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    Tytuł:
    Investigating the selectivity of calcium hypochlorite for flotation separation of chalcopyrite and pyrite pre-adsorbed collector
    Autorzy:
    Yang, Wenhui
    Qiu, Xianhui
    Yan, Huashan
    Wu, Hao
    Yang, Liu
    Lai, Ruisen
    Qiu, Tingsheng
    Powiązania:
    https://bibliotekanauki.pl/articles/2146919.pdf
    Data publikacji:
    2022
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    pyrite
    chalcopyrite
    calcium hypochlorite
    flotation separation
    Opis:
    Bulk flotation is usually used in the flotation of Cu-Fe sulfide ore, and the subsequent concentrate is difficult to be separated because the minerals have adsorbed the collector. In this paper, flotation tests showed that calcium hypochlorite (Ca(ClO)2) had a stronger depression effect on pyrite pre-adsorbed sodium butyl xanthate (SBX), while having a negligible depressive effect on chalcopyrite. A copper concentrate with Cu grade of 33.32% and Cu recovery of 94.47% could be obtained from flotation tests of mixed minerals. The depression performance and mechanism of Ca(ClO)2 were studied by contact angle measurements, Fourier transform infrared spectroscopy and X-ray photoelectron spectroscopy analyses, the results suggested that Ca(ClO)2 can decomposes SBX on the pyrite surface and oxidizes the mineral surface to form hydrophilic substances, which enhances the hydrophilicity of the pyrite surface. In contrast, Ca(ClO)2 has little effect on chalcopyrite pre-adsorbed SBX, the possible depression model is discussed.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2022, 58, 4; art. no. 150703
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The depression mechanism on pyrite in a low-alkaline system with combined depressants : Experiment, HSC, DFT and ToF–SIMS studies
    Autorzy:
    Li, Suqi
    Yuan, Jiaqiao
    Ding, Zhan
    Li, Jie
    Yu, Anmei
    Wen, Shuming
    Bai, Shaojun
    Powiązania:
    https://bibliotekanauki.pl/articles/24085821.pdf
    Data publikacji:
    2023
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    pyrite
    calcium hypochlorite
    lime
    depression
    low alkaline system
    Opis:
    Depression of pyrite in a low-alkaline system has sparked soaring interests for the multi-metal sulfide minerals flotation recently. This study investigates effects of combined depressants (Ca(ClO)2 and CaO) on pyrite flotation with butyl xanthate (KBX). Micro-flotation experiments indicate that the addition of 200 mg/L combined depressants (a mass ratios of CaO to Ca(ClO) 2 of 2:3) and 1.0×10−3 mol/L KBX at pH 9.5 can effectively depresses the flotation of pyrite, and a minimum pyrite recovery rate of 12.5% is obtained. Basic thermodynamic evaluation results confirm the participation of Ca(ClO) 2 significantly decrease the negative Gibbs free energies of pyrite oxidation reaction. Besides, the calcium species (Ca(OH) 2, Ca2+ and Ca(Cl) 2) will spontaneously transform into CaCO3,and it is the ultimate dominant calcium species in the CO32- system. Density functional theory (DFT) results indicate that CaCO3 can chemically adsorb onto the pyrite surface with an adsorption energy of –671.13 kJ/mol. The O1 and Ca atoms mainly contribute to the bonding process and are responsible for the stable adsorption of CaCO3. ToF-SIMS results provide strong evidence that the combined depressants increase the amount of hydrophilic species and decrease dixanthogen adsorption onto the pyrite surface. The thickness of the whole formed hydrophilic species is approximately 50 nm. Semiquantitative amounts of hydrophilic species follow the order of hydroxy calcium>iron carbonyl>calcium carbonate. Overall, hydrophilic species repulse adsorption of dixanthogen and significantly reduce the flotation performance of pyrite.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2023, 59, 3; art. no. 168454
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-2 z 2

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