Informacja

Drogi użytkowniku, aplikacja do prawidłowego działania wymaga obsługi JavaScript. Proszę włącz obsługę JavaScript w Twojej przeglądarce.

English (EN)·Polski (PL)·Yкраїнський (UK)
Przejdź do strony domowej biblioteki Centralna Biblioteka Wojskowa Link otwiera się w nowym oknie Logo biblioteki Prolib Integro - strona głównaCentralna Biblioteka Wojskowa

Wyszukujesz frazę "in situ X-ray diffraction" wg kryterium: Temat

  Lista filtrów
Wyrównaj
    Wyświetlanie 1-2 z 2
    Tytuł:
    Thermally Induced Polymorphic Transformation of Hexanitrohexaazaisowurtzitane (HNIW) Investigated by in-situ X-ray Powder Diffraction
    Autorzy:
    Liu, Y.
    Li, S.
    Wang, Z.
    Xu, J.
    Sun, J.
    Huang, H.
    Powiązania:
    https://bibliotekanauki.pl/articles/358065.pdf
    Data publikacji:
    2016
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    HNIW
    polymorphism
    in situ X-ray diffraction
    phase transition
    heat stimulation
    Opis:
    The ε→γ phase transition of HNIW induced by heat was investigated with in situ X-ray powder diffraction (PXRD). The effects of purity, particle size, insensitive additives and the time of isothermal heat treatment on the phase transition were evaluated. It was found that the phase transition is irreversible with changes in temperature, and the two phases can coexist in a certain temperature range. Moreover, the initial phase transition temperature increases with increasing purity and decreasing particle size of HNIW, and thus with the approximate crystal density. The addition of graphite and paraffin wax to HNIW as insensitive additives leads to a decrease in the initial phase transition temperature, but the addition of TATB does not affect the initial phase transition temperature. Thus, TATB is a suitable insensitive additive. Moreover, at the critical temperature, the isothermal time determined the efficiency of the ε- to γ-phase transition. This work lays the foundations for the choice of molding technologies, performance test methods, ammunition storage options, as well as the manufacture of HNIW-based explosive formulations.
    Źródło:
    Central European Journal of Energetic Materials; 2016, 13, 4; 1023-1037
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Micromechanical Properties and Stress Measurements with Diffraction Methods
    Autorzy:
    Gadalińska, E.
    Baczmański, A.
    Powiązania:
    https://bibliotekanauki.pl/articles/97807.pdf
    Data publikacji:
    2013
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Lotnictwa
    Tematy:
    X-ray diffraction
    stress measurements on riveted samples
    duplex steel
    composites
    stress measurements during in-situ tensile test
    stress concentarion tensor
    necking phenomenon
    Opis:
    Diffraction methods are commonly used for the determination of the elastic lattice deformation and distortion from the displacement and broadening of the diffraction peak. These methods enable researchers to measure stresses and elastic properties of polycrystalline materials. The main advantages of diffraction methods are their non-destructive character and the possibility of macrostress and microstress analysis for multiphase and anisotropic materials. Measurements are performed selectively only for crystallites contributing to the measured diffraction peak, i.e. for the grains having lattice orientations for which the Bragg condition is satisfied. When several phases are present in the sample, measurements of separate diffraction peaks allow for the behaviour of each phase to be investigated independently. This method can be applied without any limitations to flat specimens. Numerical calculations of residual stresses around the rivets imply a very high stress gradientin the case of tangential stresses as well in the case of radial stresses. Attempting to verify these predictions, the residual stress measurements with an X-ray diffractometer were performed on riveted samples after the riveting process. In addition, complementary measurements of strain values with strain gauges during the riveting process were performed as well as the finite elements modelling. The aim of these measurements was to determine the stress values around the rivets and to compare results obtained with different techniques. On the other hand, the multi-scale crystallographic model of elastoplastic deformation is very convenient for the study of elastoplastic properties in microscopic and macroscopic scales. Comparison of experimental data with model predictions allows us to understand the physical phenomena that occur during a sample's deformation at the level of polycrystalline grains. Moreover, the micro and macro parameters of elastoplastic deformation can be experimentally established. It should be stated that the characterisation of the residual stress field and elastic properties is important in the study of the mechanical behaviour of polycrystalline materials, including plasticity and damage phenomena. In this work, a new analysis method of neutron diffraction results obtained during in-situ tensile load is proposed and tested. The methodology is based on the measurements of lattice strains during in-situ tensile testing for several hkl reflections and for different orientations of the sample with respect to the scattering vector. As the result, the full stress tensor for preferred texture orientations in function of the applied stress can be determined using the crystallite group method. The experimental data are presented and compared with the self-consistent model calculations performed for groups of grains selected by different hkl reflections.
    Źródło:
    Fatigue of Aircraft Structures; 2013, 5; 18-39
    2081-7738
    2300-7591
    Pojawia się w:
    Fatigue of Aircraft Structures
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-2 z 2

      Ta witryna wykorzystuje pliki cookies do przechowywania informacji na Twoim komputerze. Pliki cookies stosujemy w celu świadczenia usług na najwyższym poziomie, w tym w sposób dostosowany do indywidualnych potrzeb. Korzystanie z witryny bez zmiany ustawień dotyczących cookies oznacza, że będą one zamieszczane w Twoim komputerze. W każdym momencie możesz dokonać zmiany ustawień dotyczących cookies