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    Tytuł:
    Determination of Glass Transition Temperature of Double-Base Rocket Propellants with the Use of Dynamic Mechanical Analysis
    Autorzy:
    Cegła, M.
    Zmywaczyk, J.
    Koniorczyk, P.
    Miszczak, M.
    Borkowski, J.
    Florczak, B.
    Powiązania:
    https://bibliotekanauki.pl/articles/403426.pdf
    Data publikacji:
    2015
    Wydawca:
    Wojskowa Akademia Techniczna im. Jarosława Dąbrowskiego
    Tematy:
    dynamic mechanical analysis
    glass transition
    double base rocket propellants
    Opis:
    The paper presents results of Dynamic Mechanical Analysis (DMA) of double-base (DB) solid rocket propellant with special attention paid to determining the glass transition temperature. The presented experiments were carried out with the use of Netzsch DMA 242C analyzer with the dual cantilever operation mode. Advantages and drawbacks of the DMA method, measured values, as well as important characteristics of solid double-base rocket propellants were briefly described. Obtained values of the storage modulus E', the loss modulus E", and tand were represented in dependence on temperature. The glass transition temperature of the tested propellant was determined according to NATO standard 4540 [7] at the peak of the loss modulus curve.
    Źródło:
    Problemy Mechatroniki : uzbrojenie, lotnictwo, inżynieria bezpieczeństwa; 2015, 6, 1 (19); 11-18
    2081-5891
    Pojawia się w:
    Problemy Mechatroniki : uzbrojenie, lotnictwo, inżynieria bezpieczeństwa
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Dynamic Mechanical Properties of Artifcially Aged Double Base Rocket Propellant and the Possibilities for the Prediction of Their Service Lifetime
    Autorzy:
    Matečić-Mušanić, S.
    Sućeska, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/358886.pdf
    Data publikacji:
    2013
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    ageing
    double base rocket propellants
    dynamic mechanical analysis
    glass transition temperature
    lifetime prediction
    loss modulus
    softening temperature
    storage modulus
    tan δ
    Opis:
    The ageing of double base (DB) rocket propellants, as a consequence of the chemical reactions and physical processes that take place over time, has a signifcant effect on their relevant properties, such as chemical composition and mechanical and ballistic properties. The changes to relevant properties limit the safe and reliable service life of DB rocket propellants. Accordingly, numerous research efforts have been undertaken to fnd reliable methods to measure the changes caused by ageing in order to assess the quality of DB rocket propellants at a given moment of their lifetime, and to predict their remaining service lifetime. In this work we studied the dynamic mechanical properties of DB rocket propellant artifcially aged at temperatures of 80, 85 and 90 °C, in order to detect and quantify changes in the dynamic mechanical properties caused by ageing, and to investigate the possibilities for the prediction of service lifetime. Dynamic mechanical properties were studied using a dynamic mechanical analyser (DMA). The results obtained have shown that ageing causes signifcant changes in the storage modulus (E´), the loss modulus (E˝) and the tan δ curves’ shape and position. These changes are quantifed by following some characteristic points on the E´-T, E˝-T, and tan δ-T curves (e.g. glass transition temperatures; storage modulus, loss modulus and tan δ at characteristic temperatures, etc.). It has been found that the monitored parameters are temperature and time dependent, and that they can be shown to be functions of the so called ‘reduced time of artifcial ageing’. In addition, it has been found that, on the basis of known changes in viscoelastic properties as a function of time and ageing temperature, and the known kinetic parameters of the ageing process, it is possible to calculate (determine) the change in the properties at any ageing temperature provided that the mechanism of the ageing process does not change. Unfortunately, the use of kinetic parameters obtained by artifcial ageing at high temperatures (above 60 °C) for the prediction of the propellant lifetime will not give reliable results, because the mechanisms of ageing at 85 °C and 25 °C are not the same.
    Źródło:
    Central European Journal of Energetic Materials; 2013, 10, 2; 225-244
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
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