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    Wyświetlanie 1-3 z 3
    Tytuł:
    Hyperfine interactions and some thermomagnetic properties of amorphous FeZr(Cr)NbBCu alloys
    Autorzy:
    Łukiewska, A.
    Olszewski, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/146540.pdf
    Data publikacji:
    2017
    Wydawca:
    Instytut Chemii i Techniki Jądrowej
    Tematy:
    amorphous Fe-based alloys
    invar effect
    Mössbauer spectroscopy
    Opis:
    In this research, we studied the magnetic phase transition by Mössbauer spectroscopy and using vibrating sample magnetometer for amorphous Fe86–xZr7CrxNb2Cu1B4 (x = 0 or 6) alloys in the as-quenched state and after accumulative annealing in the temperature range 600–750 K. The Mössbauer investigations were carried out at room and nitrogen temperatures. The Mössbauer spectra of the investigated alloys at room temperature are characteristic of amorphous paramagnets and have a form of asymmetric doublets. However, at nitrogen temperature, the alloys behave like ferromagnetic amorphous materials. The two components are distinguished in the spectrum recorded at both room and nitrogen temperatures. The low field component in the distribution of hyperfine field induction shifts towards higher field with the annealing temperature. It is assumed that during annealing at higher temperature, due to diffusion processes, the grains of α-Fe are created in the area corresponding to this component. Both investigated alloys show the invar effect and the decrease of hyperfine field induction after annealing at 600 K for 10 min is observed. It is accompanied by the lowering of Curie temperature.
    Źródło:
    Nukleonika; 2017, 62, 2; 135-140
    0029-5922
    1508-5791
    Pojawia się w:
    Nukleonika
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effects of Co, Ni, and Cr addition on microstructure and magnetic properties of amorphous and nanocrystalline Fe86−xMxZr7Nb2Cu1B4 (M = Co, Ni, CoCr, and Cr, x = 0 or 6) alloys
    Autorzy:
    Łukiewska, A.
    Świerczek, J.
    Hasiak, M.
    Olszewski, J.
    Zbroszczyk, J.
    Gębara, P.
    Ciurzyńska, W.
    Powiązania:
    https://bibliotekanauki.pl/articles/147169.pdf
    Data publikacji:
    2015
    Wydawca:
    Instytut Chemii i Techniki Jądrowej
    Tematy:
    amorphous materials
    nanocrystalline materials
    Mössbauer spectroscopy
    invar effect
    Curie temperature
    Opis:
    Mössbauer spectra and thermomagnetic curves for the Fe86-xMxZr7Nb2Cu1B4 (M = Co, Ni, CoCr, and Cr, x = 0 or 6) alloys in the as-quenched state and after the accumulative annealing in the temperature range 600–800 K for 10 min are investigated. The parent Fe86Zr7Nb2Cu1B4 amorphous alloy is paramagnetic at room temperature, and substitution of 6 at.% of Fe by Co, Ni, and CoCr changes the magnetic structure – the alloys become ferromagnetic, whereas replacing 6 at.% of Fe with Cr preserves the paramagnetic state. After the heat treatment at 600 K, the decrease of the average hyperfi ne fi eld induction, as compared to the as-quenched state, is observed due to the invar effect. After this annealing, the Curie temperature for all investigated alloys decreases. The accumulative annealing up to 800 K leads to the partial crystallization; α-Fe or α-FeCo grains with diameters in the range of 12–30 nm in the residual amorphous matrix appear.
    Źródło:
    Nukleonika; 2015, 60, 1; 103-108
    0029-5922
    1508-5791
    Pojawia się w:
    Nukleonika
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Microstructure studies of amorphous and nanocrystalline (Fe1-xCox)85.4Zr6.8-yMyB6.8Cu1 (x = 0 or 0.1, y = 0 or 1, M = Mo, Nb or Nd) alloys
    Autorzy:
    Olszewski, J.
    Zbroszczyk, J.
    Fukunaga, H.
    Ciurzyńska, W.
    Świerczek, J.
    Hasiak, M.
    Perduta, K.
    Łukiewska, A.
    Młyńczyk, A.
    Powiązania:
    https://bibliotekanauki.pl/articles/147229.pdf
    Data publikacji:
    2004
    Wydawca:
    Instytut Chemii i Techniki Jądrowej
    Tematy:
    Invar effect
    nanocrystalline alloys
    interfacial zone
    Opis:
    The amorphous and nanocrystalline (Fe1 xCox)85.4Zr6.8 yMyB6.8Cu1 (x = 0 or 0.1, y = 0 or 1, M = Mo, Nb or Nd) alloys were studied using Mössbauer spectroscopy. We have stated that after the low temperature annealing of the samples the decrease of the average hyperfine field due to the Invar effect was observed. This effect is associated with the increase of atom packing density after the annealing of the samples, which may lead to the noncolinear spin state in some regions. This phenomenon was completely suppressed after substitution of 10% of Fe atoms by Co atoms. At early stages of crystallization of the Fe85.4Zr6.8 yMyB6.8Cu1 (y = 0 or 1, M = Mo, Nb or Nd) alloys, the interfacial zone is poor in iron due to diffusion of Zr, B, Nb, Mo and Nd atoms outside regions where á-Fe fine grains are created. However, the iron content in the amorphous matrix is the same as in the as-quenched state. The iron concentration in the interfacial zone of the nanocrystalline alloys obtained by the accumulative annealing depends on the chemical composition of the as-quenched samples. In the nanocrystalline samples obtained by two-step annealing, the iron content in the interfacial layer is higher than in the amorphous matrix.
    Źródło:
    Nukleonika; 2004, 49,suppl.3; 79-83
    0029-5922
    1508-5791
    Pojawia się w:
    Nukleonika
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-3 z 3

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