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Tytuł:
EVA/zinc oxide nanocomposites for active food packaging : selected physical, and microbial properties
Nanokompozyty EVA/tlenek cynku do aktywnych opakowań do żywności : wybrane właściwości fizyczne i mikrobiologiczne
Autorzy:
Majeed, Haza Satar
Al-Juboory, Farah Khalaf Hammoud
Hamid, Raghad Ali
Zawawi, Ruzniza Mohd
Powiązania:
https://bibliotekanauki.pl/articles/24202791.pdf
Data publikacji:
2023
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Chemii Przemysłowej
Tematy:
ZnO nanoparticles
ethylene vinyl acetate copolymer
barrier properties
nanocząstki ZnO
kopolimer etylen-octan winylu
właściwości barierowe
Opis:
The melt-mixing method was used to obtain nanocomposites of poly(ethylene-co-vinyl acetate) (EVA) with 1, 3 or 5 wt% of hydrophilic zinc oxide (ZnO) nanoparticles. The contact angle, barrier and antimicrobial properties of the obtained composites were investigated. The nanocomposites were characterized by better hydrophilic and barrier properties, as evidenced by, respectively, a smaller contact angle and lower water vapor permeability and water absorption compared to EVA, which can be explained by the formation of hydrogen bonds between EVA and ZnO. In addition, the composites were characterized by greater bactericidal activity against E. coli and S. aureus. The optimal physical and microbial properties were obtained with 3 wt% ZnO content.
Metodą mieszania w stanie stopionym otrzymano nanokompozyty kopolimeru etylen-octan winylu (EVA) z dodatkiem 1, 3 lub 5% mas. hydrofilowych nanocząstek tlenku cynku (ZnO). Zbadano kąt zwilżania, właściwości barierowe i przeciwdrobnoustrojowe otrzymanych kompozytów. Nanokompozyty charakteryzowały się lepszymi właściwości hydrofilowymi i barierowymi, o czym świadczy, odpowiednio, mniejszy kąt zwilżania oraz mniejsza przepuszczalność pary wodnej i absorp¬cja wody w porównaniu z EVA, co można wyjaśnić tworzeniem się wiązań wodorowych pomiędzy EVA i ZnO. Ponadto kompozyty miały większą aktywność bakteriobójczą wobec E. coli i S. aureus. Optymalny zespół właściwości uzyskano przy 3% mas. zawartości ZnO.
Źródło:
Polimery; 2023, 68, 3; 135--141
0032-2725
Pojawia się w:
Polimery
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis and Characterization of ZnO/MnFe2O4 Nanocomposites for Degrading Cationic Dyes
Autorzy:
Yuniar
Agustina, Tuty Emilia
Faizal, Muhammad
Hariani, Poedji Loekitowati
Powiązania:
https://bibliotekanauki.pl/articles/24201760.pdf
Data publikacji:
2023
Wydawca:
Polskie Towarzystwo Inżynierii Ekologicznej
Tematy:
nanocomposite
ZnO/Fe2O4
cationic dyestuff
photocatalysis
Opis:
By breaking down harmful dye waste into harmless components under the right irradiation sources, photocatalysis is an unorthodox but promising technique that can reduce industrial wastewater pollution, particularly in the textile industry. Synthetic textile dyes called cationic dyes must be handled carefully because they are poisonous and challenging to breakdown. Photocatalytic oxidation is a useful technique for eliminating hazardous organic pigments. This investigation aims to synthesize and characterize ZnO/MnFe2O4 nanocomposites as well as investigate the effects of varying ZnO:MnFe2O4 ratios, pH levels, doses, and irradiation times on band gap reduction and photocatalytic applications tested with cationic dyes, specifically methylene blue, under the illumination of sunlight. the co-precipitation approach for the manufacture of nanocomposites with different mole ratios of ZnO:MnFe2O4 (1:0.1; 2:0.1; 3:0.1). The component comprising the nanocomposite is ZnO/MnFe2O4, according to the results of the characterisation using XRD, SEM-EDX, FTIR, and BET. UV-DRS measurements of the band gap revealed that as ZnO was reduced, the band gap of the nanocomposite likewise decreased, from 3.35 eV to 2.78 eV. The greatest degradation of 93.2% was achieved for the degradation of 50 mg/L methylene blue (MB) dye with a catalyst dosage of 20 mg at a ratio of 1:0.2 for 50 minutes of irradiation. Since the point of zero charges (pzc) was reached at a pH of 7.8, a photodegradation adsorption-friendly solution pH of 8 was created.
Źródło:
Journal of Ecological Engineering; 2023, 24, 4; 252--263
2299-8993
Pojawia się w:
Journal of Ecological Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The effect of Co and Cu co-doping ZnO thin films on structural and optical properties
Autorzy:
Saoud, Tayeb
Benramache, Said
Diha, Abdallah
Powiązania:
https://bibliotekanauki.pl/articles/31342694.pdf
Data publikacji:
2023
Wydawca:
Towarzystwo Chemii i Inżynierii Ekologicznej
Tematy:
ZnO
thin films
Co
Cu
co-doping
TCO
spray pneumatic method
cienkie warstwy
współdomieszkowanie
Opis:
Using a spray pneumatic technique, cobalt (Co) and copper (Cu) co-doped zinc oxide thin films were effectively deposited on a glass substrate. The goal of this work was to create a semiconductor with good optical and electrical properties by co-doping ZnO thin films with Cu and Co. The ZnO thin films obtained from the Co and Cu co-doping exhibit patterns of x-ray diffraction spectra that suggest they are hexagonal ZnO (wurtzite, JCPDS 36-1451). The thin film elaborated with 2 % Co and 7 % Cu has the lowest value of crystallite size (D = 14.67 nm). The transmission spectra demonstrate that all films have good optical transparency in the visible spectrum, with 7 % Cu achieving the highest transmission. Increasing Cu contents raised the band gap energy. The value at the minimum was 3.31 eV. The optical band gap’s broadening is a significant characteristic of advanced materials and may be useful in applications involving metal oxide nanostructures for visible light gas sensing.
Źródło:
Chemistry-Didactics-Ecology-Metrology; 2023, 28, 1-2; 171-178
2084-4506
Pojawia się w:
Chemistry-Didactics-Ecology-Metrology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of Synthesis Conditions on the Chemical Structure and Composition of ZnO Nanoparticles Composite Systems / Polymer Fibers
Autorzy:
Calin, Gabriela
Sachelarie, Liliana
Olaru, Niculae
Powiązania:
https://bibliotekanauki.pl/articles/2106566.pdf
Data publikacji:
2022
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
polymer
nanofibres
composite ZnO/polimer
nanocomposites
Opis:
Nanostructured systems based on ZnO nanoparticles composite systems/polymer fibers have attracted a lot of attention in the last years because of their applications in multiple areas. Nanofibres based on polymers are used in many domains such as nanocatalysis, controlled release of medicines, environmental protection and so on. This work show the synthesis of cellulose acetate butyrate (CAB) nanofiber useful as substrates for growing ZnO nanocrystals and that ZnO is an unorganic metal oxide nanoparticle used to improve the piezoelectric properties of the polymer. The piezoelectric propertiesof ZnO-doped polymeric was investigated with atomic force microscopy and measurements were performed, in contact technique, in piezoelectric response mode (PFM).In order to analyze the structural and textural features, the obtained materials were characterized using advanced physical-chemical techniques such as X-ray diffraction (XRD), Atomic Force Microscopy (AFM), Scanning Electron Microscopy (SEM). The XRD patterns show the characteristic reflections of ZnO with a hexagonal type wurtzit structure and the broad peaks of the polymer. The SEM images reveal the presence of ZnO nanoparticles on top of the polymer nanofibres.In most ZnO-based nanocomposites their morphology is uncontrolled (agglomerated granules), but in ase of using cellulose acetobutyrate this becomes controlled by observing through flower-like structures SEM and AFM) The study of the functional properties of ZnO/polymer fiber composite systems showed that they have piezoelectric properties which give them the characteristics of smart material with possible sensor and actuator applications.Recent literature reports that the synthesis and characterization of ZnO-polymer nanocomposites are more flexible materials for various applications.
Źródło:
Archives of Metallurgy and Materials; 2022, 67, 2; 601--606
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structural, Electrical, and Optical Properties of ZnO Films Grown by Atomic Layer Deposition at Low Temperature
Autorzy:
Park, Ji-Young
Weon, Ye Bin
Jung, Myeong Jun
Choi, Byung Joon
Powiązania:
https://bibliotekanauki.pl/articles/2174578.pdf
Data publikacji:
2022
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
zinc oxide
ZnO
atomic layer deposition
low temperature growth
optoelectronic properties
Opis:
Zinc oxide (ZnO) is a prominent n-type semiconductor material used in optoelectronic devices owing to the wide bandgap and transparency. The low-temperature growth of ZnO thin films expands diverse applications, such as growth on glass and organic materials, and it is also cost effective. However, the optical and electrical properties of ZnO films grown at low temperatures may be inferior owing to their low crystallinity and impurities. In this study, ZnO thin films were prepared by atomic layer deposition on SiO2 and glass substrates in the temperature range of 46-141℃. All films had a hexagonal würtzite structure. The carrier concentration and electrical conductivity were also investigated. The low-temperature grown films showed similar carrier concentration (a few 1019 cm-3 at 141°C), but possessed lower electrical conductivity compared to high-temperature (>200°C) grown films. The optical transmittance of 20 nm thin ZnO film reached approximately 90% under visible light irradiation. Additionally, bandgap energies in the range of 3.23-3.28 eV were determined from the Tauc plot. Overall, the optical properties were comparable to those of ZnO films grown at high temperature.
Źródło:
Archives of Metallurgy and Materials; 2022, 67, 4; 1503--1506
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structured Analysis of Nanostructured Zinc Oxide (ZnO) Thin Films Deposited by Sol-Gel
Autorzy:
Hussin, Rosniza
Hanafi, F.
Rashid, R. A.
Harun, Z.
Kamdi, Z.
Ibrahim, S. A.
Ainuddin, A. R.
Rahman, W.
Leman, A. M.
Powiązania:
https://bibliotekanauki.pl/articles/2134100.pdf
Data publikacji:
2022
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
sol-gel
zinc oxide
ZnO
thin films
nanostructured
Opis:
In this work, zinc oxide (ZnO) thin films are deposited on glass substrate using the sol-gel spin coating technique. The effect of annealing temperature on structural properties was investigated. The ZnO sol-gel was produced from zinc acetate dehydrate as the starting material with iso-propanol alcohol as the stabilizer. The ratio was controlled, distilled water and diethanolamine as the solvent mixing on a magnetic stirrer for an hour under constant heat of 60°C. The ZnO thin film was deposited using the spin coating technique with the speed of 3000 rpm for 30 minutes before the sample undergoes pre-heat in the oven at the temperature of 100°C for 10 minutes. The sample was annealing in the furnace for an hour at 200°C, 350°C, and 500°C. The X-ray diffraction (XRD) analysis confirms that hexagonal wurtzite structure with zincite and zinc acetate hydroxide hydrate composition. The thin films surface roughness was analyzed using an atomic force microscope (AFM) and scanning electron microscope (SEM) for surface morphology observation.
Źródło:
Archives of Metallurgy and Materials; 2022, 67, 3; 1055--1060
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Zinc oxide nanoparticles as photo-catalytic and anti-bacterial pigment for alkyd resin based coating
Autorzy:
Kavitha Sri, A.
Sivaraj, M.
Rajkumar, S.
Ruby Shelin, A.
Sajitha, L.P.
Jeyasubramanian, K.
Jeen Robert, R.B.
Hikku, G.S.
Powiązania:
https://bibliotekanauki.pl/articles/24200597.pdf
Data publikacji:
2022
Wydawca:
Stowarzyszenie Komputerowej Nauki o Materiałach i Inżynierii Powierzchni w Gliwicach
Tematy:
ZnO NPs
photocatalytic pigment
anti-bacterial pigment
alkyd resin coating
self-cleaning surface
pigment fotokatalityczny
pigment antybakteryjny
powłoka z żywicy alkidowej
powierzchnia samoczyszcząca
Opis:
Purpose: Recently, there has been an upsurge among people around the world in maintaining a sustainable and hygienic environment. This is due to the over-exploitation of recourses causing environmental pollution and spreading bacterial infections. In this regard, scientists are motivated to develop smart coatings where environmental pollutants and bacterial cells are degraded when in contact with their surfaces. Design/methodology/approach: In our previous report, ZnO nanoparticles (NPs) were prepared using the precipitation technique, showing good photocatalytic and antibacterial activity [1]. In this context, the present study details the use of ZnO NPs as pigment for the fabrication of alkyd resin-based self-cleaning coating. The coating was developed by mixing ZnO NPs and alkyd resin along with the additives using the ball milling technique. The developed coating was characterized using field emission scanning electron microscopy, energy dispersive X-ray spectroscopy, atomic force microscopy, and water contact angle measurements. Findings: To elucidate the self-cleaning and hygienic behaviour of the ZnO/alkyd resin coating, the dried coating was exposed to crystal violet (CV) solution as a model dye pollutant and bacterial strains to assess its photocatalytic and antibacterial activity. The droplets of CV solution placed over the coating almost degraded after 360 min of exposure to sunlight owing to the presence of ZnO NPs in the coating. Further, the coating exhibits reasonable antibacterial activity against E. coli and P. aeruginosa whereas it displays low antibacterial activity against S. aureus. Research limitations/implications: Even though, the self-cleaning coating shows promising results, tuning the activity of the photo-catalytic pigment can improve the pollutant degradation efficiency and elevate bactericidal activity. Originality/value: ZnO NPs-impregnated alkyd resin coating for self-cleaning applications is novel.
Źródło:
Archives of Materials Science and Engineering; 2022, 118, 1; 29--35
1897-2764
Pojawia się w:
Archives of Materials Science and Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Determination of the band structure diagram of semiconductor heterostructures applied in photovoltaics
Autorzy:
Bogaczewicz, Rafał Antoni
Popko, Ewa
Gwóźdź, Katarzyna Renata
Powiązania:
https://bibliotekanauki.pl/articles/1835761.pdf
Data publikacji:
2021
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
simulation
semiconductor
heterojunction
band diagram
n-ZnO/p-Si
Opis:
Recently it has been found that the heterostructures of n-ZnO/p-Si are promising photovoltaic alternatives to silicon homojunctions. It is well known that the energy band diagram of a heterostructure is crucial for the understanding of its operation. This paper analyzes the ZnO/p-Si heterostructure band by using free AMPS-1D computer program simulations. The obtained numerical results are compared with theoretical calculations based on the depletion region approximation model and the Poisson’s equation for electric potential. The results of the simulation are also compared with the experimental C-V characteristics of the test n-ZnO/p-Si heterostructure. The simulated C-V characteristics is qualitatively consistent with the experimental C-V curve, which confirms the correctness of the determined band diagram of the n-ZnO/p-Si heterostructure.
Źródło:
Optica Applicata; 2021, 51, 1; 135-145
0078-5466
1899-7015
Pojawia się w:
Optica Applicata
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructures and Microwave-Absorbing Properties of ZnO Smoke from Zinc Leach Residue Treated by Carbothermal Reduction
Autorzy:
Ma, Zhiwei
Wang, Sheng
Du, Xueyan
Zhang, Ji
Zhao, Ruifeng
Zhang, Shengquan
Powiązania:
https://bibliotekanauki.pl/articles/2049146.pdf
Data publikacji:
2021
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
zinc leach residue
carbothermal reduction
ZnO smoke
microwave-absorbing properties
Opis:
Much zinc residue is produced during the traditional processes involved in zinc hydrometallurgy in the leaching stage: its composition is complex and valuable metals are difficult to recover therefrom. If not handled properly, it can lead to a waste of resources and environmental pollution. To solve this problem, zinc leach residue specimens were treated using the carbothermal reduction method (CTR) that is easy to operate and has a high energy utilisation rate. The methods, such as X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and scanning transmission electron microscopy (STEM) were used for analytical characterisation. Based on this, this research investigated a structure-function relationship between microstructures and microwave-absorbing properties of ZnO smoke from CTR-treated zinc leach residue. The results demonstrate that microstructures and macro-properties of ZnO smoke obtained at different temperatures differ greatly. Under conditions including a calcination temperature of 1250°C, holding time of 60 min, and addition of 50% and 10% of powdered coal and CaO separately, the ZnO content in the obtained smoke is 99.14%, with regular micron-sized ZnO particles therein. For these particles, the minimum reflection loss (RLmin) reached –25.56 dB at a frequency of 15.84 GHz with a matching thickness of 5 mm. Moreover, frequency bandwidth corresponding to RL < –10 dB can reach 2.0 GHz. ZnO smoke obtained using this method is found to have excellent microwave-absorbing performance, which provides a new idea for high-value applications of zinc-rich residue.
Źródło:
Archives of Metallurgy and Materials; 2021, 66, 4; 1163--1170
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Oil Recovery from Oilfield Produced Water Using Zinc Oxide Nano Particle as Catalyst in Batch and Continuous System
Autorzy:
Alkhazraji, Hussein Ali Jabbar
Alatabe, Mohammed Jaafar Ali
Powiązania:
https://bibliotekanauki.pl/articles/1955502.pdf
Data publikacji:
2021
Wydawca:
Polskie Towarzystwo Inżynierii Ekologicznej
Tematy:
photocatalytic
produced water
oil content
advanced oxidation processes
AOPs
ZnO/UV
Opis:
This article describes the design of photo catalyst reactor for oil removing from produced water. Real produced water containing a combination of organic compounds was treated with zinc oxide nanoparticles. In this study, ultraviolet radiations were used to find the efficiency of removing the oil content from the water produced that brought from the Al-Ahdab oilfield in kut/ Iraq by advanced oxidation process (AOP) using (ZnO/UV) in batch system and continuous system. In batch system were studied the effect of zinc oxide concentration (nanoparticles), time of irradiation, and pH. The highest removal rate of oil from the produced water (100%) was obtained during the following optimal conditions: ZnO NPs as catalyst = 55 mg/L, pH =3, at the time of irradiation of 90 minutes in batch experiments. In the continuous system, the effects of flowrate, number of UV-A lamp and time of reaction were studied, the results obtained were the efficiency of decomposition decreases with increasing the flow rate of solution in reactor, the maximum removal efficiency of the process (ZnO/UV) was 80% at 20 mL/min and irradiation time 120 min. In general, zinc oxide is beneficial through its high oil adsorption capacity in addition, It lowers the amount of oil in the produced water.
Źródło:
Journal of Ecological Engineering; 2021, 22, 8; 278-286
2299-8993
Pojawia się w:
Journal of Ecological Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Preparation and Characterization of ZnO-Zeolite Nanocomposite for Photocatalytic Degradation by Ultraviolet Light
Autorzy:
Gayatri, Rianyza
Agustina, Tuty Emilia
Bahrin, David
Moeksin, Rosdiana
Gustini, Gustini
Powiązania:
https://bibliotekanauki.pl/articles/1838249.pdf
Data publikacji:
2021
Wydawca:
Polskie Towarzystwo Inżynierii Ekologicznej
Tematy:
nanocomposite
ZnO
synthetic zeolite
sol-gel
photocatalytic degradation
procion red
Opis:
The increasing growth of the textile industry does not only provide benefits in the economic sector but also has the potential to damage the environment, because it generates the dye wastewater which is hard to eliminate. Procion red is one of the synthetic textile dyes that is toxic to the aquatic environment and it needs to be processed properly. The photocatalytic method of processing dye wastewater is the most effective, because it can remove the harmful pollutants in the dye wastewater. This study aimed to prepare and characterize the ZnO-Zeolite nanocomposites for photocatalytic applications tested with a 50 mg/L procion red dye sample. The nanocomposites consisted of the ZnO semiconductors and synthetic zeolite adsorbents prepared by using the sol-gel method. The dye degradation test was carried out under the irradiation conditions with ultraviolet (UV) lamp. Apart from the ZnO-Zeolite nanocomposite, testing was also carried out with the synthetic zeolite and ZnO. The results of SEM-EDX and XRD characterization proved that the nanocomposite forming components were ZnO and zeolite and could be seen from the resulting peaks. BET showed that the surface area value of the ZnO-Zeolite nanocomposite increased to 95.98 m2/g, the pore size of the ZnO-Zeolite nanocomposite was 4.42 nm, and the total pore volume was 0.08 cm3/g. The obtained average crystalline size of ZnO-Zeolite nanocomposite was 32.87 nm. The percentage of dye degradation using the ZnO-Zeolite nanocomposite for 120 minutes has reached 90.42%.
Źródło:
Journal of Ecological Engineering; 2021, 22, 2; 178-186
2299-8993
Pojawia się w:
Journal of Ecological Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Pseudocapacitive Characteristics of Mg Doped ZnO Nanospheres Prepared by Coprecipitation
Autorzy:
Arul, S.
Senthilnathan, T.
Jeevanantham, V.
Satheesh Kumar, K. V.
Powiązania:
https://bibliotekanauki.pl/articles/2049144.pdf
Data publikacji:
2021
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
zinc oxide
Mg-doped ZnO
coprecipitation
cyclic voltammetry
EiS
Opis:
A n-type semiconductor ZnO has high transmittance features, excellent chemical stability and electrical properties. It is also commonly used in a range of fields, such as gas sensors, photocatalysts, optoelectronics, and solar photocell. Magnesium-doped zinc oxide (Mg-ZnO) nano powders were effectively produced using a basic chemical precipitation process at 45°C. Calcined Mg-ZnO nano powders have been characterized by FTIR, XrD, SEM-EDX and Pl studies. XRD measurements from Mg-ZnO revealed development of a crystalline structure with an average particle size of 85 nm and SEM analysis confirmed the spherical morphology. Electrochemical property of produced Mg-ZnO nanoparticles was analyzed and the specific capacitance value of 729 F g-1 at 0.5 A g-1 current density was recorded and retained a specific capacitance ~100 percent at 2 A g-1 current density.
Źródło:
Archives of Metallurgy and Materials; 2021, 66, 4; 1141-1148
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structural, morphological and photoluminescent properties of annealed ZnO thin layers obtained by the rapid sol-gel spin-coating method
Autorzy:
Sypniewska, Małgorzata
Szczesny, Robert
Popielarski, Paweł
Strzałkowski, Karol
Derkowska-Zielinska, Beata
Powiązania:
https://bibliotekanauki.pl/articles/1818231.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Stowarzyszenie Elektryków Polskich
Tematy:
FTIR and Raman spectroscopies
photoluminescence
SEM
XRD
ZnO thin films
Opis:
ZnO thin layers were deposited on p-type silicon substrates by the sol-gel spin-coating method and, then, annealed at various temperatures in the range of 573-873 K. Photoluminescence was carried out in the temperature range of 20-300 K. All samples showed two dominant peaks that have UV emissions from 300 nm to 400 nm and visible emissions from 400 nm to 800 nm. Influence of temperature on morphology and chemical composition of fabricated thin layers was examined by XRD, SEM, FTIR, and Raman spectroscopy. These measurements indicate that ZnO structure is obtained for samples annealed at temperatures above 573 K. It means that below this temperature, the obtained thin films are not pure zinc oxide. Thus, annealing temperature significantly affected crystallinity of the thin films.
Źródło:
Opto-Electronics Review; 2020, 28, 4; 182--190
1230-3402
Pojawia się w:
Opto-Electronics Review
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structural, morphological and photoluminescent properties of annealed ZnO thin layers obtained by the rapid sol-gel spin-coating method
Autorzy:
Sypniewska, Małgorzata
Szczesny, Robert
Popielarski, Paweł
Strzalkowski, Karol
Derkowska-Zielinska, Beata
Powiązania:
https://bibliotekanauki.pl/articles/1818237.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Stowarzyszenie Elektryków Polskich
Tematy:
FTIR and Raman spectroscopies
photoluminescence
SEM
XRD
ZnO thin films
Opis:
ZnO thin layers were deposited on p-type silicon substrates by the sol-gel spin-coating method and, then, annealed at various temperatures in the range of 573-873 K. Photoluminescence was carried out in the temperature range of 20-300 K. All samples showed two dominant peaks that have UV emissions from 300 nm to 400 nm and visible emissions from 400 nm to 800 nm. Influence of temperature on morphology and chemical composition of fabricated thin layers was examined by XRD, SEM, FTIR, and Raman spectroscopy. These measurements indicate that ZnO structure is obtained for samples annealed at temperatures above 573 K. It means that below this temperature, the obtained thin films are not pure zinc oxide. Thus, annealing temperature significantly affected crystallinity of the thin films.
Źródło:
Opto-Electronics Review; 2020, 28, 4; 182--190
1230-3402
Pojawia się w:
Opto-Electronics Review
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication of High Nano-ZnO Doped with Boric Acid Assembled on Cotton Fabric with Flame Retardant Properties
Badanie właściwości ognioodpornych tkaniny bawełnianej pokrytej nano-ZnO
Autorzy:
Ling, Chao
Guo, Lamei
Powiązania:
https://bibliotekanauki.pl/articles/234099.pdf
Data publikacji:
2019
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Biopolimerów i Włókien Chemicznych
Tematy:
high-load
ZnO
boric acid
cotton fabric
flame retardant
kwas borowy
tkanina bawełniana
ognioodporność
Opis:
In this study, an attempt was made to investigate the flame retardancy of cotton fabrics coated with a high nano-ZnO content. Via a simply method in situ, a novel ZnO/cotton composite can be fabricated with a high proportion of nano-ZnO assembled on cotton fabric, where the finished cotton fabric has a certain property of flame retardancy. Discussed herein is the effect of the processed liquid concentration, ammonia-smoking time, and curing temperature on fabric properties such as flame retardancy and hand feeling. Performed were also tests of doping boric acid using the vertical burning method. The finished cotton fabrics were analysed using X-Ray Diffrcation (XRD) and a field emission scanning electron microscope(FESEM), which indicated that between the fibres, and inside the lumen and mesopores of the cotton fibres are assembled with nano-ZnO. The results show that the nano-ZnO content on cotton fabrics can reach up to 15.63 wt%, with the finished cotton fabric having excellent flame retardancy, despite the long after-glow time; however, doping with 0.8 wt% boric acid on the cotton fabric can markedly reduce this. Therefore, a high amount of nano-ZnO doped with boric acid assembled on cotton fabric has great potential in the future.
W pracy podjęto próbę zbadania ognioodporności tkanin bawełnianych pokrytych nano-ZnO. Omówiono wpływ przetworzonej cieczy, stężenie, czas palenia amoniaku i temperaturę utwardzania (wulkanizacji) na właściwości tkaniny bawełnianej, takie jak: ognioodporność i chwyt. Wykonano również analizę kwasu borowego metodą pionowego spalania. Gotowe tkaniny bawełniane analizowano za pomocą dyfrakcji rentgenowskiej (XRD) i skaningowego mikroskopu elektronowego z emisją polową (FESEM), które wskazywały, że między włóknami oraz w lumenach i mezoporach włókien bawełnianych zgromadził się nano-ZnO. Wyniki pokazują, że zawartość nano-ZnO na tkaninach bawełnianych może dochodzić do 15,63% wag., Przy czym gotowa tkanina bawełniana ma doskonałą ognioodporność, pomimo długiego czasu po żarzeniu, jednak dodanie 0,8% wag. kwasu borowego może to znacznie zmniejszyć. Stwierdzono, że zastosowanie nano-ZnO z kwasem borowym na tkaninie bawełnianej ma ogromny potencjał do zastosowania w przyszłości.
Źródło:
Fibres & Textiles in Eastern Europe; 2019, 4 (136); 65-70
1230-3666
2300-7354
Pojawia się w:
Fibres & Textiles in Eastern Europe
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 72

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