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    Wyświetlanie 1-10 z 10
    Tytuł:
    Synthesis and characterization of InWO3 - TiO2 nanocomposite material and multi application
    Autorzy:
    Kamalakkannan, J.
    Chandraboss, V. L.
    Senthilvelan, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/1193047.pdf
    Data publikacji:
    2016
    Wydawca:
    Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
    Tematy:
    Photocatalytic activity
    Antimicrobial activity
    Electrochemical activity
    Opis:
    InWO3 -TiO2 nanocomposite material was synthesised by co-precipitation method and sonication technique. The synthesized nanomaterial was characterized by FE-SEM with EDX, HR-TEM, XRD, FT-RAMAN, AFM and BET surface area measurements. The photocatalytic activity of InWO3-TiO2 nanocomposite material was studied from the photodegradation of malachite green (MAG) under UV-light irradiation. The photodegradation of MAG at various parameters are reported. The Photodegradation was found to follow the pseudo-first-order kinetics. The Hydroxyl radical formation in the mechanism was confirmed by fluorescence quenching technique. The antimicrobial activity of the prepared nanomaterials has also been investigated. Cyclic voltammeter (CV)) measurements analysis of the prepared nonamaterial was discussed in detail. It was proposed that the catalyst was found to be stable and reusable.
    Źródło:
    World Scientific News; 2016, 58; 97-121
    2392-2192
    Pojawia się w:
    World Scientific News
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Coating of Ordered Large-Pore Mesoporous Silica with TiO₂ Nanoparticles and Evaluation of Its Photocatalytic Activity
    Autorzy:
    Haghighatzadeh, A.
    Mazinani, B.
    Abdolahpour Salari, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/1030097.pdf
    Data publikacji:
    2017-09
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    mesoporous
    titania
    silica
    photocatalytic activity
    Opis:
    In this work, at first large pore size SiO₂ mesostructure was prepared using amphiphilic triblock copolymer (P123) as a template, tetraethyl orthosilicate (TEOS) as Si source and hexane as micelle expander by hydrothermal procedure. Separately, a stable transparent titania sol was synthesized using titanium isopropoxide (TTIP) as titanium source. Then achieved mesoporous silica structure was stirred in the titania sol resulting in formation of a titanium dioxide anatase layer on the silica structure. The sample was characterized with wide angle X-ray diffraction, N₂ adsorption-desorption analysis, X-ray photoelectron spectroscopy, field-emission scanning electron microscopy, and energy dispersive X-ray spectroscopy maps of silicon and titanium. The photocatalytic performance of prepared composite material was evaluated using UV-vis spectroscopy as well. The prepared material showed much higher photodegradation of methyl blue (MB) than commercial P-25 which was attributed to high surface area (290 m²/g), anatase phase, small crystallite size and accessible pores.
    Źródło:
    Acta Physica Polonica A; 2017, 132, 3; 420-422
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Morphology convenient flower like nanostructures of CdO-SiO2 nanomaterial and its photocatalytic application
    Autorzy:
    Kamalakkannan, J.
    Senthilvelan, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/1182834.pdf
    Data publikacji:
    2017
    Wydawca:
    Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
    Tematy:
    FE-SEM; HR-TEM; Photocatalytic activity; •OH analysis
    Opis:
    Highly efficient CdO-SiO2 nanomaterial was synthesized by Sol-gel method and sonication technique. The nanomaterial was characterized by Field-emission Scanning electron microscopy (FE-SEM) with elementary dispersive X-ray (EDX), High-resolution transmission electron microscopy (HR-TEM), photoluminescence spectroscopy (PL) and Ultraviolet-Visible diffuse reflectance spectra (DRS). The photocatalytic activity of CdO-SiO2 nanomaterial was studied from the photodegradation of Rh B as it has maximum efficiency at pH = 7 under UV-light irradiation at 365 nm. The photodegradation of dye various Catalyst loading and dye concentration is parameters have been studied. The hydroxyl radical formation in the mechanism was confirmed by fluorescence quenching technique. The mineralization of dye is confirmed by chemical oxygen demand measurements. An achievable mechanism is proposed for higher activity of CdO-SiO2 under UV-light at 365 nm. This catalyst was found to be stable and reusable.
    Źródło:
    World Scientific News; 2017, 62; 46-63
    2392-2192
    Pojawia się w:
    World Scientific News
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Photocatalytic TiO2 Nanostructures Developed on the Grade 2 Ti Material
    Autorzy:
    Tarcea, Claudia I.
    Pantilimon, Cristian Mircea
    Coman, George
    Turcanu, Andreea A.
    Predescu, Andra Mihaela
    Matei, Ecaterina
    Berbecaru, Andrei-Constantin
    Predescu, Cristian
    Powiązania:
    https://bibliotekanauki.pl/articles/2134103.pdf
    Data publikacji:
    2022
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Ti material
    nanostructures
    photocatalytic activity
    alkaline treatment
    advanced oxidation
    Opis:
    The research focused on TiO2 nanostructures environmental applications due to the special characteristics that displayed degradation of the organic compounds into environmentally friendly products through exposure to UV light. The protocol behind obtaining the nanostructures involved the use of a Ti material exposed to alkaline treatment and advanced oxidation using NaOH solution and acetone. These studied nanostructures were analyzed extensively by using methods such as scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDS) and X-ray diffraction (XRD) for characterizing the elements, compounds and morphological properties of the material. These differences in morphology is attributed to different NaOH solution concentrations. The Ti sheets were immersed into NaOH and acetone mixed solutions for 72 hours. The best results were recorded by using 30% NaOH solution. After obtaining the 3D structures, which improve specific surface and contact area with the environment, the samples were tested under UV light in order to degrade methylene blue in order to determine their photocatalytic performance.
    Źródło:
    Archives of Metallurgy and Materials; 2022, 67, 3; 1079--1084
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Facile Synthesis and Characterization of Novel CdS/BiOI Heterojunctions with Enhanced Visible-Light Photocatalytic Performances
    Autorzy:
    Fang, Shanshan
    Lu, Min
    Zhou, Man
    Li, Zhongyu
    Xu, Song
    Peng, Yanyan
    Li, Qinchi
    Lu, Dayong
    Powiązania:
    https://bibliotekanauki.pl/articles/1030343.pdf
    Data publikacji:
    2017-02
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    CdS/BiOI heterojunctions
    visible-light photocatalyst
    photocatalytic activity
    nanocomposites
    Opis:
    Novel CdS/BiOI heterojunction photocatalysts were successfully prepared by facile method. The as-prepared samples were characterized by transmission electron microscopy, field-emission scanning electron microscopy, X-ray diffraction, the Raman spectroscopy, UV-vis diffuse reflectance spectra, the Fourier transform infrared spectra, and photoluminescence. It was found that CdS nanoparticles were uniformly distributed on the surface of BiOI microspheres. The photodegradation tests showed that the photocatalytic efficiency was increased at first and then decreased when further increasing CdS content in the nanocomposites. The highest activity was obtained by 3%-CdS/BiOI nanocomposites. The enhanced photocatalytic performances were attributed to the matched band potentials of CdS and BiOI, which resulted in the efficient separation of photogenerated electron-hole pairs. Based on the experimental results, a reasonable photocatalytic mechanism of CdS/BiOI photocatalysts was also proposed.
    Źródło:
    Acta Physica Polonica A; 2017, 131, 2; 263-270
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    KTaO3 a perovskite for water and air treatment
    Autorzy:
    Różańska, Anna
    Namieśnik, Jacek
    Powiązania:
    https://bibliotekanauki.pl/articles/1179565.pdf
    Data publikacji:
    2017
    Wydawca:
    Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
    Tematy:
    hydrothermal method
    perovskite
    photocatalytic activity
    potassium tantalate
    transitions metals
    Opis:
    Perovskites are inorganic compounds that exhibit dielectric properties. These minerals belong to the crystal ceramics family. These compounds are described by the formula: ABX3 where, A and B are 2, 3 or 4 valuable metal ions, and X is an ion of oxygen or fluorine. An example of perovskite is the compound KTaO3. There are many methods for producing KTaO3, but the hydrothermal method is most commonly used. Perovskites can be characterized by magnetic, photocatalytic and electrical properties. For this reason, the most effective methods for obtaining perovskite structures are sought, and research methods for their characterization are developed. In this thesis, KTa0.8A0.2O3 (A = Co, Fe, Ni) was obtained by hydrothermal method. The influence of dopants on the photocatalytic was verified. As a result of experiments, it was found that two samples had a single phase the pyrochlore structure (KTaO3 and KTa0.8Fe0.2O3). The Ni-doping increased photocatalytic activity, while Fe-doping reduced photocatalytic activity.
    Źródło:
    World Scientific News; 2017, 75; 73-80
    2392-2192
    Pojawia się w:
    World Scientific News
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Enhancement photocatalytic activity of spinel oxide (Co, Ni)3O4 by combination with carbon nanotubes
    Autorzy:
    Kahdum, B. J.
    Lafta, A. J.
    Johdh, A. M.
    Powiązania:
    https://bibliotekanauki.pl/articles/780087.pdf
    Data publikacji:
    2017
    Wydawca:
    Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
    Tematy:
    MWCNT
    spinel oxide
    spinel/CNTs composite
    Bismarck brown G degradation
    photocatalytic activity
    Opis:
    In this study, some types of composites consisting of multi-walled carbon nanotubes (MWCNTs) and spinel oxide (Co, Ni)3 O4  were synthesized by simple evaporation method. These composites were characterized by UV–Vis diffuse reflectance spectroscopy, X-rays diffraction(XRD), Scanning electron microscopy (SEM) and specific surface area(SBET ). The photocatalytic activity of the prepared composites was investigated by the following removal of Bismarck brown G (BBG) dye from its aqueous solutions. The obtained results showed that using MWCNTs in combination with spinel oxide to produced composites (spinel/MWCNTs) which succeeded in increasing the activity of spinel oxide and exhibited higher photocatalytic activity than spinel oxide alone. Also it was found that, multiwalled carbon nanotubes were successful in increasing the adsorption and improving the activity of photocatalytic degradation of Bismarck brown G dye(BBG). The obtained results showed that spinel/MWCNTs was more active in dye removal in comparison with each of spinel oxide and MWCNTs alone under the same reaction conditions. Also band gap energies for the prepared composites showed lower values in comparison with neat spinel. This point represents a promising observation as these composites can be excited using a lower energy radiation sources.
    Źródło:
    Polish Journal of Chemical Technology; 2017, 19, 3; 61-67
    1509-8117
    1899-4741
    Pojawia się w:
    Polish Journal of Chemical Technology
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Investigation of the effect of heat treatment process on characteristics and photocatalytic activity of TiO2-UV100 nanoparticles
    Autorzy:
    Behnajady, M. A.
    Alamdari, M. E.
    Modirshahla, N.
    Powiązania:
    https://bibliotekanauki.pl/articles/208146.pdf
    Data publikacji:
    2013
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    titanium dioxide
    photocatalysis
    X ray diffraction
    Brunauer Emmett Tellers
    heat treatment
    photocatalytic activity
    dwutlenek tytanu
    ditlenek tytanu
    fotokataliza
    dyfrakcja promieniowania rentgenowskiego
    izotermy Brunauer Tellers Emmett
    obróbka cieplna
    aktywność fotokatalityczna
    Opis:
    The effect of heat treatment process on crystallite size, phase content, surface area, band gap energy and photocatalytic activity of TiO 2-UV100 nanoparticles were investigated. Heat treated TiO2 nanoparticles were characterized by X-ray diffraction (XRD), Brunauer-Emmett-Teller (BET) isotherm and diffuse reflectance spectroscopy (DRS) techniques, and its photocatalytic activity was investigated in the removal of C.I. Acid Red 88 (AR88), an anionic monoazo dye of acid class, as a model contaminant. Heat treatment process at 600 °C causes an increase in crystallite size and band gap energy of TiO2-UV100 nanoparticles. The results indicate that the nanoparticles treated for 1 h at 600 °C show the highest photocatalytic activity which can effectively degrade AR88 under UV-irradiation. Increasing heat treatment temperature above 600 °C led to reduction in TiO2 photoactivity which may be related to the anatase-rutile phase transformation, increasing particle size and decreasing specific surface area. Removal efficiency of AR88 with heat treated TiO 2-UV100 nanoparticles was sensitive to the operational parameters such as catalyst dosage, pollutant concentration and light intensity.
    Źródło:
    Environment Protection Engineering; 2013, 39, 1; 33-46
    0324-8828
    Pojawia się w:
    Environment Protection Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Photocatalytic coatings - promising way to improve a quality of urban building surfaces
    Powłoki fotokatalityczne - obiecujący sposób poprawy jakości powierzchni budynków miejskich
    Autorzy:
    Sázavská, T.
    Šubrt, J.
    Jakubičková, M.
    Peterka, F.
    Powiązania:
    https://bibliotekanauki.pl/articles/106581.pdf
    Data publikacji:
    2015
    Wydawca:
    Towarzystwo Chemii i Inżynierii Ekologicznej
    Tematy:
    TiO2-SiO2 nanocomposite
    photoactive
    transparent coatings
    self-cleaning surface
    antibacterial photocatalytic activity
    architectural heritage
    nanokompozyt TiO2-SiO2
    fotoaktywność
    powłoki przezroczyste
    samoczyszczące się powierzchnie
    antybakteryjna aktywność fotokatalityczna
    dziedzictwo architektoniczne
    Opis:
    With the increasing air pollutants particularly in the cities the deteriorating conditions of the buildings accelerate. One of the non-invasive and cheap promising ways how to prevent the buildings against the aged processes caused by biological pollutants or smog exhalation is the innovation of suitable photocatalytic coatings. This work focuses on the characterization of prepared photocatalytic nanocomposite TiO2-SiO2 system to be applied on the building objects in order to improve a quality of their surfaces. The structure and the texture characterization of prepared nanocomposite were determined by electron microscopy (SEM, TEM + EDS). The photocatalytic activity of the composite was determined considering the self-cleaning ability and the antibacterial activity. For self-cleaning characterization the methylene blue degradation was measured. These self-cleaning properties were tested on the various types of supports, which are commonly used in the building facades. To estimate antibacterial and biocidal activity the Gram-negative bacterium Escherichia coli and the gram-positive bacteria Staphylococcus aureus were used. Both methods were done according to standard ISO tests. Next to the laboratory testing the application of the composite under the real condition was implemented. There were treated parts of the concrete outside wall with the composite and after more than one year the colour changed analysis of the wall surface was characterized.
    Wraz ze wzrostem zanieczyszczenia powietrza, szczególnie w miastach, następuje coraz szybsze pogorszenie stanu budynków. Jednym z obiecujących, nieinwazyjnych i tanich sposobów zapobiegania niszczeniu budynków wywołanemu zanieczyszczeniem biologicznym lub smogiem jest stosowanie innowacyjnych powłok fotokatalitycznych. W pracy scharakteryzowano przygotowane nanokompozytowe TiO2-SiO2 systemy fotokatalityczne, wykorzystane do poprawy jakości powierzchni obiektów budowlanych. Strukturę i charakterystykę tekstury przygotowanego nanokompozytu określono metodą mikroskopii elektronowej (SEM, TEM + EDS). Oceniono aktywność fotokatalityczną kompozytu, biorąc pod uwagę jego zdolność do samooczyszczania i aktywność przeciwbakteryjną. Miarą samooczyszczania była degradacja błękitu metylowego. Właściwości samoczyszczące były badane na różnego rodzaju podłożach, powszechnie stosowanych do pokrywania fasad budynków. Do oceny właściwości antybakteryjnych i działania biobójczego wykorzystano Gram-ujemnych bakterie Escherichia coli i Gram-dodatnie bakterie Staphylococcus aureus. Badania wykonano zgodnie ze standardowymi testami ISO. Po badaniach laboratoryjnych kompozyt testowano w warunkach rzeczywistych. Badanym materiałem pokryto zewnętrzne fragmenty betonowego budynku, a po upływie ponad roku oceniono zmiany koloru tych powierzchni.
    Źródło:
    Chemistry-Didactics-Ecology-Metrology; 2015, 20, 1-2; 113-122
    2084-4506
    Pojawia się w:
    Chemistry-Didactics-Ecology-Metrology
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Highly developed construction of Heterostructured InWO3-InMoO3 loaded-TiO2 nanomaterial and Expanding multi-application
    Autorzy:
    Kamalakkannan, J.
    Senthilvelan, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/1178704.pdf
    Data publikacji:
    2017
    Wydawca:
    Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
    Tematy:
    HR-TEM
    Photocatalytic
    antibacterial activity
    electrochemical study
    Opis:
    InWO3-InMoO3 loaded-TiO2 nanomaterial was synthesised by co-precipitation method and sonication technique. The nanomaterial was characterized by High-resolution scanning electron microscopy (HR-SEM) with elementary dispersive X-ray (EDX), High-resolution transmission electron microscopy (HR-TEM), photoluminescence spectroscopy (PL) and UV-Vis diffuse reflectance spectroscopy (DRS). The photocatalytic activity of InWO3-InMoO3 loaded-TiO2 nanomaterial was studied from the photodegradation of methyl green (MEG) and methylene blue (MB) under UV-light irradiation at 365 nm. The hydroxyl radical formation in the mechanism was confirmed by fluorescence quenching technique. The mineralization confirmed by chemical oxygen demand measurements. A flaxisible mechanism is proposed for higher catalytic activity of InWO3-InMoO3-TiO2 under UV-light for 365 nm. This catalyst was found to be stable and reusable without appreciable loss of catalytic activity up to five cycles. The InWO3- InMoO3 loaded-TiO2 nanomaterial on MEG was high photocatalytic activity that of MB so high photocatalytic activity has been discussed by first order kinetics, rate constant value and high quantum yield. This material was showed increased hydrophobicity that of TiO2 electrochemical study and antibacterial activity of the analysis was also studied.
    Źródło:
    World Scientific News; 2017, 67, 2; 338-364
    2392-2192
    Pojawia się w:
    World Scientific News
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
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