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Wyświetlanie 1-15 z 749
Tytuł:
Evaluation of the quality of titanium oxide and copper oxide layers by means of optical microscopy
Autorzy:
Głuszek, A.
Sawicka-Chudy, P.
Wisz, G.
Sibiński, M.
Cholewa, M.
Powiązania:
https://bibliotekanauki.pl/articles/101772.pdf
Data publikacji:
2018
Wydawca:
Instytut Polityki Energetycznej im. Ignacego Łukasiewicza
Tematy:
titanium oxide
copper oxide
optical microscopy
histograms
Opis:
The aim of this paper is to analyse high-resolution optical images of the surface layers of titanium oxide and copper oxide. The materials were produced using the PREVAC Modular Platform for layer deposition located at the University of Rzeszów. Images with a magnification of 50x were obtained using an optical microscope. On the basis of the results obtained, the quality of the layers was evaluated based on the image analysis. The quantitative method of analysis was applied, as a result of which the conditions of the manufacturing process for which the obtained layers had the highest homogeneity were indicated. The minimum range of grey shade counting was from 65 to 150 and the maximum range from 135 to 220. The standard deviation was from 8 to 40%.
Źródło:
Energy Policy Studies; 2018, 1 (2); 39-51
2545-0859
Pojawia się w:
Energy Policy Studies
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis and Characterization of Nanocomposite Sulfonated PVDF Membrane
Autorzy:
Juliandri, Juliandri
Rukiah, Rukiah
Ernawati, E. E.
Silitonga, M. P. R.
Nasir, M.
Powiązania:
https://bibliotekanauki.pl/articles/1167197.pdf
Data publikacji:
2018
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
PVDF membrane
nanocomposites
silicon oxide
titanium oxide
Opis:
As a commercial fuel cell membrane, Nafion has disadvantages such as low stability at high temperature and low conductivity at low humidity. Sulfonated Polyvinylidene fluoride (PVDF) is known for good mechanical and thermal properties as a membrane. The purpose of this research is to synthesis a nanocomposite PVDF-TiSiO4 membrane as a potential replacement of Nafion. PVDF sulfonation was performed using concentrated sulfuric acid. The nanocomposites TiSiO4 were synthesized from TiCl4 and TEOS. Ultrasonification was used to insert the nanomaterial to the sulfonated membrane. The infrared spectra analysis shows the peak for the Ti-O-Si angel. SEM-EDX analysis shows that the nanocomposite PVDF-TiSiO4 membrane contents titanium oxide. The conductivity analysis shows the increasing of conductivity on addition of nanomaterials.
Źródło:
World Scientific News; 2018, 105; 218-224
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Adsorption of Zn2+, Cd2+ and Cu2+ on zeolites coated by manganese and iron oxides
Autorzy:
Irannajad, M.
Hhaghighi, H. K.
Soleimanipour, M.
Powiązania:
https://bibliotekanauki.pl/articles/110138.pdf
Data publikacji:
2016
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
adsorption
wastewater
manganese oxide
iron oxide
zeolite
Opis:
Adsorption of copper, cadmium and zinc on manganese and iron oxide coated zeolite from aqueous solution was investigated in a batch mode. Experiments were conducted to investigate the effects of the initial concentration of metals, initial pH, contact time and temperature on the adsorption of ions. According to the results, adsorption of ions on manganese and iron oxide coated zeolite increased with the enhancement of initial Cu2+, Zn2+ and Cd2+ concentrations and contact time and also with increase of temperature. The results showed that at the beginning, the adsorption rate of Cu2+ and Cd2+ was more than 90 %. This rate continued to be slower for Zn2+ in both zeolites. Furthermore, the amount of Cu2+, Zn2+, and Cd2+ adsorption on the manganese oxide coated zeolite (qe) was equal to 14 mg/g, 9 mg/g and 16 mg/g and on the iron oxide coated zeolite it was 11 mg/g, 7 mg/g and 13mg/g, respectively. It was shown that at the concentrations below 100 mg/dm3 adsorption was rapid and almost all heavy metals were adsorbed. As a result, the significant factor affecting qe is the proportion of weight to liquid and pH in the solutions. Finally, the results showed that the adsorption of Zn2+, Cu2+ and Cd2+ onto the manganese oxide coated zeolite followed both the Langmuir and Freundlich isotherm models.
Źródło:
Physicochemical Problems of Mineral Processing; 2016, 52, 2; 894-908
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis and Thermal Properties of Europium-Cerium Oxide as a New Fluorite-Type Ceramic Material for Thermal Barrier Coatings Applications
Autorzy:
Mikuśkiewicz, M.
Stopyra, M.
Moskal, G.
Powiązania:
https://bibliotekanauki.pl/articles/352272.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
TBC
cerium oxide
europium oxide
thermal properties
Opis:
In the present paper the structure and thermal properties of europium cerium oxides were investigated. The material for the research was obtained via solid state synthesis. The initial powders: ceria CeO2 and europia Eu2O3 were mixed in 1:1 mass ratio (non-stoichiometric proportion with the excess of CeO2) and milled. The sintering process was performed using high temperature vacuum press at 1350°C. Calorimetric analysis was conducted both for initial powders and milled mixture. The structure, phase composition and thermal diffusivity of obtained material were investigated in as-sintered condition. It was revealed that the obtained material was multi-phase. Non-stoichiometric phases including Ce0.5Eu0.5O1.75 with fluorite type structure and different lattice parameters were present. Thermal diffusivity decreased in the range from 25 to 900°C from 1.49 to 0.57 mm2 /s and then increased to 0.70 mm2 /s at 1400°C.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 4; 2089-2093
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis and Thermal Properties of Cerium-Dysprosium Oxide
Autorzy:
Mikuśkiewicz, M.
Stopyra, M.
Moskal, G.
Powiązania:
https://bibliotekanauki.pl/articles/356941.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
cerium oxide
dysprosium oxide
hermal properties
TBC
Opis:
The paper presents results of investigation on synthesis and characterization of cerium-dysprosium oxide. The input powders - dysprosium oxide Dy,sub>2O3 and cerium oxide CeO2 - were mixed so as to obtain equimolar ratio of cations, milled in alcohol and synthesized via solid state reaction process at 1350°C under 15MPa in vacuum for 2h. The microstructure, phase composition and thermal properties were analyzed. The obtained material was multiphase. Non-stoichiometric compounds were identified. Thermal diffusivity of investigated material decreased in the temperature range of 25-1000°C from 0,71 to 0,45 mm2/s.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 2B; 965-969
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Morphology and properties of the graphene layer on the copper substrate
Autorzy:
Pietrzak, K.
Olesińska, W.
Strąk, C.
Siedlec, R.
Gładki, A.
Powiązania:
https://bibliotekanauki.pl/articles/778091.pdf
Data publikacji:
2015
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
copper
graphene
graphene oxide
reduced graphene oxide
Opis:
The aim of the work presented in the article was to clarify controversial comments about anti-corrosion and mechanical properties of graphene coatings, deposited on copper substrates. It was designed special experimental cycle comprising: preparation of graphene forms and copper, the observation of layers Cu / GO (rGO) after the thermal reduction processes and oxidative test in air at 150°C temperature and 350 h in time. The resulting coatings and graphene layers were subjected to tribological test for hardness. The observed differences in the continuity of the coverage copper surface by graphene forms, allowed to understand the macroscopic effect of increased hardness and wear resistance layers rGO/Cu.
Źródło:
Polish Journal of Chemical Technology; 2015, 17, 4; 104-108
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis of Copper-based Multi-walled Carbon Nanotube Composites
Autorzy:
Domagała, K.
Borlaf, M.
Kata, D.
Graule, T.
Powiązania:
https://bibliotekanauki.pl/articles/355954.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
MWCNT
water treatment
copper
cuprous oxide
cupric oxide
Opis:
In this study, the synthesis of copper-based multi-walled carbon nanotube compositesis described. Over the last years, carbon nanotubes (CNTs) have been widely used in many scientific research fields and have found applications in several sectors, e.g. for water treatment. This work focuses on combining the exceptional characteristics of CNTs, such as high specific surface areaand antibacterial properties, with the antimicrobial / antivirus features of copper oxides. The influence of synthesis parameters and thermal treatment on the final product was studied. Copper leakage was evaluated at both pH 5 and pH 7, confirming the possibility of applying Cu-based MWCNT composites in water filtration systems.
Źródło:
Archives of Metallurgy and Materials; 2020, 65, 1; 157-162
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Investigation of Metal Oxides as Catalysts for the Thermal Decomposition of Potassium Chlorate(VII)
Autorzy:
Wojewódka, A.
Zakusylo, R.
Kravets, V.
Romanchenko, A.
Jarosz, T.
Powiązania:
https://bibliotekanauki.pl/articles/358236.pdf
Data publikacji:
2018
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
metal oxide catalysts
thermal decomposition
potassium perchlorate
manganese oxide
copper oxide
differential thermal analysis
Opis:
The results of studies on the thermal decomposition of potassium chlorate(VII) (PP) and the catalytic effects of copper, iron, nickel, titanium, magnesium, chromium and manganese oxides on the process are presented in this paper. The investigated oxides are ranked according to the magnitude of their catalytic effect; of these, CuO and МnО2 show the best catalytic performance. These oxides reduce the PP decomposition temperature from 919.3 K down to even 825.2 K. The share of the catalytic additive in the composition, required to achieve a desirable thermal decomposition profile, was found to be no more than 0.5 wt.%. The activation energy of the decomposition process was determined, using the modified Freeman and Carroll method for both neat PP and PP supplemented with MnO2; the addition of the catalyst produced a 48.8% decrease in the activation energy of thermal decomposition.
Źródło:
Central European Journal of Energetic Materials; 2018, 15, 2; 327-338
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Metody syntez i badania właściwości grafenu
Methods of synthesis and testing properties of graphene
Autorzy:
Jonik, J.
Purchała, M.
Grajek, H.
Powiązania:
https://bibliotekanauki.pl/articles/270836.pdf
Data publikacji:
2016
Wydawca:
Centralny Ośrodek Badawczo-Rozwojowy Aparatury Badawczej i Dydaktycznej, COBRABiD
Tematy:
tlenek grafitu
tlenek grafenu
zredukowany tlenek grafenu
graphite oxide
graphene oxide
reduced graphene oxide
Opis:
Grafen i jego pochodne są materiałami o unikalnych właściwościach biochemicznych, elektrycznych, optycznych i mechanicznych, co wzbudza zainteresowanie w wielu ośrodkach badawczych. Z tego powodu, na podstawie dostępnej literatury, podjęliśmy próbę zestawienia i interpretacji wyników badań uprzednio wymienionych materiałów otrzymanych różnymi metodami. Analizując wyniki badań różnych materiałów grafenopodobnych, można przypuszczać, że najbardziej ekonomiczną metodą otrzymywania grafenu jest zmodyfikowana metoda Hummersa. Najlepszymi technikami pomiarowymi są spektroskopia Ramana i rentgenowska spektroskopia fotoelektronów. Obydwie techniki umożliwiają ocenę składu chemicznego badanych próbek oraz stopnia ich zdefektowania. W pracy przedstawiono również niektóre z licznych zastosowań tych materiałów oraz wnioski.
Graphene and its derivatives are the materials with unique biochemical, electric, optical and mechanical properties, which has aroused interest in many research centres. Therefore, on the basis of the accessible literature, we attempt to collate and interpret the results of the aforesaid materials obtained by different methods. Analysing the results for the different graphene-like materials one can suppose, that the most economical method of the graphene synthesis is the modified Hummers’ method. The most useful testing techniques are the Raman spectroscopy and the X-ray photoelectron spectroscopy. Both techniques enable the estimation of the chemical composition and the presence of defect structure in the materials. Some of the many applications of the materials and conclusions are also presented in our review.
Źródło:
Aparatura Badawcza i Dydaktyczna; 2016, 21, 2; 110-117
2392-1765
Pojawia się w:
Aparatura Badawcza i Dydaktyczna
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Graphene oxide and green-synthesized reduced graphene oxide in chitosanbased nanocomposites
Autorzy:
Kosowska, K.
Domalik-Pyzik, P.
Chłopek, J.
Powiązania:
https://bibliotekanauki.pl/articles/284287.pdf
Data publikacji:
2017
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Polskie Towarzystwo Biominerałów
Tematy:
graphene oxide
reduced graphene oxide
chitosan
hydroxyapatite
biomaterial
Opis:
The first part of the paper concerns synthesis and characterization of two types of nanomaterials: graphene oxide (GO) prepared by modified Marcano method and reduced graphene oxide (rGO) synthesized using green reductant, L-ascorbic acid. Their structural properties were investigated by attenuated total reflection Fourier-transform infrared spectroscopy (ATR-FTIR) and X-ray diffraction (XRD). Results confirmed that L-ascorbic acid is an effective reducing agent. Intensity of the oxygen-groups decreased dramatically what resulted in reduction of the GO interlayer spacing from 0.8 nm to 0.4 nm. The second part of the research was concentrated on the properties of chitosan nanocomposites modified with GO and rGO. Films were prepared by mixing of the chitosan solution with the nanoparticles dispersion. Scanning electron microscopy (SEM) was used to investigate the microstructure of the composites surface. In addition, wettability and pore size of the freeze-dried scaffolds were evaluated. Results of the mechanical tests (increase in Young’s modulus) and structural characterization confirmed that chitosan solution and GO dispersion can be mixed homogeneously. Reduction of GO during composite synthesis resulted in better dispersion of the nanosheets what increased surface roughness, wettability and stability in distilled water, PBS and Ringer’s solution compared to composite with GO. After detailed biological examination, rGO-modified nanocomposites can be potentially applied in tissue engineering.
Źródło:
Engineering of Biomaterials; 2017, 20, 142; 11-16
1429-7248
Pojawia się w:
Engineering of Biomaterials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication of a Novel Silver-Based Electrical Contact Composites and Assessment of Its Mechanical and Electrical Properties
Autorzy:
Kumar, Praveen S.
Senthil, S. M.
Parameshwaran, Rathinasamy
Rathanasamy, Rajasekar
Powiązania:
https://bibliotekanauki.pl/articles/2049131.pdf
Data publikacji:
2021
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
silver tin oxide
electrical contact
composites
tungsten oxide
conductivity
Opis:
The electrical contactors play a crucial role in closing the circuit in many power distribution components like overhead lines, underground cables, circuit breakers, transformers, and control systems. The failure in these components mainly occurs due to the break-down of contactors due to the continuous opening and closing action of contacts. Silver (Ag)-based oxide contact materials are widely used in practice, among which silver tin oxide (AgSnO2) is most common. An attempt is made in increasing the performance of AgSnO2, by adding Tungsten Oxide (WO3) in various weight proportions, thus finding the optimal proportion of AgSnO2WO3 to have increased mechanical and electrical performances. All the composite samples are fabricated in-house using powder metallurgy process. The assessment of physical and electrical properties namely, density, hardness, porosity, and electrical conductivity, showed that 90%Ag-8.5%SnO2-1.5%WO3 composite yielded superior results. With help of morphological tests, wear characteristics are also investigated, which showed that 90%Ag-8.5%SnO2-1.5%WO2 composite has a wear coefficient of 0.000227 and a coefficient of friction of 0.174 at an optimized load of 10 N and sliding velocity of 0.5 mm/s.
Źródło:
Archives of Metallurgy and Materials; 2021, 66, 4; 1087-1094
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of Co2 on the Catalytic Performance Of La2O3/CeO2 and CaO/CeO2 Catalysts in the Oxidative Coupling of Methane
Autorzy:
Litawa, B.
Michorczyk, P.
Ogonowski, J.
Powiązania:
https://bibliotekanauki.pl/articles/779348.pdf
Data publikacji:
2013
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
CO2 effect
OCM
lanthanum oxide
calcium oxide
ethylene
Opis:
In this work the La2O3/CeO2 (33 mol % of La) and CaO/CeO2 (33 mol % of Ca) catalysts were prepared by the impregnation method and characterized by XRD and CO2-TPD. The catalytic properties of the catalysts were tested in the OCM process at 1073 K using the methane/oxygen mixture of the mole ratio 3.7 or 2.5 additionally containing CO2 and helium balance. It was found that in the presence of both catalysts an addition of CO2 enhances the selectivity to the ethylene and ethane and it does not have Any negative infl uence on methane conversion. In the case of the CaO/CeO2 catalyst the promoting effect of CO2 was the highest. When the partial pressure of CO2 equals to 39 kPa the increase in selectivity from 36 to 41% was noted while the conversion of methane equal to 19.4-19.7 %.
Źródło:
Polish Journal of Chemical Technology; 2013, 15, 1; 22-26
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Rhenium Addition on Microstructures and Mechanical Properties of Oxide Dispersion Strengthened Ferrtic Steels
Autorzy:
Noh, Sanghoon
Kang, Suk Hoon
Kim, Tae Kyu
Powiązania:
https://bibliotekanauki.pl/articles/354176.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
oxide dispersion strengthened steel
rhenium
oxide particles
tensile
creep
Opis:
In this study, to investigate effects of rhenium addition on the microstructures and mechanical properties, 15Cr-1Mo ODS ferritic steels with rhenium additions were fabricated by the mechanical alloying, hot isostatic pressing, and hot rolling processes. Unremarkable differences on grain morphologies and nano-oxide distributions were estimated in the microstructure observations. However, the ODS ferritic steels with 0.5 wt.% rhenium showed higher tensile and creep strengths at elevated temperature than that without rhenium. It was found that rhenium is very effective to improve the mechanical properties.
Źródło:
Archives of Metallurgy and Materials; 2020, 65, 4; 1261-1264
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructures and Mechanical Properties of ODS Ferritic Stainless Steels for High Temperature Service Applications
Autorzy:
Noh, Sanghoon
Kang, Suk Hoon
Kim, Tae Kyu
Powiązania:
https://bibliotekanauki.pl/articles/355864.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
stainless steel
oxide dispersion strengthening
oxide particles
tensile strength
Opis:
In this study, ODS ferritic stainless steels were fabricated using a commercial alloy powder, and their microstructures and mechanical properties were studied to develop the advanced structural materials for high temperature service applications. Mechanical alloying and uniaxial hot pressing processes were employed to produce the ODS ferritic stainless steels. It was revealed that oxide particles in the ODS stainless steels were composed of Y-Si-O, Y-Ti-Si-O, and Y-Hf-Si-O complex oxides were observed depending on minor alloying elements, Ti and Hf. The ODS ferritic stainless steel with a Hf addition presented ultra-fine grains with uniform distributions of fine complex oxide particles which located in grains and on the grain boundaries. These favorable microstructures led to superior tensile properties than commercial stainless steel and ODS ferritic steel with Ti addition at elevated temperature.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 3; 921-924
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Surface oxide layers with an increased carbon content for applications in oil-less tribological systems
Autorzy:
Kmita, T.
Bara, M.
Powiązania:
https://bibliotekanauki.pl/articles/185636.pdf
Data publikacji:
2012
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
tribologia
surface oxide layer
composite surface oxide layer
tribology
Opis:
The paper presents the properties of surface oxide layers with an increased content of carbon for tribological applications. The composite surface oxide layers were produced using a two-step technology through hard anodising of the surface of an aluminium alloy, followed by thermochemical treatment of anodic oxide coatings. The surface oxide layers were subjected to tribological tests in an oil-less sliding couple with T5W plastic. The presented test results confirm the usefulness of the proposed modifications of surface oxide layers for the purpose of enhancing the operational durability of oil-less sliding couples in a reciprocating motion.
Źródło:
Chemical and Process Engineering; 2012, 33, 3; 479-486
0208-6425
2300-1925
Pojawia się w:
Chemical and Process Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 749

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