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    Tytuł:
    Characterization of oxide layers made on aluminum alloy 7075 by different methods
    Charakterystyka warstw tlenkowych wytworzonych na stopie aluminium 7075 z zastosowaniem różnych metod
    Autorzy:
    Jędrusik, M.
    Dębowska, A.
    Kopia, A.
    Petrzak, P.
    Koclęga, D.
    Kalemba-Rec, I.
    Powiązania:
    https://bibliotekanauki.pl/articles/263954.pdf
    Data publikacji:
    2016
    Wydawca:
    Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Wydawnictwo AGH
    Tematy:
    oxide layers
    aluminum alloy 7075
    micro-arc oxidation
    phosphate coating
    chemical method
    warstwy tlenkowe
    stop aluminium 7075
    MAO
    fosforanowanie
    metoda chemiczna
    Opis:
    Aluminum and aluminum alloys are now being widely used as materials for structural applications due to a number of valuable properties. Improvement in the functional and decorative properties of aluminum can be obtained by forming an oxide layer on its surface. The aim of the present study was to produce and compare the properties of oxide layers on the surface of aluminum alloy 7075 and compare their properties. The methods that were used during the study were as follows: phosphating, micro-arc oxidation, and a chemical method involving the formation of a passive layer. The layers were subjected to corrosion tests. SEM and EDS methods were used for characterization of the received results. Also, some tests on an optical profilometer were done. It was proven that the micro-arc oxidation method allowed us to obtain a layer with the greatest thickness and highest corrosion resistance.
    Glin i jego stopy są obecnie powszechnie wykorzystywanym materiałem do zastosowań konstrukcyjnych ze względu stosunek masy do wytrzymałości. Poprawę własności funkcyjnych i dekoracyjnych aluminium uzyskać można przez wytworzenie warstwy tlenku na jego powierzchni. Celem badań było wytworzenie warstw tlenkowych na podłożu ze stopu aluminium 7075 i porównanie ich właściwości. Zastosowano trzy metody: fosforanowanie, micro-arc oxidation oraz metodę chemiczną polegającą na wytworzeniu warstwy pasywnej. Otrzymane powłoki poddano testom korozyjnym oraz charakteryzowano z zastosowaniem następujących metod: SEM, EDS. Wykonano też badania na profilometrze optycznym. Metoda micro-arc oxidation pozwala na uzyskanie warstwy o największej grubości oraz najlepszej odporności na korozję.
    Źródło:
    Metallurgy and Foundry Engineering; 2016, 42, 3; 187-193
    1230-2325
    2300-8377
    Pojawia się w:
    Metallurgy and Foundry Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Development and SEM/EDS characterisation of porous coatings enriched in magnesium and copper obtained on titanium by PEO with ramp voltage
    Autorzy:
    Rokosz, Krzysztof
    Hryniewicz, Tadeusz
    Pietrzak, Kornel
    Dudek, Łukasz
    Powiązania:
    https://bibliotekanauki.pl/articles/1179226.pdf
    Data publikacji:
    2017
    Wydawca:
    Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
    Tematy:
    CP Titanium Grade 2
    Micro Arc Oxidation (MAO)
    Plasma Electrolytic Oxidation (PEO)
    calcium nitrate Mg(NO3)2∙6H2O
    linear polarization
    ramp voltage
    zinc nitrate Ca(NO3)2∙3H2O
    Opis:
    In the present paper, the SEM and EDS results of porous and enriched in calcium and/or zinc coatings, which were obtained during 3-minute treatments by Plasma Electrolytic Oxidation/ Micro Arc Oxidation processes on CP Titanium Grade 2 at ramp potentials (liner polarization) from 0 up to 650 VDC in electrolytes containing 500 g Mg(NO3)2∙6H2O and/or 500 g Cu(NO3)2∙3H2O in 1 L H3PO4, are reported. It was found that the obtained coatings, dependent on the PEO process conditions, have pores with different shapes and diameters. The Mg/P and Cu/P ratios by atomic concentration are the same and equal to 0.09±0.01 (by wt %) | 0.11±0.01 (by at%) and/or 0.40±0.08 (by wt %) | 0.19±0.04 (by at%), respectively. That may testify the hydroxyapatite-like structures of Mg-Ti-PO43– and/or Cu-Ti-PO43– have been identified to occur.
    Źródło:
    World Scientific News; 2017, 80; 29-42
    2392-2192
    Pojawia się w:
    World Scientific News
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Fabrication and characterisation of porous coatings obtained by plasma electrolytic oxidation
    Autorzy:
    Rokosz, K.
    Hryniewicz, T.
    Raaen, S.
    Malorny, W.
    Powiązania:
    https://bibliotekanauki.pl/articles/95249.pdf
    Data publikacji:
    2017
    Wydawca:
    Politechnika Koszalińska. Wydawnictwo Uczelniane
    Tematy:
    Plasma Electrolytic Oxidation
    PEO
    micro arc oxidation
    MAO
    CP Titanium Grade 2
    niobium
    Ti2448
    Ti6Al4V
    TNZ
    plazmowe utlenianie elektrolityczne
    utlenianie mikro-łukowe
    tytan
    stopy tytanu
    niob
    Opis:
    In the paper, characteristics of porous coatings enriched in copper on pure Titanium and its alloys (NiTi, Ti6Al4V, TNZ, Ti2448) as well as on niobium obtained by Plasma Electrolytic Oxidation (PEO) in electrolyte containing H3PO4 within Cu(NO3)2, are presented. All obtained surfaces of PEO coatings have different shapes and diameters of pores. The binding energies of main peaks for titanium Ti2p3/2, niobium Nb3d5/2, zirconium Zr3d5/2, phosphorus (P2p) and oxygen (O1s) suggest the presence of titanium Ti4+, niobium Nb5+ and zirconium Zrx+ (x≤2) as well as PO4 3–.
    Źródło:
    Journal of Mechanical and Energy Engineering; 2017, 1, 1; 23-30
    2544-0780
    2544-1671
    Pojawia się w:
    Journal of Mechanical and Energy Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Porous PEO coatings on titanium, obtained under DC regime, enriched in magnesium, calcium, zinc, and copper
    Autorzy:
    Rokosz, Krzysztof
    Hryniewicz, Tadeusz
    Pietrzak, Kornel
    Dudek, Łukasz
    Powiązania:
    https://bibliotekanauki.pl/articles/1156239.pdf
    Data publikacji:
    2018
    Wydawca:
    Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
    Tematy:
    plasma electrolytic oxidation (peo)
    micro arc oxidation (mao)
    cp titanium grade 2
    calcium nitrate ca(no3)2•4h2o
    magnesium nitrate mg(no3)2∙6h2o
    zinc nitrate zn(no3)2∙6h2o
    copper nitrate cu(no3)2∙3h2o
    Opis:
    In the present paper, the analysis of SEM and EDS results of porous and enriched in calcium, magnesium, zinc, copper and phosphorus coatings, obtained during 3-minute treatments performed by Plasma Electrolytic Oxidation (PEO)/Micro Arc Oxidation (MAO) processes on CP Titanium Grade 2, is presented. The PEO process was carried out at DC potentials of 500 VDC, 575 VDC, and 650 VDC in electrolytes containing 125 g Ca(NO3)2•4H2O, and 125 g Mg(NO3)2∙6H2O, and 125 g Zn(NO3)2∙6H2O, and 125 g Cu(NO3)2∙3H2O in 1 L H3PO4. It was found that obtained coatings have pores with different shapes and diameters and/or size/dimentions. The Ca/P, Mg/P, Zn/P, Cu/P, and M/P ratios (M=Ca+Mg+Zn+Cu) were equal to 0.074, 0.046, 0.056, 0.042, and 0.218, respectively. The highest value of each of these ratios was recorded for 650 VDC. It may be concluded that the obtained PEO coatings structures most likely are similar to hydroxyapatite-like structures, in which the Ca2+ may be replaced with Zn2+, Mg2+, Cu2+.
    Źródło:
    World Scientific News; 2018, 94, 2; 99-114
    2392-2192
    Pojawia się w:
    World Scientific News
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Powierzchniowa modyfikacja stopu tytanu z zastosowaniem elektrolitycznoplazmowego utleniania
    Surface modification of titanium alloy by micro-arc oxidation
    Autorzy:
    Karbowniczek, J.
    Buzgo, M.
    Muhaffel, F.
    Czyrska-Filemonowicz, A.
    Powiązania:
    https://bibliotekanauki.pl/articles/285992.pdf
    Data publikacji:
    2013
    Wydawca:
    Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Polskie Towarzystwo Biominerałów
    Tematy:
    stop tytanu
    elektrolityczno-plazmowe utlenianie
    powłoka hydroksyapatytowa
    titanium alloy
    micro-arc oxidation
    hydroxyapatite coatings
    Opis:
    Implanty na bazie stopów tytanu są z powodzeniem stosowane w ortopedii i dentystyce. W celu poprawienia integracji implantu z kością wykonano porowatą, hydroksyapatytową powłoką na stopie Ti-6Al-7Nb techniką elektrolityczno-plazmowego utleniania. Otrzymaną powłokę poddano analizie pod kątem mikrostruktury, chropowatości i składu fazowego. Dodatkowo wykonano wstępne badania in vitro.
    Titanium based implants are used both in orthopedics and dentistry. For better integration of implant with bone porous, hydroxyapatite crystals containing coating was deposited on Ti-6Al-7Nb alloy by microarc oxidation process. Microstructure, roughness and phases composition of the coating was analyzed. Moreover preliminary in vitro studies were done.
    Źródło:
    Engineering of Biomaterials; 2013, 16, no. 122-123 spec. iss.; 40-42
    1429-7248
    Pojawia się w:
    Engineering of Biomaterials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    SEM and EDS analysis of enriched in phosphorus and copper coatings fabricated by AC-PEO treatment
    Autorzy:
    Rokosz, Krzysztof
    Hryniewicz, Tadeusz
    Pietrzak, Kornel
    Dudek, Łukasz
    Powiązania:
    https://bibliotekanauki.pl/articles/1178082.pdf
    Data publikacji:
    2018
    Wydawca:
    Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
    Tematy:
    CP Titanium Grade 2
    Micro Arc Oxidation (MAO)
    Plasma Electrolytic Oxidation (PEO)
    copper nitrate Cu(NO3)2∙3H2O
    Opis:
    In the present paper, SEM and EDS studies of coatings obtained on CP Titanium Grade 2 under sinusoidal alternating voltage (AC) with frequency 50 Hz in Plasma Electrolytic Oxidation (PEO) process at voltages of 200 Vpp, 250 Vpp and 300 Vpp during 3-minute treatments, are displayed. Based on SEM micrographs it may be stated that the porous surfaces, which are needed for biomedical and catalysis application, are obtained only for samples fabricated at 200 Vpp. It was found out that thickest and most morphologically developed surfaces were obtained at 200 Vpp, too. The surfaces obtained at 250 Vpp and 300 Vpp are cracked and had low concentration of copper, i.e. 0.9 at% and 1.1 at%, respectively, while that one obtained at 200 Vpp was porous and had 8.6 at% copper.
    Źródło:
    World Scientific News; 2018, 95; 246-259
    2392-2192
    Pojawia się w:
    World Scientific News
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    SEM and EDS studies of porous coatings enriched in calcium and zinc obtained by PEO with ramp voltage
    Autorzy:
    Rokosz, Krzysztof
    Hryniewicz, Tadeusz
    Pietrzak, Kornel
    Powiązania:
    https://bibliotekanauki.pl/articles/1178366.pdf
    Data publikacji:
    2017
    Wydawca:
    Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
    Tematy:
    CP Titanium Grade 2
    Micro Arc Oxidation (MAO)
    Plasma Electrolytic Oxidation (PEO)
    calcium nitrate Ca(NO3)2∙4H2O
    linear polarization
    ramp voltage
    zinc nitrate Zn(NO3)2∙6H2O
    Opis:
    In this work, the SEM and EDS results of porous and enriched in calcium or zinc coatings, which were obtained during 3-minute treatments using Plasma Electrolytic Oxidation (Micro Arc Oxidation) processes on CP Titanium Grade 2 at ramp potentials (linear polarization) from 0 up to 650 VDC in electrolytes containing 500 g Ca(NO3)2∙4H2O and/or 500 g Zn(NO3)2∙6H2O in 1 L H3PO4, are presented. It was found that obtained coatings have pores with different shapes and diameters. The Ca/P and Zn/P ratios by atomic concentration are the same and equal to 0.2, what may suggest hydroxyapatite-like structure (M,Ti)x(PO4)y, where M = {Ca, Zn}.
    Źródło:
    World Scientific News; 2017, 77, 2; 242-255
    2392-2192
    Pojawia się w:
    World Scientific News
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    SEM and EDS studies of selected porous coatings obtained on titanium by Plasma Electrolytic Oxidation
    Autorzy:
    Rokosz, Krzysztof
    Hryniewicz, Tadeusz
    Pietrzak, Kornel
    Dudek, Łukasz
    Malorny, Winfried
    Powiązania:
    https://bibliotekanauki.pl/articles/1178480.pdf
    Data publikacji:
    2017
    Wydawca:
    Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
    Tematy:
    CP Titanium Grade 2
    Micro Arc Oxidation (MAO)
    Plasma Electrolytic Oxidation (PEO)
    calcium nitrate Ca(NO3)2∙4H2O
    copper nitrate Cu(NO3)2∙3H2O
    magnesium nitrate Mg(NO3)2∙6H2O
    Opis:
    In present work, SEM and EDS results of porous and enriched in calcium, copper, magnesium and phosphorus coatings, which were obtained during 3-minute treatments of Plasma Electrolytic Oxidation PEO (Micro Arc Oxidation MAO) processes on CP Titanium Grade 2 at two potentials, i.e. 500 VDC and 650 VDC, are presented. It was found that the voltage of that process influences the chemical composition of coatings shapes obtained on titanium in electrolytes containing calcium, copper and magnesium nitrates. The pores shapes of PEO coatings formed on titanium in electrolytes containing calcium, copper and magnesium nitrates are presented, too. In addition, it was also noted that with using of higher voltage (here 650 VDC) of PEO treatments, the higher Ca/P, Cu/P and Mg/P ratios were found than those after treatments at 500 VDC.
    Źródło:
    World Scientific News; 2017, 70, 2; 71-85
    2392-2192
    Pojawia się w:
    World Scientific News
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Synthesis and characterisation of porous, calcium enriched coatings formed on Titanium via Plasma Electrolytic Oxidation
    Autorzy:
    Rokosz, Krzysztof
    Hryniewicz, Tadeusz
    Pietrzak, Kornel
    Powiązania:
    https://bibliotekanauki.pl/articles/1179160.pdf
    Data publikacji:
    2017
    Wydawca:
    Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
    Tematy:
    85% orthophosphoric acid H3PO4
    CP Titanium Grade 2
    Micro Arc Oxidation (MAO)
    Plasma Electrolytic Oxidation (PEO)
    calcium nitrate tetrahydrate Ca(NO3)2∙4H2O
    Opis:
    The SEM and EDS study results of porous and calcium enriched coatings obtained via Plasma Electrolytic Oxidation (Micro Arc Oxidation) on the Commercial Purity Titanium Grade 2 samples, at three potentials 450 VDC, 550 VDC, 650 VDC in electrolytes containing 500 g Ca(NO3)2∙4H2O in 1000 mL H3PO4, are presented in the paper. In the same electrolyte three Titanium samples, one after other, were treated, with the PEO processing time equaling 3 minutes after each immersion. Based on SEM and EDS results, it was possible to state that all obtained coatings are porous and their calcium-to-phosphorus (Ca/P) ratio decreases with decreasing PEO voltage. In addition, it was found out that electrolyte aging results in decreasing Ca/P ratio, too.
    Źródło:
    World Scientific News; 2017, 83; 29-44
    2392-2192
    Pojawia się w:
    World Scientific News
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The technology of preparing green coating by conducting micro-arc oxidation on AZ91D magnesium alloy
    Autorzy:
    Wang, S.
    Liu, P.
    Powiązania:
    https://bibliotekanauki.pl/articles/778739.pdf
    Data publikacji:
    2016
    Wydawca:
    Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
    Tematy:
    magnesium alloy
    micro-arc oxidation
    coating
    Opis:
    Micro-arc oxidation was applied to AZ91D magnesium alloy by taking K2Cr2O7  as the colouring salt in the silicate system. It was shown that the green coating obtained through performing micro-arc oxidation on magnesium alloy consisted of Mg, Mg2SiO4 , MgO, and Mg2SiO4  based on analysis of X-ray diffraction (XRD), and scanning electron microscopy (SEM). Among which, Mg2SiO4 was the colouring salt; there were something in the lamellar, pit, and convex forms found on the surface of the coating. The coating consisted of a porous, and a compact, layer from the outside to the inside. As demonstrated, the colour of the coating depended on the K2Cr2O7 concentration: it became gradually deeper with the addition of K2Cr2O7 and the increasing micro-arc oxidation time. The corrosion resistance and hardness of the green coating were greater than that of the matrix.
    Źródło:
    Polish Journal of Chemical Technology; 2016, 18, 4; 36-40
    1509-8117
    1899-4741
    Pojawia się w:
    Polish Journal of Chemical Technology
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
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