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Wyszukujesz frazę "Spray Pyrolysis" wg kryterium: Temat


Tytuł:
Structural and optical properties of nanocrystalline CdS films prepared by spray pyrolysis
Autorzy:
Aljarrah, Radhyah M. S.
Aljobory, Adnan H.
Powiązania:
https://bibliotekanauki.pl/articles/1179009.pdf
Data publikacji:
2017
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Cadmium Sulphide
CdS films
spray pyrolysis
Opis:
Cadmium Sulphide (CdS) thin films are produced using spray pyrolysis deposition technique. Films are annealed in air at 400, 500, and 600 K of 1 h. It characterized by X-Ray Diffraction (XRD), Atomic Force Microscope (AFM) and optical properties of CdS. XRD shows that these films are polycrystalline in nature with cubic and hexagonal crystalline structure. The crystallite size, microstrain, and dislocation density were measured. AFM shows that the total substrate surface is finely covered with uniformly distributed spherical shaped grains. Optical transmittance was shown that direct transition with band gap energy was decreased between 2.44 to 2.27 eV with annealing.
Źródło:
World Scientific News; 2017, 87; 175-190
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The impact of Cu alloy on auxiliary and invisible options of splash kept CdS slims
Autorzy:
Kadhim, Mohammed A.
Powiązania:
https://bibliotekanauki.pl/articles/1188099.pdf
Data publikacji:
2016
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
CdS
spray pyrolysis
optical properties
Cu concentration
Opis:
Cadmium Sulfide and copper alloyed Cd1-xS Cux slims have been set up by the spray pyrolysis technique. The optical gap crevices at unadulterated and doped Cadmium Sulfide were observed to be shifted from (2.34 to 2.45) eV with increment x from (0 to 0.1). The X-beam diffraction (XRD) investigation uncovered that slims were polycrystalline and showed two phases cubic and hexagonal structure with increasing the hexagonal phase with increment Cu ratio.
Źródło:
World Scientific News; 2016, 56; 217-228
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Plasma-Enhanced Atmospheric Pressure Spray Pyrolysis System for the Production of Few Walls Carbon Nanotubes
Autorzy:
Soto, Gerardo
Ramírez-Hernández, Felipe
Muñoz-Muñoz, Franklin
Covarrubias, Cristian
Powiązania:
https://bibliotekanauki.pl/articles/1162427.pdf
Data publikacji:
2018
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
few-walls carbon nanotubes
plasma enhanced
spray pyrolysis
Opis:
Spray pyrolysis is a recognized technique for the preparation of multi-walled Carbon Nano-Tubes (CNTs). Likewise, gas-phase plasma synthesis has the best potential to produce nanoparticles with narrow sized distribution in short times. Here we present a combination of both concepts to design an atmospheric-pressure plasma reactor in a configuration which can be scaled for massive production of few-walls CNTs. This hybrid setup uses a pneumatic nebulizer which produces an aerosol from a solution of toluene (the carbon source) in the presence of ferrocene (the catalyst). The mist goes toward the plasma zone, which is generated by a DC-soldering torch. The plasma effect is to reduce the droplet size of the nebulizer. By this mean the agglomeration of Fe nanoparticles is reduced and consequently, the number of walls and diameter of CNTs are decreased.
Źródło:
World Scientific News; 2018, 111; 64-73
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis of Single Crystalline Titanium Oxide and Sodium Titanate Nanorods via Salt-Assisted Ultrasonic Spray Pyrolysis
Autorzy:
Hwangbo, Y.
Yoo, J.-H.
Lee, Y.-I.
Powiązania:
https://bibliotekanauki.pl/articles/352337.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
TiO2
nanorods
salt
Ultrasonic Spray Pyrolysis
optical properties
Opis:
The simple and continuous synthesis of single crystalline anatase titanium dioxide and sodium titanate nanorods by a saltassisted ultrasonic spray pyrolysis method is demonstrated. This method does not require expensive precursors, long reaction time, and physical templates or surfactant. In addition, its continuous nature makes it a suitable method for the large-scale preparation. Moreover, the effect of a salt concentration in a starting solution on material properties, including morphology and phase of the synthesized products was systematically investigated. The synthesized nanorods had one-dimensionality, a single crystalline and the average diameter of 12.3 nm with dual phases of titanium dioxide and sodium titanate by FE-SEM, XRD, HR-TEM as well as FFT-converted SAED pattern analysis.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1411-1414
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fluorine-Doped SnO2 Thin Films in Solar Cell Applications. Morphological, Optical and Electrical Properties
Autorzy:
Lisnic, Petru
Hrostea, Laura
Leontie, Liviu
Girtan, Mihaela
Powiązania:
https://bibliotekanauki.pl/articles/27313873.pdf
Data publikacji:
2023
Wydawca:
Polska Akademia Nauk. Czasopisma i Monografie PAN
Tematy:
fluorine tin oxide
FTO
thin films
spray pyrolysis
solar cells
Opis:
This study examines the optimal parameters for obtaining fluorine-doped SnO2 (FTO) films with promising potential for photovoltaic applications. Due to its properties, tin oxide is used in a wide range of technologies, among which the manufacture of solar cells is one of the most important. Being doped with fluorine, tin dioxide becomes a good transparent and conductive electrode, suitable for solar cell applications. The chemical stability and low cost of the doped SnO2 makes it an advantageous alternative to tin-doped indium oxide (ITO). Among the most important characteristics of FTO thin films are high photoconductivity under sunlight irradiation and strong UV absorption. The SnO2 compound, doped with fluorine, exhibits a considerable chemical and physical stability, good electrical conductivity and high transmission (over 85%) in the visible range. The spray pyrolysis technique is the most preferable and efficient deposition method of fluorine-doped SnO2 thin films. This work aims to identify the optimal parameters for the spray pyrolysis of SnO2:F films and to analyze the morphology, transparency and strength of as obtained films in relation to the doping amount in the precursor solution, spraying distance and film thickness.
Źródło:
Archives of Metallurgy and Materials; 2023, 68, 2; 483--490
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Optical dispersion characterization of sprayed Zn1-xMnxO thin films
Autorzy:
Habubi, N.F.
Chiad, S.S.
Oboudi, S.F.
Toma, Z.A.
Powiązania:
https://bibliotekanauki.pl/articles/411575.pdf
Data publikacji:
2013
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
TCOs
Dispersion parameters
spray pyrolysis
zinc oxide
Zn1-xMnxO
Opis:
Uniform and adherent Zn1-xMnxO films have been deposited by using spray pyrolysis technique on glass substrates. The optical properties and dispersion parameters of zinc oxide have been studied as a function of doping concentration with Mn. Changes in direct optical energy band gap of cobalt oxide films were confirmed after doping, The optical energy gap Eg increased from 3.13 eV for the undoped ZnO to 3.39 eV with increasing the doping concentration of Mn to 4%. The changes in dispersion parameters and Urbach tails were investigated. An increase in the doping concentration causes a decrease in the average oscillator strength. The single-oscillator parameter has been reported.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2013, 4; 1-8
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication and Characterization of ZnO/p-Si Heterojunction Solar Cell
Autorzy:
Habubi, Nadir F.
Mousa, Abdulazeez O.
Powiązania:
https://bibliotekanauki.pl/articles/1193961.pdf
Data publikacji:
2015
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
chemical spray pyrolysis
heterojunction solar cell
n-ZnO/p-Si
Opis:
Zinc oxide thin films was deposited by chemical spray pyrolysis (CSP) at 400 °C substrate temperature and different thickness (60, 80, and 100) nm on the texturized p-Si wafer to fabricate ZnO/p-Si heterojunction solar cell. Structural, optical, electrical and photovoltaic properties are investigated for the samples. XRD analysis reveals that all the as deposited ZnO films show polycrystalline structure, without any change due to increase of thickness. Average diameter calculated from AFM images shows an increase in its value with increasing thickness, ranging from 59.82-95.7 nm. The optical reflections for samples are measured using UV-Vis spectrophotometer. Photoluminescence (PL) spectra of (CSP) grown ZnO/p-Si with different thickness were used to study the energy gap. The electrical properties of heterojunction were obtained by I-V (dark and illuminated) and C-V measurement. I-V characteristic of the ZnO/p-Si heterojunction shows good rectifying behavior under dark condition. The ideality factor and the saturation current density was calculated. Under illuminated the photovoltaic measurements (open-circuit voltage (Voc), short-circuit current density (JSC), fill factor (FF), and quantum efficiencies are calculated for all samples. The built- in potential (Vbi), carrier concentration and depletion width are determined under different thickness from C-V measurement.
Źródło:
World Scientific News; 2015, 18; 78-92
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Urbach energy and dispersion parameters of CdS chemically deposited thin films on the effect of thickness
Autorzy:
Hadi, Ahmed Hussin
Powiązania:
https://bibliotekanauki.pl/articles/1177946.pdf
Data publikacji:
2018
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
CdS thin film
Dispersion parameters
Urbach energy
chemical spray pyrolysis
Opis:
Optical transmittance spectra of CdS thin films were recorded from UV-Visible spectrophotometer in the range 380-900 nm. The films were prepared by chemical spray pyrolysis by spraying an aqueous solution of cadmium chloride (CdCl2) and thiourea [(NH2)2CS] with de-ionized water. UV-Visible spectrophotometer used to recording the transmittance spectra in the range of 380-900 nm. The transmittance decreased with the increasing of CdS film thickness, while the reflectance increases. The energy gap decreased with the increasing of film thickness, while Urbach energy increased. Dispersion parameters such as; Ed, Eo, ε∞, n(0), So, λo, M-1, and M-3 are studied.
Źródło:
World Scientific News; 2018, 97; 241-249
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Optical characteristics of Portulaca grandiflora-doped Cellulose using the spray pyrolysis technique
Autorzy:
Alaridhee, Tahseen
Obeed, Mohammed T.
Malk, Fatima H.
Dhahi, Baheya A.
Powiązania:
https://bibliotekanauki.pl/articles/27315701.pdf
Data publikacji:
2023
Wydawca:
Polska Akademia Nauk. Stowarzyszenie Elektryków Polskich
Tematy:
green materials
optical properties
natural dye
biopolymer
spray pyrolysis technique
Opis:
Thin films were prepared based on cellulose polymer doped with different ratios of natural dye derived from Portulaca grandiflora concentrations. The polymer and natural dye were extracted from eco-friendly materials - the cell walls of millet husks and Portulaca grandiflora, respectively. The spray pyrolysis technique was applied to prepare thin film samples to control the film morphology and reduce the roughness of the surface. Optical microscope and Fourier transform infrared were used to analyse structural, morphological, and functional groups for all samples, respectively. The peak absorbance, extinction coefficient, optical bandgap, Urbach energy, and optical conductivity for the thin films were determined using ultraviolet-visible spectroscopy. The results show an enhancement in the optical characteristics when the natural cellulose is doped with a dye. Doping cellulose with 5% P. grandiflora has led to a considerable reduction in the energy bandgap (to 1.95 eV), compared to the sample doped with 1%.
Źródło:
Opto-Electronics Review; 2023, 31, 3; art. no. e146553
1230-3402
Pojawia się w:
Opto-Electronics Review
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Heat Treatment on the Optical Properties of Cobalt Doped Stannic Oxide
Autorzy:
Hasan, J. S.
Powiązania:
https://bibliotekanauki.pl/articles/411548.pdf
Data publikacji:
2014
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
thin films
chemical spray pyrolysis
dilute magnetic semiconductor
stannic oxide
doping
Opis:
This study investigates The effect of annealing on The optical properties of (SnO2:Co) films prepared by spray pyrolysis (SP) technique at a glass substrate temperature (Ts = 773 K). The absorbance and transmittance spectra have been recorded in order to calculate the optical constant and the optical band gap energy of the films. It was found that the annealing affects all the parameters under investigations.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2014, 9; 59-70
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Nanostructured CdO thin films for LPG and CO2 gas sensor prepared by spray pyrolisis technique
Autorzy:
Bari, R. H.
Patil, S. B.
Powiązania:
https://bibliotekanauki.pl/articles/411726.pdf
Data publikacji:
2014
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
spray pyrolysis techniques
LPG
CO2 sensor
nanostructured CdO
gas response
Opis:
Nanostructured CdO thin films were deposited by spray pyrolysis techniques at different spray deposition time on glass substrates. Nanostructured CdO thin films was prepared using 0.05 M of cadmium acetate dehydrate (CH3COO) 2Cd•2H2O) was dissolved in the deionised water. These thin films were annealing in air at temperatures 500 °C for 60 min. The thickness of the films, crystallite and grain size were observed to increase with the increase in spray deposition time. As prepared thin films were characterized using XRD, FE-SEM and EDAX. The XRD analysis shows that CdO films were cubic structured. The electrical and gas sensing properties of these films were investigated. Prepared nanostructure CdO thin films show LPG (S = 1600) and CO2 (S = 435) gas response at different operating temperature. Gas response, selectivity, response and recovery time of the sensor were measured and presented.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2014, 18; 31-46
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Substrate Temperature on Structural and Optical Properties of CdO Thin Films
Autorzy:
Ali, H. R. A.
Powiązania:
https://bibliotekanauki.pl/articles/411893.pdf
Data publikacji:
2014
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
cadmium oxide
spray pyrolysis technique
XRD
AFM
thin films
sol-gel
Opis:
Thin films of CdO have been prepared by spray pyrolysis technique. XRD analysis reveals that all the prepared samples were polycrystalline and have preferred orientation along [111] orientation. The surface topography was determined by AFM which indicate that surface roughness and rms roughness were increased by the increasing of substrate temperature. The optical energy gap were determined and its value lies between (2.4-2.5) eV.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2014, 8; 47-55
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structural and Optical Properties of Fe2O3 - NiO mixed Thin Films Prepared by Chemical Spray Pyrolysis
Autorzy:
Mohmmed, N. J.
Habubi, M. N.
Powiązania:
https://bibliotekanauki.pl/articles/412381.pdf
Data publikacji:
2014
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Fe2O3
spray pyrolysis technique
structural properties
optical properties
Opis:
Mixed Fe2O3 - NiO thin films have been prepared by chemical Spray pyrolysis technique onto glass substrate preheated to 450 °C. The thickness of thin films was found to be (400 ±20) nm. XRD measurements reveal that all the film exhibit polycrystalline hexagonal wrutzite with a preferred orientation along (104) plane for pure and 10 % and 20 % Ni, while for the rest the structure was amorphous. AFM analysis indicate a nanostructure for all the films. The optical energy gap was found to be increased from optical transitions seems to be direct and the optical energy gap seems to be increased from 2.5 to 2.69 eV as the percentage of NiO increase.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2014, 14, 1; 65-85
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Co Doping on Structural and Optical Properties of NiO Thin Films Prepared By Chemical Spray Pyrolysis Method
Autorzy:
Bakr, N. A.
Salman, S. A.
Shano, A. M.
Powiązania:
https://bibliotekanauki.pl/articles/412102.pdf
Data publikacji:
2015
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
NiO thin films
Co Doping
Chemical Spray Pyrolysis
Optical Properties
Structural Properties
Opis:
In this work, nickel-cobalt oxide (Ni(1-x)CoxO) thin films, where x = 0, 4, 6 and 8 % have been successfully deposited on glass substrates by chemical spray pyrolysis (CSP) technique at substrate temperature of (400 °C) and thickness of about 300 nm. The structural and optical properties of these films have been studied using XRD, AFM, and UV-Visible spectroscopy. The XRD results showed that all films are polycrystalline in nature with cubic structure and preferred orientation along (111) plane. The crystallite size was calculated using Scherrer formula and it is found that the undoped NiO sample has maximum crystallite size (51.16 nm). AFM results showed homogenous and smooth thin films. The absorbance and transmittance spectra have been recorded in the wavelength range of (300-900) nm in order to study the optical properties. The optical energy gap for allowed direct electronic transition was calculated using Tauc equation. It is found that the band gap decreases as the Co-concentration increases and the band gap values were in the range of 3.58-3.66 eV and 3.58 eV for the prepared Nickel-Cobalt Oxide thin films. The Urbach energy increases as the Co-concentration increases and the Urbach. The optical constants including (absorption coefficient, real and imaginary parts of dielectric constant) were also calculated as a function of photon energy. Refractive index and extinction coefficient for Nickel- Cobalt Oxide thin films were estimated as a function of wavelength.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2015, 41; 15-30
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis of Y2O3-Dispersed W Powders Prepared by Ultrasonic Spray Pyrolysis and Polymer Solution Route
Autorzy:
Jo, Hyeonhui
Lee, Young-In
Suk, Myung-Jin
Jeong, Young-Keun
Oh, Sung-Tag
Powiązania:
https://bibliotekanauki.pl/articles/2049335.pdf
Data publikacji:
2021
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
tungsten
Y2O3 dispersion
ultrasonic spray pyrolysis
wet chemical route
Opis:
The nano-sized Y2O3 dispersed W composite powder is prepared by ultrasonic spray pyrolysis of a tungsten precursor using ammonium metatungstate hydrate and a polymer addition solution method using Y-nitrate. XRD analysis for calcined powder showed the formation of WO2 phase by partial oxidation of W powder during calcination in air. The TEM and phase analysis for further hydrogen reduction of calcined powder mixture exhibited that the W powder with a uniform distribution of Y2O3 nanoparticles can be successfully produced. These results indicate that the wet chemical method combined with spray pyrolysis and polymer solution is a promising way to synthesis the W-based composites with homogeneous dispersion of fine oxide particles.
Źródło:
Archives of Metallurgy and Materials; 2021, 66, 3; 799-802
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł

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