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Tytuł:
Analysis of the effect of assembly joints technology on the strength of adhesive joints of poly(methyl methacrylate) (pmma) used in advertising elements
Analiza wpływu technologii wykonania połączeń montażowych na wytrzymałość połączeń adhezyjnych polimetakrylanu metylu, stosowanych w elementach reklamowych
Autorzy:
Rudawska, Anna
Penkała, Piotr
Miszczuk, Bartosz
Stančeková, Dana
Powiązania:
https://bibliotekanauki.pl/articles/31232975.pdf
Data publikacji:
2023
Wydawca:
Politechnika Rzeszowska im. Ignacego Łukasiewicza. Oficyna Wydawnicza
Tematy:
adhesive joint
angular joint
poly(methyl methacrylate)
wettability
contact angle
strength
połączenie adhezyjne
połączenie kątowe
poli(metakrylan metylu)
zwilżalność
kąt zwilżania
wytrzymałość
Opis:
The aim of the article was to present issues related to the influence of the assembly joints technology (the type of adhesive material and the adhesive application) on the strength of the adhesive joints of poly(methyl methacrylate) (PMMA) used in the production of advertising elements. Angular adhesive joints, which are one of the types of joints made in the construction of advertising elements, were used in the study. The bonded material was poly(methyl methacrylate) (PMMA) of 8 mm thick. Two types of adhesives were used to make the adhesive joints: one-component solvent-based adhesives and methylene chloride as a solvent. Experimental tests determined the wettability of the surface of the adherends (with and without a protective coating) and the work of adhesion based on the measurement of the contact angle, as well as the strength of adhesive joints in accordance with the ISO 4578 standard. Based on the results of strength tests, it can be seen that the use of a solvent allows for obtaining equally strong joints as with the use of solvent-based adhesives. The purposefulness of using coatings protecting not only against dirt or mechanical damage in the form of scratches was also confirmed, but also the possibility of increasing (security) adhesive properties, defined in this case by wettability.
Celem artykułu było przedstawienie zagadnień związanych z wpływem technologii połączeń montażowych (rodzaju materiału klejącego i sposobu aplikacji kleju) na wytrzymałość połączeń klejowych z poli(metakrylanu metylu) (PMMA) stosowanych w produkcji elementów reklamowych. W badaniach wykorzystano połączenia klejowe kątowe, które są jednym z rodzajów połączeń wykonywanych w konstrukcji elementów reklamowych. Łączonym materiałem był poli(metakrylan metylu) (PMMA) o grubości 8 mm. Do wykonania połączeń klejowych zastosowano dwa rodzaje jednoskładnikowych klejów rozpuszczalnikowych oraz chlorek metylenu, jako rozpuszczalnik. W badaniach doświadczalnych określono zwilżalność powierzchni klejonych elementów (z powłoką ochronną i bez) oraz pracę adhezyjną na podstawie pomiaru kąta zwilżania, a także wytrzymałość połączeń klejowych zgodnie z normą ISO 4578. Na podstawie wyników badań wytrzymałościowych można stwierdzić, że zastosowanie rozpuszczalnika pozwala na uzyskanie połączeń równie wytrzymałych, jak przy zastosowaniu klejów rozpuszczalnikowych. Potwierdzono również celowość stosowania powłok zabezpieczających nie tylko przed zabrudzeniami czy uszkodzeniami mechanicznymi w postaci zarysowań, ale także w celu zwiększenia (zabezpieczenia) właściwości adhezyjnych, określanych w tym przypadku przez zwilżalność.
Źródło:
Technologia i Automatyzacja Montażu; 2023, 2; 3-10
2450-8217
Pojawia się w:
Technologia i Automatyzacja Montażu
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Modification of Concrete Surface with Higher Fatty Acids
Autorzy:
Barnat-Hunek, Danuta
Andrzejuk, Wojciech
Szafraniec, Małgorzata
Kachel, Magdalena
Hunek, Robert
Powiązania:
https://bibliotekanauki.pl/articles/2201909.pdf
Data publikacji:
2023
Wydawca:
Stowarzyszenie Inżynierów i Techników Mechaników Polskich
Tematy:
contact angle
higher fatty acid
hydrophobic agent
hydrophobization
water tightness
vapor permeability
Opis:
The research presented in the paper concerns the production of innovative hydrophobizing agents and demonstration their effectiveness on a concrete surface. The starting materials are based on natural oils, water‒soluble silanes and siloxanes, and/or tap water. Aqueous preparations are characterized by properties which reduce the impact of volatile organic compounds (VOCs) on the environment, as they consist only of biodegradable components. Studies have shown that the higher fatty acids from vegetable oils and derived from the glycerin phase can be used as a component of concrete hydrophobizing agents, meeting the standard requirements for such agents. Analysis of the use of vegetable oil as a base compound for the production of industrial agents provides at least 95% confidence in its biodegradability. The reference concrete after the frost resistance test showed a weight loss of 1.8%. In the case of hydrophobization, the weight loss was 33.3 to 72% less than the reference samples. In the case of concrete hydrophobized with the glycerin agents, the salt crystallization occurred inside the structure of the material without causing any damage, with the reference concrete showing a weight loss of 0.8%.
Źródło:
Advances in Science and Technology. Research Journal; 2023, 17, 2; 307--321
2299-8624
Pojawia się w:
Advances in Science and Technology. Research Journal
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Control of glass surface wettability via esterification with n-alkyl alcohols
Autorzy:
Kruszelnicki, Mateusz
Polowczyk, Izabela
Kowalczuk, Przemyslaw B.
Powiązania:
https://bibliotekanauki.pl/articles/2146948.pdf
Data publikacji:
2022
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
hydrophobicity
surface free energy
contact angle
zeta potential
roughness
Opis:
Surface wettability plays an essential role in many processes and materials applications. It depends mainly on the surface roughness and chemical composition, thus through a controlled modification of these parameters, the wettability can be restrained. Glass is an inorganic solid material, composed mainly of amorphous silica, which surface, due to the presence of reactive hydroxyl groups, can be quite easily chemically modified. This feature can be used to control the wettability of glass by reaction with organic compounds. In this study, the esterification of glass silanol groups with n-alkyl alcohols (Cn/H2n+1/OH, n=3, 4, 6, 8, 10) was employed to modify its wettability. The effect of such modification on the physicochemical properties of glass surface was comprehensively investigated and characterised by the water contact angle, surface free energy, zeta potential, atomic force microscopy (AFM) and X-ray photoelectron spectroscopy (XPS) measurements. We demonstrate that the wettability of the esterified glass surface is strongly dependent on both the chain length of used alcohol and modification time. The alcohol molecule binds to the glass surface through a Si-O-C bond, leading to the formation of a monolayer that does not significantly affect the surface morphology and zeta potential. Conducted studies provided a broader view of the influence of this technique for modifying surface wettability on its physicochemical properties.
Źródło:
Physicochemical Problems of Mineral Processing; 2022, 58, 2; art. no. 145147
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Electrokinetic and surface properties of some methacrylate-based copolymers
Autorzy:
Ersoy, Bahri
Çiftçi, Hakan
Evcin, Atilla
Merdivenci, Yılmaz
Powiązania:
https://bibliotekanauki.pl/articles/2146940.pdf
Data publikacji:
2022
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
methacrylate copolymer
zeta potential
contact angle
hydrophobicity
surface free energy
Opis:
In this study, some electrokinetic and surface properties of MBAOM-GMA copolymers synthesized from 2-[(methoxy-1,3-benzothiazole-2-yl) amino]-2oxoethyl methacrylate (MBAOM) and glycidyl methacrylate (GMA) monomers were investigated. Accordingly, (i) pH-dependent zeta (ζ) potential changes of the copolymers were investigated under a constant ionic strength (in 1.10-3mol/dm3 NaCl) and the corresponding isoelectric points (iep) were determined, (ii) zeta potential changes depending on the salt concentration in the presence of mono-, di- and tri-valent metal salts were examined, (iii) contact angles (θ) of the copolymers with water were measured and their wetting behavior was assessed, and (iv) surface free energies (SFE) of the copolymers were determined by Acid-Base approach using Van Oss-Chaudhury-Good method. The compositions of the copolymers were 77% MBAOM - 23% GMA, 45% MBAOM - 55% GMA, and 19% MBAOM - 81% GMA. FeCl3, CaCl2, and KCl salts were used for the salt solutions for the zeta potential measurements. As a result, (i) it was determined that the chemical structure of methacrylate copolymers showed a decisive effect on both electrokinetic and surface properties, (ii) the hydrophobic character of copolymer increased with the increase of the GMA ratio, and correspondingly, the SFE decreased, and (iii) the iep of the copolymers varied between pH 3.1-3.7 depending on composition.
Źródło:
Physicochemical Problems of Mineral Processing; 2022, 58, 5; art. no. 152162
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Multiscale water drop contact angles at selected silica surfaces
Autorzy:
Zhang, Chen
Wang, Xuming
Li, Lixia
Jin, Jiaqi
Polson, Randy
Miller, Jan D.
Powiązania:
https://bibliotekanauki.pl/articles/2146924.pdf
Data publikacji:
2022
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
contact angle
atomic force microscopy
hollow tip
submicron-drop
wettability
MD simulation
Opis:
In this study, multiscale advancing contact angles for glycerol/water drops at silica surfaces are reported for millidrops, submicron-drops, and nanodrops. Selected silica surfaces were muscovite, silicon, and talc. The contact angles for millidrops (1–2 mm) were determined by the traditional sessile drop technique. For submicron-drops (0.1–1.0 μm), a hollow tip Atomic Force Microscope (AFM) procedure was used. The contact angles for nanodrops (~7 nm) were examined from Molecular Dynamics (MD) simulation. The results were compared to evaluate the effect of drop size on the contact angle. In the case of the hydrophobic talc surface, the 75° advancing contact angle did not vary significantly with drop size. For the hydrophilic muscovite surface, the water drop wet the surface and an advancing contact angle of about 10° was found for the millidrops and submicron-drops. However, for the MD simulated nanodrops, attachment and spreading of the ~7 nm drop created a 2D film of molecular dimensions, the contact angle of which was difficult to define and varied from 0° to 17°. Perhaps of equal interest from the MD simulation results was that the spreading of the glycerol/water nanodrop at the muscovite surface resulted in crystallographic directional transport of water molecules to the extremities of the 2D film. Such separation and segregation left the center of the film with an increased concentration of glycerol. Based on these results, the line tension, which has been found in other investigations to account for contact angle decrease with a decrease in drop size, does not seem to be a significant factor in this study.
Źródło:
Physicochemical Problems of Mineral Processing; 2022, 58, 5; art. no. 152154
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Relative wettability measurement of porous diffuser and its impact on the generated bubble size
Autorzy:
Al-Yaqoobi, Atheer M.G.
Zimmerman, William B.
Powiązania:
https://bibliotekanauki.pl/articles/2173415.pdf
Data publikacji:
2022
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
kąt kontaktu
dyfuzor porowaty
metoda Washburn
zwilżalność
bubble size
contact angle
porous diffuser
Washburn method
wettability
Opis:
Controlling the bubble size is a major concern in enhancing transport performance in gas-liquid systems. The role of wettability of diffuser surface on bubble size is the subject of the current work. The study inspects the contact angle of a set of liquids on HP ceramic diffusers using the Washburn method. The results demonstrate that organic liquids like toluene, methanol–water (1:1 v/v), ethanol– water (1:1 v/v) and decane have small contact angles of 12.9, 37.5, 24.4 and 22.5 respectively. Water has a lower wettability than the organic compounds where the contact angle was about 67.4. The effect of wettability of the bubble size is investigated by measuring the size of air bubble produced using the same diffuser material. The results of bubble size measurement demonstrates that with liquids of small contact angle, i.e. good wetting properties, small bubble sizes are produced in comparison with liquids with a higher contact angle. The study demonstrates the viability of Washburn method in characterization of wettability of porous diffuser, which was verified by measuring the bubble size produced. A high reduction in bubble size can be obtained by a carefully chosen diffuser material that provides better wettability.
Źródło:
Chemical and Process Engineering; 2022, 43, 1; 45--55
0208-6425
2300-1925
Pojawia się w:
Chemical and Process Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Characteristic of polypropylene nanocomposite material reinforcement with hydroxyapatite for bone replacement
Autorzy:
Obaid, M. N.
Sabr, O. H.
Hussein, A. A.
Powiązania:
https://bibliotekanauki.pl/articles/1818801.pdf
Data publikacji:
2021
Wydawca:
Stowarzyszenie Komputerowej Nauki o Materiałach i Inżynierii Powierzchni w Gliwicach
Tematy:
polypropylene
hydroxyapatite
osteoplastic cells
surface roughness
contact angle
wettability
bone replacement
clots creation
coagulates creation
polipropylen
hydroksyapatyt
chropowatość powierzchni
kąt zwilżania
zwilżalność
substytut kości
tworzenie
Opis:
Purpose: Human bone suffered some degeneration due to age and accidents; therefore, there are many interests in the prepared synthetic bone with properties nearer to natural bone. The present study prepared a nanocomposite of polypropylene reinforced with different weight fraction of Nano hydroxyapatite (HAp) to be used as a bone replacement with good biological properties that enhanced the growth of osteoplastic cells and enhance the prevention of clots and coagulates creation. Design/methodology/approach: Nanocomposite from polypropylene reinforced with different weight fraction of Hydroxyapatite (HAp) (1,2 and 3) % prepared by first dispersion Nano hydroxyapatite insolvent and then mixing with a pellet of polypropylene by the twin-screw extrusion process, the current research study the surface properties ( atomic force microscopy (AFM), contact angle test) Moreover, it studied the characteristics of prepared nanocomposite materials (Differential Scanning Calorimetry (DSC), Field Emission-Scanning Electron Microscopy (FE-SEM) and Fourier Transform Infrared (FTIR)). Findings: The AFM results show the surface roughness decreased with increasing content of HAp, which diminished the chance of creation clots and coagulates on it. The contact angle results referred to polypropylene behaviour transformed from hydrophobic to hydrophilic with addition HAp that permission to grow the osteoplastic cell on it, so the healing process is accelerated. Moreover, the FE-SEM images revealed uniform distribution and good bonding between polypropylene and Hydroxyapatite. The thermal properties were measured by the DSC test showed the melting temperature, and the enthalpy of melting (indicated to increase the crystalline structure per cent) are increased with increasing the percentage of Hydroxyapatite. Research limitations/implications: This research studied the characteristics of nanocomposite materials prepared by three steps (dispersion by ultrasonic device, manually mixed and melting and mixing by twin extruder) which can be used as a bone replacement. However, the main limitation was the uniform distribution of nano-hydroxyapatite within the matrix. In a further study, the cytotoxic test can be tested to study the effect of prepared nanocomposite on living cells’ growth. Practical implications: The interest object is how to connect among different properties to prepared bone replacement with good properties and biocompatibility that made able to stimulate the growth and healing process. Originality/value: The nano-hydroxyapatite is a biomaterial that has a composition similar to the natural mineral phase of the bone and does not have any negative effect, which enhanced the growth of osteoplastic cells and decreased the clots and coagulates creation; therefore, nano-hydroxyapatite is used to decrease the surface roughness which decreased the chance of coagulation creation and to enhance the hydrophilic properties.
Źródło:
Journal of Achievements in Materials and Manufacturing Engineering; 2021, 104, 1; 21--30
1734-8412
Pojawia się w:
Journal of Achievements in Materials and Manufacturing Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of chitosan film surface structure on the contact angle
Autorzy:
Jagodzińska, Sylwia
Pałys, Beata
Wawro, Dariusz
Powiązania:
https://bibliotekanauki.pl/articles/2131497.pdf
Data publikacji:
2021
Wydawca:
Sieć Badawcza Łukasiewicz - Polskie Towarzystwo Chitynowe
Tematy:
cellulose
chitosan
contact angle
films
microstructure
Opis:
The aim of this study was to evaluate the influence of the surface microstructure of chitosan films on the contact angle. Films without plasticising additives made of chitosan or regenerated chitosan were selected for the tests. A sessile drop method based on the European Pharmacopoeia was used to determine the contact angle. Due to the method of film production, the contact angle measurements were made on both the top and bottom surfaces of the film. For chitosan or regenerated chitosan films, the method of preparation slightly affected the difference in wettability between the top and bottom of the films, as confirmed by scanning electron microscopy. On the other hand, the wettability of the top and bottom of cellulose films varied greatly depending on the side of the film. Both chitosan and cellulose films had a homogeneous structure. There were differences in the microstructure between the top and the bottom of the sample in the cellulose film, a factor that affected the contact angle and thus the wettability of the surface.
Źródło:
Progress on Chemistry and Application of Chitin and its Derivatives; 2021, 26; 89-100
1896-5644
Pojawia się w:
Progress on Chemistry and Application of Chitin and its Derivatives
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Wpływ działania plazmy niskotemperaturowej na zmiany zwilżalności wybranych polimerów
Effect of low-temperature plasma on changes in wettability of selected polymers
Autorzy:
Hołysz, Lucyna
Kamela (Rymuszka), Diana
Terpiłowski, Konrad
Chibowski, Emil
Powiązania:
https://bibliotekanauki.pl/articles/1853718.pdf
Data publikacji:
2021
Wydawca:
Polskie Towarzystwo Chemiczne
Tematy:
polimer
plazma niskotemperaturowa
zwilżalność
kąt zwilżania
swobodna energia powierzchniowa
adhezja
polymer
low-temperature plasma
wettability
contact angle
surface free energy
adhesion
Opis:
The effects of air, oxygen and argon plasma treatment on wetting and energetic properties of polymers: polymethylmethacrylate (PMMA), polyetheretherketone (PEEK), polyoxymethylene (POM), polyamide (PA6G), polycarbonate (PC) and polypropylene (PP) were studied. The changes in surface properties of PMMA, PEEK, POM, PA6G polymers after the air plasma treatment, and PP and PC polymers after the Ar or O2 plasma treatment were determined via the measurement of advancing and receding contact angles of three liquids having different polarity, i.e. water, formamide and diiodomethane. Having the determined contact angles the surface free energy and its components of the polymers were calculated using three different theoretical approaches, namely: acid-base Lifsthitz-van der Waals (LWAB), contact angle hysteresis (CAH) and Owens and Wendt (O-W). The effects of plasma treatment were further determined by calculations of the adhesion work and work of spreading of water on modified polymer and compared to values calculated for the unmodified surfaces. Then for the PEEK and POM modified with the air plasma, their surface wettability was determined after 14 days from the exposure to the plasma. It was found that plasma treatment caused better wettability what reflected in a decreased contact angles measured on the modified polymer surfaces. The greatest changes appeared for polar liquids, i.e. water and formamide. It pointed to an increased the surface hydrophilicity after the plasma treatment. The changes correlated also with the increased polar interactions due to appearance polar groups on the surface. For the studied polymer surfaces, generally the dispersive interactions practically did not change, regardless the treatment time and plasma type. The total surface free energy values calculated for the polymers from three different approaches to interfacial interactions are similar. However, the energy values are apparent because they depend s upon the kind of liquid used for the contact angles measurement. Irrespectively of the plasma type, for all polymers an increase of the adhesion work of water in reference to the unmodified surfaces was observed. The most appropriate time to improve the adhesion between the polymer surface and liquid was found to be 25 or 60 s. However, the effects of plasma treatment are not permanent. With the storage time the contact angles have increased. This can be due to the structure reorganization within a few nm thick the surface layer.
Źródło:
Wiadomości Chemiczne; 2021, 75, 9-10; 1270-1295
0043-5104
2300-0295
Pojawia się w:
Wiadomości Chemiczne
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
An investigation of continuous interaction process between air bubble and various roughness coal surfaces using microbalance
Autorzy:
Guo, Zhimin
Yang, Jianguo
Wang, Yuling
Powiązania:
https://bibliotekanauki.pl/articles/1450050.pdf
Data publikacji:
2020
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
surface roughness
air bubble
contact angle
continuous interaction
Opis:
Surface roughness of particles plays an important role in bubble-particle interaction process. However, the continuous attachment and detachment process have rarely been characterized between the surface of different roughness and air bubble. In this study, the continuous attachment and detachment processes between the surface of different roughness and air bubble were investigated by a highly sensitive microbalance. The bubble–surface interaction process was monitored by a high-speed camera to analyze the geometry parameters, including distance, adhesion diameter, and contact angle. It was found that the bubble-particle attachment time increased with the increase of surface roughness. The magnitude of the repulsive force in the bubble-surface approaching process increased with the increase of surface roughness, while the attractive force in the bubble-particle retracting process decreased monotonically with the surface roughness. The force measured by microbalance was finally compared with the calculated one. The calculated force at the biggest force point also increased with the decrease of surface roughness. These results indicate that coal particles with lower surface roughness, which have less water-filled pores and pillars, is more conducive to flotation due to the lower repulsive force in the bubble-particle attachment process and higher adhesive force in the bubble-particle detachment process, and vice versa.
Źródło:
Physicochemical Problems of Mineral Processing; 2020, 56, 1; 11-23
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Comparison of components and parameters of some sulfide minerals surface tension with regards to stability of mineral-air bubble system
Autorzy:
Jańczuk, Bronisław
Zdziennicka, Anna
Powiązania:
https://bibliotekanauki.pl/articles/1450639.pdf
Data publikacji:
2020
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
contact angle
wettability
surface tension
detachment force
sulfide minerals
Opis:
The measurements of the advancing contact angle of water, glycerol, formamide, ethylene glycol, diiodomethane, α-bromonaphthalene, 1,2,3-tribromopropane on unoxidized and oxidized galena, pyrite, chalcopyrite, djurleite, bornite and covellite at the temperature equal 293 K were made. Additionally, the measurements of the force air bubble detachment from these sulfide minerals including also chalcocite in water were performed. Using the values of the obtained contact angle of water, glycerol, formamide, ethylene glycol, diiodomethane, α-bromonaphthalene, 1,2,3-tribromopropane the components and parameters of the unoxidized and oxidized sulfide minerals surface tension were calculated. For this calculation the van Oss et al. method was applied after analysis of the components and parameters of the surface tension of liquids used for contact angle measurements. Taking into account the contact angle of water on the sulfide minerals, the detachment force of air bubble from these minerals in water was determined using our equation and comparing to that of measured one. As follows from the measurements and calculations the wetting properties of sulfide minerals and the stability of mineral-air bubble depends to a larger extent on the degree of sulfide minerals oxidation than on the type of mineral.
Źródło:
Physicochemical Problems of Mineral Processing; 2020, 56, 6; 22-31
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Enhancement of tribological properties and characteristic of polymer matrix composite (UHMWPE reinforced with short fibres of polyester) for Total Disc Replacement (TDR)
Autorzy:
Obaid, M. N.
Radhi, S. H.
Powiązania:
https://bibliotekanauki.pl/articles/1818822.pdf
Data publikacji:
2020
Wydawca:
Stowarzyszenie Komputerowej Nauki o Materiałach i Inżynierii Powierzchni w Gliwicach
Tematy:
total disc replacement
UHMWPE
polyester fibres
tribological
contact angle
crystalline degree
roughness
melting temperature
volume loss
całkowita wymiana dysku
całkowita endoprotezoplastyka krążka międzykręgowego
włókna poliestrowe
tribologia
kąt zwilżania
stopień krystaliczności
chropowatość
temperatura topnienia
utrata objętości
Opis:
Purpose: The number of people suffering from Degenerative Disc Disease (DDD) is increasing. The disease causes heavy pain and restrict a number of day-to-day life activities. In extreme cases, the degraded disc is removed under total disc replacement which is usually made up of Ultra-High Molecular Weight Polyethylene (UHMWPE). The material has astounding biocompatible characteristics mechanical properties and wear resistance. However, these characteristics are insufficient in arthroplasty application. Therefore, research investigations are ongoing to improve tribological properties through reinforcement that may result in a composite material of UHMWPE. Thus the current study is aimed at reinforcing UHMWPE with short fibres of polyesters to enhance the tribological properties and surface characteristic so as to improve wear resistance and nourish the fibroblast cells on synthetic disc. Design/methodology/approach: The researcher prepared UHMWPE composite material, reinforced with different weight fractions of short polyester fibres (2, 4, 6, 8 and 10% following hot press method. Further pin-on-disc device was used to study the tribological properties (coefficient of friction and volume of wear). The study tested surface roughness and surface characteristics by atomic force microscopy (AFM) device, hardness by shore D device, contact angle to study the effect of polyester short fibres on wettability of UHMWPE surface and tested the thermal properties and crystalline degree using Differential Scanning Calorimetry measurement (DSC) device. Findings: The results infer that the wear resistance got improved when using 2% w.t polyester though it got decreased initially. However, the value was still more than neat UHMWPE. There was a decrease observed in coefficient of friction, but after 4 w.t% polyester, the coefficient of friction got increased due to increasing percentage of fibres which make it harder and stiff compared to UHMWPE. There was a decline observed in surface roughness due to alignment of the fibres with smooth surface. The contact angle got increased in a moderate range while the roughness enhanced the growth of fibroblast cell. The hardness of composite material got increased, because the fibres turned stiffer and harder than the matrix. DSC results infer the improvements in thermal stability due to high thermal properties of polyester fibres compared to UHMWPE. The degree of crystallinity got increased which in turn enhanced wear resistance, especially at 6 w.t % polyester fibres. There was a mild increase observed in density since the density of polyester is higher than polymer. Research limitations/implications: The major challenge was the dispersion of fibres. Uniform distribution of fibres within the matrix (UHMWPE) was achieved through two steps of mixing processes such as mechanical mixture and twin extruder. In future studies, fatigue tests must be conducted to study the behaviour of prepared composite materials under fatigue cycle. Practical implications: A significant objective is how to connect among different properties to obtain good improvement in tribological and surface properties so as to enhance wear resistance and growth of fibrolase cells. Originality/value: In this study, polymeric short fibres were used as reinforcement with polymeric matrix to enhance the wettability of fibres with matrix. In this way, the bonding among them got increased which supports the tribological, surface, and crystalline behaviour.
Źródło:
Journal of Achievements in Materials and Manufacturing Engineering; 2020, 102, 2; 55--65
1734-8412
Pojawia się w:
Journal of Achievements in Materials and Manufacturing Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Evaluation of the contact angle and wettability of hydrophobised lightweight concrete with sawdust
Ocena kąta zwilżania i zwilżalności hydrofobizowanego betonu lekkiego z trocinami
Autorzy:
Szafraniec, Małgorzata
Barnat-Hunek, Danuta
Powiązania:
https://bibliotekanauki.pl/articles/391199.pdf
Data publikacji:
2020
Wydawca:
Politechnika Lubelska. Wydawnictwo Politechniki Lubelskiej
Tematy:
sawdust
lightweight aggregate concrete
organosilicon compounds
hydrophobisation
contact angle
trociny
beton z kruszywa lekkiego
związki krzemoorganiczne
hydrofobizacja
kąt zwilżania
Opis:
The aim of the research presented in the paper was to evaluate the feasibility of using hydrophobic preparations based on organosilicon compounds for protection treatment on the lightweight concrete modified with sawdust. The experimental part of the work concerns the physical and mechanical properties of lightweight concrete and the influence of two hydrophobic agents on the contact angle of the material. Lightweight concrete contact angle (θw) was determined as a time function using one measuring liquid. Water repellent coatings in lightweight concrete structure with the coarse aggregate sawdust (CASD) using electron microscopy were presented. The effectiveness of hydrophobisation of porous lightweight concretes was determined on the basis of the research. For the hydrophobic surface, the contact angle decreased and it depended on the used agents. The lowest contact angle of 40.2° (t=0) was obtained for reference concrete before hydrophobisation and 112.2° after hydrophobisation with a methyl-silicone resin based on organic solvent. The results of scientific research confirm the possibility to produce lightweight concretes modified with CASD with adequate surface protection against external moisture.
Celem badań przedstawionych w pracy była ocena możliwości zastosowania preparatów hydrofobowych na bazie związków krzemoorganicznych do zabezpieczania betonu lekkiego modyfikowanego trocinami. Część doświadczalna pracy dotyczy właściwości fizycznych i mechanicznych betonu lekkiego oraz wpływu dwóch preparatów hydrofobowych na kąt zwilżania materiału. Określono kąt zwilżania betonu lekkiego (θw) w funkcji czasu za pomocą jednej cieczy pomiarowej. Za pomocą mikroskopu elektronowego pokazano powłoki hydrofobowe w strukturze betonu lekkiego, w którym zastosowano trociny jako kruszywo grube (CASD). Na podstawie badań określono skuteczność hydrofobizacji porowatych betonów lekkich. Dla powierzchni hydrofobowej zmniejszył się kąt zwilżania i był on zależny od zastosowanych środków. Najniższy kąt zwilżania 40,2° (t=0) uzyskano dla betonu wzorcowego przed hydrofobizacją i 112,2° po hydrofobizacji żywicą metylo-silikonową na bazie rozpuszczalnika organicznego. Wyniki badań naukowych potwierdzają możliwość otrzymywania betonów lekkich modyfikowanych za pomocą CASD z odpowiednią ochroną powierzchni przed działaniem wilgoci z zewnątrz.
Źródło:
Budownictwo i Architektura; 2020, 19, 2; 19-32
1899-0665
Pojawia się w:
Budownictwo i Architektura
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Failure characteristics and strength model of composite rock samples in contact zone under compression
Autorzy:
Wang, Qihu
Wang, Jie
Ye, Yicheng
Jiang, Wei
Yao, Nan
Powiązania:
https://bibliotekanauki.pl/articles/219633.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
materiał kompozytowy
kąt zwilżania
awaria
contact zone
composite rock sample
contact angle
failure characteristics
constraint stress
strength model
Opis:
Significant differences in the physical and mechanical properties exist between the rock masses on two sides of an ore-rock contact zone, which the production tunnels of an underground mine must pass through. Compared with a single rock mass, the mechanical behavior of the contact zone composite rock comprising two types of rock is more complex. In order to predict the overall strength of the composite rock with different contact angles, iron ore-marble composite rock sample uniaxial compression tests were conducted. The results showed that composite rock samples with different contact angles failed in two different modes under compression. The strengths of the composite rock samples were lower than those of both the pure iron ore samples and pure marble samples, and were also related to the contact angle. According to the stress-strain relationship of the contact surface in the composite rock sample, there were constraint stresses on the contact surface between the two types of rock medium in the composite rock samples. This stress state could reveal the effect of the constraint stress in the composite rock samples with different contact angles on their strengths. Based on the Mohr-Coulomb criterion, a strength model of the composite rock considering the constraint stress on the contact surface was constructed, which could provide a theoretical basis for stability researches and designs of contact zone tunnels.
Źródło:
Archives of Mining Sciences; 2020, 65, 2; 347-361
0860-7001
Pojawia się w:
Archives of Mining Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Finite element analysis of mini-plate stabilization of human mandible angle fracture – a comparative study
Autorzy:
Wądołowski, Piotr
Krzesiński, Grzegorz
Gutowski, Piotr
Powiązania:
https://bibliotekanauki.pl/articles/27324127.pdf
Data publikacji:
2020
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
finite element analysis
maxillofacial surgery
mandibular angle fracture
miniplate osteosynthesis
contact mechanics
analiza elementów skończonych
chirurgia szczękowo-twarzowa
złamanie kąta żuchwy
osteosynteza minipłytkowa
mechanika kontaktowa
Opis:
Purpose: The purpose of this study was to analyze three patterns of mandible angle fracture treatment by means of the finite element analysis. Methods: Investigation has been based on the mandible geometry reconstructed with use of hospitalized patient CT data. The KLS Martin mini-plates with corresponding screws were used to establish proper fracture stabilization. Models were run assuming isotropic and elasto-plastic material properties of connecting devices and cortical bone. The main masticatory muscles and artificial temporomandibular joint have been incorporated to assure mandible physiological movement. The gage loading has been applied in three different locations to cover wider range of possible mastication loading cases during daily routine. A different contact conditions have been applied to the fracture plane to simulate both load bearing and sharing behaviors. Prepared FEM models reflect the most frequently used surgery’s approaches to mandible angle fracture treatment. A specific nomenclature has been introduced to describe particular model. The tension plate, with one connecting mini-plate, two-point fixation and combined fixation, both using two mini-plates respectively. Results: Performed analysis allowed for a detailed estimation of the mini-plate connection response under the applied gauge loading. The equivalent stress within the mini-plates and surrounding cortical bone have been compared between all models. Regarding the fracture plane, the contact status and pressure have been considered. Conclusions: The combined fixation model, acting as a biplanar fastener system, presents the highest flexibility and connection efficiency.
Źródło:
Acta of Bioengineering and Biomechanics; 2020, 22, 3; 105--116
1509-409X
2450-6303
Pojawia się w:
Acta of Bioengineering and Biomechanics
Dostawca treści:
Biblioteka Nauki
Artykuł

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