis allowing determination the kind or stage of pathogenic alteration.
Źródło:
Acta Physica Polonica A; 2017, 132, 5; 1616-1619
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
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