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Tytuł:
Optical and TEM characterization of phase transformation in Zn ion implanted and thermal oxidized quartz
Autorzy:
Privezentsev, Vladimir
Powiązania:
https://bibliotekanauki.pl/articles/763347.pdf
Data publikacji:
2016
Wydawca:
Uniwersytet Marii Curie-Skłodowskiej. Wydawnictwo Uniwersytetu Marii Curie-Skłodowskiej
Tematy:
quartz, zinc, ion implantation, annealing, ZnO nanoparticles
Opis:
Metal and metal oxide nanoparticles (NPs) embedded in various matrices have been the object of increasing interest due to their peculiar physical properties significantly different from the corresponding ones of bulk material. Metallic Zn NPs can be used in UV photo-detectors. Zinc oxide NPs play an important role too, since ZnO has direct band gap of 3.37eV, large exiton binding energy of 60meV, sorption effect, room temperature ferromagnetism and others. So they can be used in varies perspective electron devices. In this paper the optical parameters and transmission electron microscopy (TEM) characterization of Zn implanted quartz during NP formation at annealing are reported.Optical-grade high-pure (OH-: 50ppb) amorphous quartz slides were implanted by 64Zn+ ions with fluence of 5×1016/cm2 and energy of 50keV. To avoid the magnificent substrate heating during implantation the ion current density was less than 0.5μA/cm2. Than the samples were subjected to isochronally during 1h oxidation in temperature ranges from 400 up to 800oC. The Zn contained phase creation and its thermal evolution were investigated by recording the optical transmittance spectra at room temperature in a spectral range of 200-800nm and by photoluminescence at temperatures of 10-300K in a spectral range of 350-800nm using an illumination of He-Cd laser with wavelength of 325nm. Visualization and identification of NPs was made by study of the cross section samples TEM fitted with electron diffraction, an EDAX detector attachment for X-ray energy dispersive spectroscopy (EDS), and with a high angle annular dark field detector (HAADF) for scanning operation. The EDS maps of the element distribution and the NP sizes were determined in the scanning TEM regime.As a result of these studies it was found that after the quartz implantation by 64Zn+ ions with fluence of 5×1016/cm2 and energy of 50keV the amorphous metallic Zn NPs with an average radius of 3 nm were created. During process of sequentially isochronally furnace annealing in oxygen atmosphere in 1h in temperature ranges from 400 up to 800oC in samples there was phase transformation from metallic Zn phase to its oxide form. After annealing at 800oC the Zn NPs transform to the ZnO or/and Zn2SiO4 phase with average radius of 4,5nm. 
Źródło:
Annales Universitatis Mariae Curie-Skłodowska, sectio AAA – Physica; 2016, 71
0137-6861
Pojawia się w:
Annales Universitatis Mariae Curie-Skłodowska, sectio AAA – Physica
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Preparation and characterization of ZnO-PMMA resin nanocomposites for denture bases
Autorzy:
Cierech, M.
Wojnarowicz, J.
Szmigiel, D.
Bączkowski, B.
Grudniak, A. M.
Wolska, K. I.
Łojkowski, W.
Mierzwińska-Nastalska, E.
Powiązania:
https://bibliotekanauki.pl/articles/307186.pdf
Data publikacji:
2016
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
nanocząstka ZnO
Candida albicans
polimery akrylowe
ZnO nanoparticles
acrylic resins
Opis:
Purpose: The aim of the paper was to investigate the antifungal activity of zinc oxide nanoparticles (ZnONPs) against Candida albicans. Some attempts have been made to find out the best way to introduce ZnONPs into polymethyl methacrylate (PMMA) resin material and to determine some parameters of a newly formed composite. Material and methods: Zinc oxide nanoparticles were manufactured and their basic physical parameters were determined (average particle size, density, specific surface area). Minimal inhibitory concentration (MIC) of ZnONPs was determined for the Candida albicans standard strain. The average size of ZnO conglomerates in the monomer solution of PMMA resin was measured using a dynamic light scattering instrument. PMMA resin samples with incorporated ZnONPs were produced. The morphology of nanopowder and the newly formed composite was examined under a scanning electron microscope (SEM). In addition, the roughness parameter of PMMA resin material was investigated before and after ZnONPs modification. Results: Nanopowder with the average particle size of 30 nm, density of 5.24 g/cm3 and surface area of 39 m2 /g was obtained. MIC was determined at the level of 0.75 mg/mL. The average size of ZnO conglomerates in the monomer solution of acrylic resin dropped by 11 times after ultrasound activation. SEM examination of a newly formed composite showed a successful introduction of ZnONPs confirmed by the energy dispersive X-ray spectroscopy (EDS) analysis. There were no statistically significant differences in the biomaterial roughness before and after the modification of ZnONPs. Conclusion: Zinc oxide nanoparticles were successfully incorporated into acrylic resin used for the production of denture bases. The presence of nanoparticles with sizes below 100 nm was confirmed. Nevertheless a newly created composite needs to be further investigated to improve its homogeneity, and to check its microbiological properties, strength and biocompatibility prior to its possible clinical use.
Źródło:
Acta of Bioengineering and Biomechanics; 2016, 18, 2; 31-41
1509-409X
2450-6303
Pojawia się w:
Acta of Bioengineering and Biomechanics
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Optical Properties of ZnO Nanoparticles Synthesised from a Polysaccharide and ZnCl₂
Autorzy:
Bindu, P.
Thomas, S.
Powiązania:
https://bibliotekanauki.pl/articles/1032335.pdf
Data publikacji:
2017-06
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
ZnO nanoparticles
UV-vis
band gap
Urbach energy
Opis:
In this article we study the optical properties of ZnO nanoparticles. This paper describes cost effective, high yield, and a facile synthetic method for the synthesis of ZnO nanoparticles from precursors viz. linear polysaccharide, chitosan, and ZnCl₂ by a precipitation method. The synthesized ZnO nanoparticles were characterized by surface area, pore size, and UV-visible measurements. The optical band gap and the Urbach energy were also calculated and the optical band gap energy of the synthesized ZnO nanoparticles was found to be 3.26 eV and the nature of the optical transition has been identified as direct allowed.
Źródło:
Acta Physica Polonica A; 2017, 131, 6; 1474-1478
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Oxidative stress and apotosis to zebrafish (Danio rerio) embryos exposed to perfluorooctane sulfonate (PFOS) and ZnO nanoparticles
Autorzy:
Du, Jia
Cai, Jun
Wang, Shutao
You, Hong
Powiązania:
https://bibliotekanauki.pl/articles/2161865.pdf
Data publikacji:
2017-03-30
Wydawca:
Instytut Medycyny Pracy im. prof. dra Jerzego Nofera w Łodzi
Tematy:
ZnO nanoparticles
perfluorooctane sulfonate
PFOS
zebrafish
Oxidative stress
Apoptosis
Opis:
Objectives Perfluorooctane sulfonate (PFOS) and zinc oxide nanoparticles (ZnO-NPs) are frequently detected in the environment but few studies have assessed the joint toxicity of them. Oxidative stress and apoptosis to zebrafish (Danio rerio) embryos induced by the PFOS and ZnO-NPs were investigated in this study. Material and Methods The embryos were exposed to the PFOS (0, 0.4, 0.8 and 1.6 mg/l), ZnO-NPs (12.5, 25, 50 mg/l) and PFOS plus ZnO-NPs (0.4+12.5, 0.8+25 and 1.6+50 mg/l) mixture solutions until 96 h post-fertilization. Activities of superoxide dismutase (SOD), catalase (CAT), glutathione peroxidase (Gpx) and malondialdehyde (MDA) content were measured in zebrafish embryos after exposure lasting for 96 h. At the same time, the genes expression related to reactive oxygen species (ROS) generation, oxidative damage and apoptosis were also measured. Results A significant induction of the ROS accompanied by the increase in the activity of the Gpx and MDA contents were found in co-treatment groups. Furthermore, several apoptosis pathway related genes such as Bax, p53, caspase-3 and caspase-9 were significantly up-regulated in the PFOS plus ZnO-NPs exposure groups, while anti-apoptotic gene Bcl-2 was significantly down-regulated in the PFOS plus ZnO-NPs exposure groups. In addition, some oxidative stress-related genes such as Cat, GSH peroxidase 1 (Gpx1a) and superoxide dismutase 1 (Sod1) were also significantly down-regulated after the PFOS plus ZnO-NPs co-treatments. Conclusions The results demonstrated that the PFOS plus ZnO-NPs co-exposure could cause more serious oxidative stress and apoptosis than the PFOS and ZnO-NPs exposure alone at the exposure concentrations above. The synergistic effects of the PFOS and ZnO-NPs may be the important mechanisms of their toxicity to zebrafish embryos. Int J Occup Med Environ Health 2017;30(2):213–229
Źródło:
International Journal of Occupational Medicine and Environmental Health; 2017, 30, 2; 213-229
1232-1087
1896-494X
Pojawia się w:
International Journal of Occupational Medicine and Environmental Health
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Antibacterial Composite Layers on Ti: Role of ZnO Nanoparticles
Autorzy:
Roguska, A.
Belcarz, A.
Suchecki, P.
Andrzejczuk, M.
Lewandowska, M.
Powiązania:
https://bibliotekanauki.pl/articles/354849.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
bone implants
TiO2 nanotubes
ZnO nanoparticles
Staphylococcus epidermidis
antibacterial properties
Opis:
Problem of Post-operative infections of implant materials caused by bacterial adhesion to their surfaces is very serious. Enhancement of antibacterial properties is potentially beneficial for biomaterials value. Therefore, the metallic and metallic oxide nanoparticles attract particular attention as antimicrobial factors. The aim of this work was to create nanotubular (NT) oxide layers on Ti with the addition of ZnO nanoparticles, designed for antibacterial biomedical coatings. Antimicrobial activities of titanium, TiO2 NT and ZnO/TiO2 NT surfaces were evaluated against bacterial strain typical for orthopaedic infections: S. epidermidis. TiO2 NT alone killed the free bacterial cells significantly but promoted their adhesion to the surfaces. The presence of moderate amount of ZnO nanoparticles significantly reduced the S. epidermidis cells adhesion and viability of bacterial cells in contact with modified surfaces. However, higher amount of loaded nanoZnO showed the reduced antimicrobial properties than the medium amount, suggesting the overdose effect.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 1; 213-216
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Antibacterial Composite Layers on Ti: Role of ZnO Nanoparticles
Autorzy:
Roguska, A.
Belcarz, A.
Suchecki, P.
Andrzejczuk, M.
Lewandowska, M.
Powiązania:
https://bibliotekanauki.pl/articles/355309.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
bone implants
TiO2 nanotubes
ZnO nanoparticles
Staphylococcus epidermidis
antibacterial properties
Opis:
Problem of post-operative infections of implant materials caused by bacterial adhesion to their surfaces is very serious. Enhancement of antibacterial properties is potentially beneficial for biomaterials value. Therefore, the metallic and metallic oxide nanoparticles attract particular attention as antimicrobial factors. The aim of this work was to create nanotubular (NT) oxide layers on Ti with the addition of ZnO nanoparticles, designed for antibacterial biomedical coatings. Antimicrobial activities of titanium, TiO2 NT and ZnO/TiO2 NT surfaces were evaluated against bacterial strain typical for orthopaedic infections: S. epidermidis. TiO2 NT alone killed the free bacterial cells significantly but promoted their adhesion to the surfaces. The presence of moderate amount of ZnO nanoparticles significantly reduced the S. epidermidis cells adhesion and viability of bacterial cells in contact with modified surfaces. However, higher amount of loaded nanoZnO showed the reduced antimicrobial properties than the medium amount, suggesting the overdose effect.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 2B; 937-940
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis of ZnO nanoparticles by thermal decomposition of basic zinc carbonate
Synteza nanocząstek ZnO na drodze termicznego rozkładu zasadowego węglanu cynku
Autorzy:
Hutera, B.
Kmita, A.
Olejnik, E.
Tokarski, T.
Powiązania:
https://bibliotekanauki.pl/articles/351533.pdf
Data publikacji:
2013
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
ZnO nanoparticles
thermal decomposition
X-ray methods
SEM
nanocząstki ZnO
rozkład termiczny
metody rentgenowskie
Opis:
The paper presents a method for obtaining nanoparticles of ZnO by thermal decomposition of the Zn-containing compounds. The experiment was based on the thermal decomposition of basic zinc carbonate to zinc oxide (with a content of 58-61 wt.%). Basic zinc carbonate was analysed by derivatography and then annealed at a selected temperature (about 600ºC) for about 1 h. Products of thermal decomposition of the compound were studied by XRD analysis and SEM scanning microscopy.
W pracy zaprezentowano metodę otrzymywania nanocząstek ZnO na drodze termicznego rozkładu związków zawierających Zn. W eksperymencie wykorzystano termiczny rozkład zasadowego węglanu tlenku cynku (o zawartości od 58-61% mas.). Zasadowy węglan cynku poddano analizie derywatograficznej a następnie wygrzewaniu w określonej temperaturze (ok. 600ºC przez ok. 1 godz.). Produkty termicznego rozkładu związku badano analizą XRD oraz mikroskopia skaningowa SEM.
Źródło:
Archives of Metallurgy and Materials; 2013, 58, 2; 489-491
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
EVA/zinc oxide nanocomposites for active food packaging : selected physical, and microbial properties
Nanokompozyty EVA/tlenek cynku do aktywnych opakowań do żywności : wybrane właściwości fizyczne i mikrobiologiczne
Autorzy:
Majeed, Haza Satar
Al-Juboory, Farah Khalaf Hammoud
Hamid, Raghad Ali
Zawawi, Ruzniza Mohd
Powiązania:
https://bibliotekanauki.pl/articles/24202791.pdf
Data publikacji:
2023
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Chemii Przemysłowej
Tematy:
ZnO nanoparticles
ethylene vinyl acetate copolymer
barrier properties
nanocząstki ZnO
kopolimer etylen-octan winylu
właściwości barierowe
Opis:
The melt-mixing method was used to obtain nanocomposites of poly(ethylene-co-vinyl acetate) (EVA) with 1, 3 or 5 wt% of hydrophilic zinc oxide (ZnO) nanoparticles. The contact angle, barrier and antimicrobial properties of the obtained composites were investigated. The nanocomposites were characterized by better hydrophilic and barrier properties, as evidenced by, respectively, a smaller contact angle and lower water vapor permeability and water absorption compared to EVA, which can be explained by the formation of hydrogen bonds between EVA and ZnO. In addition, the composites were characterized by greater bactericidal activity against E. coli and S. aureus. The optimal physical and microbial properties were obtained with 3 wt% ZnO content.
Metodą mieszania w stanie stopionym otrzymano nanokompozyty kopolimeru etylen-octan winylu (EVA) z dodatkiem 1, 3 lub 5% mas. hydrofilowych nanocząstek tlenku cynku (ZnO). Zbadano kąt zwilżania, właściwości barierowe i przeciwdrobnoustrojowe otrzymanych kompozytów. Nanokompozyty charakteryzowały się lepszymi właściwości hydrofilowymi i barierowymi, o czym świadczy, odpowiednio, mniejszy kąt zwilżania oraz mniejsza przepuszczalność pary wodnej i absorp¬cja wody w porównaniu z EVA, co można wyjaśnić tworzeniem się wiązań wodorowych pomiędzy EVA i ZnO. Ponadto kompozyty miały większą aktywność bakteriobójczą wobec E. coli i S. aureus. Optymalny zespół właściwości uzyskano przy 3% mas. zawartości ZnO.
Źródło:
Polimery; 2023, 68, 3; 135--141
0032-2725
Pojawia się w:
Polimery
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of water glass modification on its viscosity and wettability of quartz grains
Autorzy:
Kmita, A.
Hutera, B.
Powiązania:
https://bibliotekanauki.pl/articles/380220.pdf
Data publikacji:
2012
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
szkło wodne
synteza termiczna
nanocząstka ZnO
lepkość
zwilżalność
water glass
modification
thermal synthesis
ZnO nanoparticles
viscosity
wettability
Opis:
The aim of the present study was to develop a modifier for water glass. The method of thermal generation of metal oxide nanoparticles was adapted and used in the research. Nanoparticles of ZnO from the thermal decomposition of basic zinc carbonate were used. A method for the modifier introduction was developed, and the effect of modifier content and organic solvent type on the physico-chemical properties of binder (viscosity) and quartz wettability was determined. Binder viscosity was examined from the flow curves plotted with the help of a RHEOTEST 2 rotational rheometer equipped with proper software. Quartz wettability was determined examining time-related changes in the value of the contact angle in a quartz-binder system, until full stabilisation of the angle value has been achieved. Binder modification was carried out on sodium water glass designated as R"145". The water glass modifiers were suspensions of ZnO nanoparticles in propanol and methanol at a fixed concentration of c = 0.3 M and with the size of nanoparticles comprised in a range of <61 - 981 nm>. Water glass modification with the suspensions of ZnO nanoparticles in methanol and propanol showed the effect of modifier on the water glass viscosity and quartz wettability. This effect depends on the type of alcohol used. The ZnO suspension in propanol (alcohol with a longer hydrocarbon chain) affects more strongly the viscosity of binder and quartz wettability than the methanol suspension.
Źródło:
Archives of Foundry Engineering; 2012, 12, 3; 59-62
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of water glass modification with nanoparticles of zinc oxide on selected physical and chemical properties of binder and mechanical properties of sand mixture
Autorzy:
Kmita, A.
Hutera, B.
Olejnik, E.
Janas, A.
Powiązania:
https://bibliotekanauki.pl/articles/381352.pdf
Data publikacji:
2012
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
thermal synthesis
ZnO nanoparticles
wettability
tensile strength
moulding sand
synteza termiczna
nanocząsteczki ZnO
wytrzymałość na rozciąganie
masa formierska
Opis:
In this paper, an attempt was made to use the ZnO nanoparticles as a modifier of foundry binder - water glass. The modifier was a colloidal suspension of the ZnO zinc oxide nanoparticles in propanol. A thermal method to obtain metal oxide nanoparticles was adopted. The modifier was product of the thermal decomposition of the basic zinc carbonate ([ZnCO3]2•[Zn(OH)2]3), and was introduced into the water glass in an amount of 1 and 3 wt%. To determine the interfacial reactions taking place in a quartz - modified water glass system, the binder wettability of the quartz grains was measured. The effect of water glass modification on the mechanical properties of moulding sands was verified by testing the tensile strength Rmu of moulding sands with the modified binders. Water glass modification with the colloidal solution of ZnO nanoparticles in propanol confirmed the effect of modifier on the water glass wettability of sand grains and on the mechanical properties of the sand mixtures with this additive.
Źródło:
Archives of Foundry Engineering; 2012, 12, 2s; 37-40
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Production of Zinc oxide nanoparticles using extracts of Passiflora edulis Sims. f. flavicarpa Deg.
Autorzy:
Manokari, M.
Shekhawat, Mahipal S.
Powiązania:
https://bibliotekanauki.pl/articles/1192673.pdf
Data publikacji:
2016
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Passiflora edulis Sims. f. flavicarpa Deg.
UV-Visible double beam spectrophotometry
aqueous extracts
ZnO nanoparticles
Opis:
The synthesis of zinc oxide nanoparticles (ZnO) using herbal extract is always environmentally benign. The present investigation focuses on the synthesis of ZnO nanoparticles using aqueous extracts of various parts of Passiflora edulis Sims. f. flavicarpa Deg. (Passion fruit). The plant is rich in alkaloids, glycosides, flavonoids and triterpenes. UV-Visible double beam spectrophotometric analysis was used for characterization of ZnO nanoparticles with different time intervals which were synthesized by plant extracts. The bio-reduction completes in two hr incubation of reaction mixtures with strong broad peaks at 332 nm from leaves, 296 nm from stem and 326 nm from flower extracts. Hence the biosynthesis of ZnO nanoparticles using aqueous extracts of P. edulis could be an alternative to chemical methods and exploited in various biofields.
Źródło:
World Scientific News; 2016, 47, 2; 267-278
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Electrochemical synthesis of ZnO nanoparticles during anodic dissolution of zinc in alcohols solvents
Elektrochemiczna synteza nanocząstek ZnO na drodze anodowego roztwarzania cynku w rozpuszczalnikach alkoholowych
Autorzy:
Stypuła, B.
Starowicz, M.
Hajos, M.
Olejnik, E.
Powiązania:
https://bibliotekanauki.pl/articles/351108.pdf
Data publikacji:
2011
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
cynk
roztwarzanie anodowe
rozpuszczalniki organiczne
nanocząstki ZnO
zinc
anodic dissolution
organic solvents
nanoparticles ZnO
Opis:
Studies of the effect of the kind of alcohol, electrolyte concentration and water on the anodic dissolution of zinc and the nature of dissolution products were performed. The dissolution products were analyzed by spectroscopic methods (SEM/EDS, XPS and UV-vis) and X-ray diffraction. These studies have shown that the process of anodic dissolution of zinc in alcohol electrolytes (methanol and ethanol) in the presence of water (1-5% vol.), is a simple way to obtain ZnO nanoparticles.
Przeprowadzono badania wpływu rodzaju alkoholu, stężenia elektrolitu oraz zawartości wody na proces anodowego roztwarzania cynku i charakter tworzących się produktów roztwarzania w obszarze wysokich potencjałów. Do identyfikacji produktów anodowego roztwarzania wykorzystano spektroskopowe techniki badawcze (SEM/EDS, XPS, UV-vis) oraz metodę dyfrakcji rentgenowskiej. Badania te wykazały że proces anodowego roztwarzania cynku w alkoholowych elektrolitach (metanolowych i etanolowych) w obecności wody (1-5% obj.), jest prostym sposobem otrzymywania nanocząstek ZnO.
Źródło:
Archives of Metallurgy and Materials; 2011, 56, 2; 286-292
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of annealing temperature on the optical properties of ZnO nanoparticles
Autorzy:
Ismail, R. A.
Habubi, N. F.
Abid, H. R.
Powiązania:
https://bibliotekanauki.pl/articles/412203.pdf
Data publikacji:
2014
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
nanoparticles
ZnO film
optical properties
drop casting technique
Opis:
In this work, ZnO films were prepared by drop casting technique. The films were deposited on quartz substrates under different annealing time (15,30,45 and 60 min.) at a constant temperature (800 °C). The optical properties were achieved by measuring the absorbance and transmittance spectra in the wavelength range (200-900) nm. It was found that the absorbance decreases while transmission increases as the annealing time increases, while the reflectance decreases as the annealing time increases. The optical measurements indicate the kind of transition which was a direct allowed with an average band gap energies lie between 3.3 eV and 3.54 eV with the change of annealing time.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2014, 4; 37-47
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Antibacterial activity of modified zinc oxide nanoparticles against Pseudomonas aeruginosa isolates of burn infections
Autorzy:
Aysa, Noor Hadi
Salman, Halah Dawood
Powiązania:
https://bibliotekanauki.pl/articles/1191368.pdf
Data publikacji:
2016
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Antimicrobial activity
Pseudomonas aeruginosa
ZnO
burn infection
nanoparticles
surface modification
Opis:
In this research antimicrobial activity of nanoparticles ZnO on perilous bacteria such as Pseudomonas aeruginosa was evaluated. P. aeruginosa is important pathogen that caused burn wound infections as it is multi-drug resistant and has several virulence factors. Fifteen samples of P. aeruginosa were collected from patients who suffering from Burn infections in Al-Hilla teaching hospital burn unit with the age range between (7-80) years old for both genders. After collecting burn samples, the diagnosis and characterization were performed by culturing and biochemical tests. ZnO NPs were synthesized by chemical method, Zinc oxide nanoparticles are well-known to be one of the multifunctional inorganic compounds which are widely used in medical applications. This study aims to prepare ZnO nanoparticles with particle size ranging from 23-29  nm. In the present study, surface modification of ZnO nanoparticles was performed, and influence of modification of the structure and morphological properties was investigated. The resulting nanoparticles were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and atomic force (AFM). Zinc oxide nanoparticles with the average diameter of about 29 nm were modified with an oleic acid to exert more compatibility. From the results obtained it is suggested that modified ZnO-nanoparticles could be used effectively in safety environmental and medical applications. Antibacterial activity for nanoparticle ZnO against P. aeruginosa isolates was measured by: Agar Diffusion Technique and Minimum Inhibitory Concentration (MIC)/Minimum bactericidal Concentration (MBC) with microdilution. The best zone of inhibition was (35.5mm) at a concentration of 40 μg/ml of nano-ZnO in one strain of P. aeruginosa while the lowest inhibition zone was (16 mm) at a concentration of 20 μg/ml of nano ZnO in one strain also. In addition, all P. aeruginosa isolates were completely inhibited at the concentration of 3.7 μg/ml of nano-ZnO (MIC) but no significant antibacterial activity was observed at concentrations less than 1.8 μg/ml of nano-ZnO and the (MBC) was same as MIC (3.7 μg/ml) for all P.aeruginosa isolates.
Źródło:
World Scientific News; 2016, 33; 1-14
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Si/ZnO nanorods with Ag nanoparticles/AZO heterostructures in PV applications
Autorzy:
Gwóźdź, K.
Płaczek-Popko, E.
Gumienny, Z.
Zielony, E.
Pietruszka, R.
Witkowski, B. S.
Wachnicki, Ł.
Gierałtowska, S.
Godlewski, M.
Chang, L. B.
Powiązania:
https://bibliotekanauki.pl/articles/201432.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
solar cells
ZnO
Si
heterojunction
nanorods
nanoparticles
ogniwa słoneczne
nanopręty
nanocząstki
Opis:
Our studies focus on test structures for photovoltaic applications based on zinc oxide nanorods grown using a low-temperature hydrothermal method on a p-type silicon substrate. The nanorods were covered with silver nanoparticles of two diameters – 20–30 nm and 50–60 nm – using a sputtering method. Scanning electron microscopy (SEM) micrographs showed that the deposited nanoparticles had the same diameters. The densities of the nanorods were obtained by means of atomic force microscope (AFM) images. SEM images and Raman spectroscopy confirmed the hexagonal wurtzite structure of the nanorods. Photoluminescence measurements proved the good quality of the samples. Afterwards an atomic layer deposition (ALD) method was used to grow ZnO:Al (AZO) layer on top of the nanorods as a transparent electrode and ohmic Au contacts were deposited onto the silicon substrate. For the solar cells prepared in that manner the current-voltage (I-V) characteristics before and after the illumination were measured and their basic performance parameters were determined. It was found that the spectral characteristics of a quantum efficiency exhibit an increase for short wavelengths and this behavior has been linked with the plasmonic effect.
Źródło:
Bulletin of the Polish Academy of Sciences. Technical Sciences; 2016, 64, 3; 529-533
0239-7528
Pojawia się w:
Bulletin of the Polish Academy of Sciences. Technical Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 16

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