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    Wyświetlanie 1-4 z 4
    Tytuł:
    UV polymerization and property analysis of maleacylated methyl cellulose acrylic acid absorbent resin
    Autorzy:
    Li, Ying
    Sawut, Amatjan
    Hou, Gongbo
    He, Mingyu
    Yimit, Mamatjan
    Powiązania:
    https://bibliotekanauki.pl/articles/778577.pdf
    Data publikacji:
    2020
    Wydawca:
    Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
    Tematy:
    ultraviolet
    maleylated methylcellulose
    absorbent resin
    Opis:
    In this paper, maleic anhydride (MA) was grafted onto methyl cellulose (MC) and then reacted with acrylic acid to synthesize a high gel strength and fast water absorption resin (AA-co-MC-g-MA) by UV polymerization. The reaction conditions of maleylated methylcellulose (MC-g-MA) were investigated, including the ratio of MC to MA, reaction time and catalyst amount. In addition, the reaction conditions for the synthesis of super absorbent resin were as follows: the amount of MC-g-MA, the degree of substitution of MC-g-MA, polymerization time, and the amount of initiator. Under optimal conditions, the maximum water absorption volume of synthetic resin was 2116 g/g, and the maximum salt absorption rate was 139 g/g. The water absorption resin prepared this time had high water absorption, water retention, excellent pH sensitivity, etc. It was hoped that it will have a good application prospect in the field of industrial production and agriculture in the future.
    Źródło:
    Polish Journal of Chemical Technology; 2020, 22, 2; 34-41
    1509-8117
    1899-4741
    Pojawia się w:
    Polish Journal of Chemical Technology
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Development and validation of analytical method for assessment of calcium dobesilate in varied hydrogel compositions
    Autorzy:
    Lisik, Anna
    Pilch, Ewa
    Słowiak, Laura
    Musiał, Witold
    Powiązania:
    https://bibliotekanauki.pl/articles/895665.pdf
    Data publikacji:
    2018-08-31
    Wydawca:
    Polskie Towarzystwo Farmaceutyczne
    Tematy:
    HPLC
    Hydrogel
    validation
    calcium dobesilate
    methylcellulose
    Opis:
    Standardized analytical methods for testing pharmaceutical preparations are not readily available in the literature for calcium dobesilate hydrogels. The aim of the study was to develop and validate analytical method for methylcellulose gel containing calcium dobesilate as an active ingredient. Samples from dissolution experiments were assessed via HPLC with UV-VIS detector. The optimal composition of mobile phase included acetonitrile with water 1:1, acidified to 2.5 pH value. The applied column was Standard Purospher Star 18e 250 x 4.6 (5µm), and the maximum wavelength was set on 240 nm, at 25 °C. The total run time of analysis was set at 5 min and acquired retention time was 2.7 and 3.1 min for calcium dobesilate depending on the hydrogel formulation. Validity study of the method revealed that all obtained calibration curves showed good linearity (r2 > 0.9927). Linearity (100% level) was found to be 99.42, 100.12, 99.48, 99.89, 100.70, 100.08, 99.82, 100.23 for A, B, C, D, E, F, G and H formulation, respectively. Accuracy was in the range of 98-102% on three different spike levels for all eight formulations. Precision results was around 100% with RSD lower than 1% in all cases indicating that the method can be used as a validated method. Limit of quantitation (LOQ) was found to be 13.25 μg∙ml-1 for all eight formulations. The method is feasible for evaluation of hydrophilic gels with calcium dobesilate.
    Źródło:
    Acta Poloniae Pharmaceutica - Drug Research; 2018, 75, 4; 843-849
    0001-6837
    2353-5288
    Pojawia się w:
    Acta Poloniae Pharmaceutica - Drug Research
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Application of chitosan in the formulation of methyl cellulose-based hydrogels
    Autorzy:
    Szcześniak, Maria
    Grimling, Bożena
    Meler, Jan
    Pluta, Janusz
    Powiązania:
    https://bibliotekanauki.pl/articles/1035190.pdf
    Data publikacji:
    2014
    Wydawca:
    Sieć Badawcza Łukasiewicz - Polskie Towarzystwo Chitynowe
    Tematy:
    chitosan
    methylcellulose
    pharmaceutical availability
    rheological parameters
    Opis:
    The aim of this work was to study the properties of methylcellulose hydrogels with supplements containing chitosan and 1% hydrocortisone. Depending on the composition of the substrate, gels are characterised by a variety of pharmaceutical availabilities. Increasing the concentration of chitosan has an influence on increasing the viscosity, hardness, and cohesiveness of the tested gels.
    Źródło:
    Progress on Chemistry and Application of Chitin and its Derivatives; 2014, 19; 139-144
    1896-5644
    Pojawia się w:
    Progress on Chemistry and Application of Chitin and its Derivatives
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Comparative study on physicochemical properties of alpha-TCP / calcium sulphate dihydrate biomicroconcretes containing chitosan, sodium alginate or methylcellulose
    Autorzy:
    Czechowska, Joanna
    Zima, Aneta
    Ślósarczyk, Anna
    Powiązania:
    https://bibliotekanauki.pl/articles/307328.pdf
    Data publikacji:
    2020
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    alpha-tricalcium phosphate
    calcium sulphate
    chitosan
    sodium alginate
    methylcellulose
    biomicroconcrete
    siarczan wapnia
    chitozan
    alginian sodu
    metyloceluloza
    Opis:
    Recently, the attention has been drawn to complex systems – biomicroconcretes composed of a bone cement matrix and resorbable granules or microspheres. This paper presents novel bone substitutes composed of α-tricalcium phosphate (α-TCP; cement matrix), calcium sulphate dihydrate granules (GCSD; aggregates in biomicroconcrete) and various polymers (chitosan, sodium alginate, methylcellulose) used for the improvement of material properties. The aim of this work was to study α-TCP-GCSD-polymer interactions and to compare the impact of organic additives on the physicochemical properties of biomicroconcretes. Methods: Scanning electron microscopy (SEM), mercury intrusion porosimetry (MIP), X-ray diffractometry (XRD) as well as universal testing machine (INSTRON), Gilmore apparatus and pH/ conduct-meter were used. Results: The chemical bonding between α-TCP matrix and CSD granules resulted in a compressive strength appropriate for low-load bearing applications (7–12 MPa) and clinically relevant setting times (8–33 min). Biomicroconcretes consisting of sodium alginate possessed the highest mechanical strength (12 ± 2 MPa). It has also been found that the dissolution-precipitation reactions of the α-TCP were retarded with the addition of chitosan and acetic acid. This effect was not observed in the case of methylcellulose and sodium alginate. Chemical stability and bioactivity of materials were demonstrated during in vitro studies in simulated body fluid. Conclusions: Materials containing calcium sulphate-based granules were surgically handy, possessed promising physicochemical properties and are supposed to ensure desired macroporosity as well as gradual resorption in vivo. It has been demonstrated that the presence of CSD granules and polymers influenced the physicochemical properties of composites.
    Źródło:
    Acta of Bioengineering and Biomechanics; 2020, 22, 1; 47-56
    1509-409X
    2450-6303
    Pojawia się w:
    Acta of Bioengineering and Biomechanics
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-4 z 4

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