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Wyszukujesz frazę "Sol–gel process" wg kryterium: Temat

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    Wyświetlanie 1-6 z 6
    Tytuł:
    Study on Magnetic Properties of the U-Type Ferrite According to Substituted Elements
    Autorzy:
    Jeong, Kwang-Pil
    Kim, Jeong-Gon
    Yang, Su-Won
    Yun, Jae-Ho
    Choi, Jin-Hyuk
    Powiązania:
    https://bibliotekanauki.pl/articles/354006.pdf
    Data publikacji:
    2019
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    U-type ferrite
    hexagonal ferrite
    sol-gel process
    Opis:
    The magnetic properties of the U-type ferrite synthesized by a sol-gel process had studied by substituting cobalt with manganese or zinc in cobalt-based U-type ferrite. The substituted U-type ferrite showed a dominant crystal structure at a different substitution ratio of manganese and zinc. The change of the starting temperature of U-type ferrite formation according to substitutional elements was confirmed by TG-DTA analysis. In the case of manganese substitution, the starting temperature of U-type ferrite formation lowered, and on the contrary, when zinc was substituted, it became higher. The magnetic properties of the U-type ferrite substituted with manganese showed a tendency that the saturation magnetization was decreased and the coercivity was increased as the manganese ratio increased. The highest saturation magnetization was 57.9 emu/g in the specific composition (Ba4Co0.5Zn1.5Fe36O60) substituted with zinc.
    Źródło:
    Archives of Metallurgy and Materials; 2019, 64, 2; 501-505
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Microspheres and Pellets of UO2 Prepared Via ADU by Complex Sol-Gel Process and ICHTJ Process
    Autorzy:
    Brykala, M.
    Rogowski, M.
    Wawszczak, D.
    Olczak, T.
    Smolinski, T.
    Powiązania:
    https://bibliotekanauki.pl/articles/357030.pdf
    Data publikacji:
    2020
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    uranium dioxide
    microspheres
    pellets
    Complex Sol-Gel Process
    ICHTJ Process
    Opis:
    This study is devoted to synthesis and characterization of uranium dioxide microspheres (Ø < 100 μm) and pellets by application of powder-free process called the Complex Sol-Gel Process. The precursors of prepared sols were ascorbic acid solution with dissolved a freshly precipitated ammonium diuranate. The microspheres of uranyl-ascorbate gel were obtained using the ICHTJ Process. The pellets were formed by pressing and sintering of uranium dioxide powder. Studies allowed determining an optimal heat treatment of calcination, reduction and sintering processes at temperatures of 700°C, 900°C and 1300°C, respectively. The main parameters which play a key role in the process of synthesis method and features of the pellets and microspheres of uranium dioxide are described in this article.
    Źródło:
    Archives of Metallurgy and Materials; 2020, 65, 4; 1397-1404
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Carbonization of solid uranyl-ascorbate gel as an indirect step of uranium carbide synthesis
    Autorzy:
    Brykala, M.
    Rogowski, M.
    Olczak, T.
    Powiązania:
    https://bibliotekanauki.pl/articles/147109.pdf
    Data publikacji:
    2015
    Wydawca:
    Instytut Chemii i Techniki Jądrowej
    Tematy:
    carbonization
    complex sol-gel process (CSGP)
    uranium carbide
    uranyl-ascorbate complex
    Opis:
    The studies of the synthesis of uranium carbide from uranyl-ascorbate gels using the complex sol-gel process (CSGP) have been carried out. The synthesis of uranyl-ascorbate mixture as liquid sol from uranium trioxide and ascorbic acid and solid gel by extraction of water from sol were carefully examined. Ascorbic acid was used as a complexing agent in complex sol-gel process and as a carbon source. The crucial step to obtain final uranium carbides from the aforementioned substrates is the carbonization process. The thermal behavior of ascorbic acid and uranyl-ascorbate gels in a nitrogen atmosphere in the temperature range of 25–900°C were investigated using TG-DTG. Furthermore, the products of the carbonization of uranyl-ascorbate gels in nitrogen, argon and vacuum atmosphere were identifi ed by X-ray diffraction. TG-DTG was used also as a method for determining of carbon residues in the samples.
    Źródło:
    Nukleonika; 2015, 60, No. 4, part 2; 921-925
    0029-5922
    1508-5791
    Pojawia się w:
    Nukleonika
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Thermal properties of porous sodium polyacrylate/silica nanocomposites
    Właściwości termiczne porowatych nanokompozytów poliakrylan sodu/krzemionka
    Autorzy:
    Korobeinyk, Alina
    Yurchenko, Gabriella
    Matkovsky, Alexander
    Tertykh, Valentin
    Powiązania:
    https://bibliotekanauki.pl/articles/24202781.pdf
    Data publikacji:
    2023
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Chemii Przemysłowej
    Tematy:
    sol-gel process
    porous nanocomposites
    sodium polyacrylate
    proces zol-żel
    porowate nanokompozyty
    poliakrylan sodu
    Opis:
    Porous sodium polyacrylate/silica (SPA/SiO2) nanocomposites were obtained in a single-stage sol-gel process involving the acidic hydrolysis of tetramethoxysilane (TMOS) in the presence of SPA. The TMOS/SPA molar ratio ranged from 2:1 to 8:1. The physical and thermal properties of the nanocomposites were characterized by FTIR, SEM, TGA and adsorption analysis (BET, BJH). The mechanical and chemical treatment of the composite after the synthesis increased its specific surface area without significantly changing thermal properties. The process enables pore size control.
    Porowate nanokompozyty poliakrylan sodu/krzemionka (SPA/SiO2) otrzymano w jednoetapowym procesie zol-żel polegającym na kwaśnej hydrolizie tetrametoksysilanu (TMOS) w obecności SPA. Stosunek molowy TMOS/SPA wynosił od 2:1 do 8:1. Właściwości fizyczne i termiczne otrzymanych nanokompozytów scharakteryzowano za pomocą FTIR, SEM, TGA i analizy adsorpcyjnej (BET, BJH). Mechaniczna i chemiczna obróbka kompozytu po procesie syntezy zwiększyła jego powierzchnię właściwą bez znaczącej zmiany właściwości termicznych. Proces umożliwia kontrolę wielkości porów.
    Źródło:
    Polimery; 2023, 68, 2; 106--112
    0032-2725
    Pojawia się w:
    Polimery
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Synthesis and investigation of optical, structural, and morphological characteristics of nanostructured TiO2-ZnO thin films
    Autorzy:
    Yasir, Nagham Abdulameer
    Hlail, Alzubaidy Muneer
    Mohsin, Ali Kamel
    Powiązania:
    https://bibliotekanauki.pl/articles/1070855.pdf
    Data publikacji:
    2019
    Wydawca:
    Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
    Tematy:
    Crystallite size
    Photocatalysis
    Sol–gel process
    Titanium dioxide
    X-Ray Diffraction
    Zinc oxide
    drop casting
    energy gap
    thin films
    Opis:
    TiO2-ZnO thin films have been prepared by using drop casting technique. The optical, structural, and morphological properties of nanostructured TiO2-ZnO thin films deposited by drop casting technique was studied by using several experimental techniques were used to characterize optical, structural, and morphological properties; X-Ray Diffraction (XRD) was used to study the crystal structures, the crystallite size, the dislocation density, and the number of crystallites per unit area of TiO2-ZnO thin films. The surface topography, surface roughness parameters, and average grain size for all samples were done by Atomic Force Microscopy (AFM) micrograph which confirm the existence of Nano-structured thin films. The optical energy gap of the TiO2-ZnO thin films was determined by using UV spectroscopy. It was found that one type of basic electrons transitions, through which the values of the optical energy gap for all the prepared thin films which are allowed direct transition.
    Źródło:
    World Scientific News; 2019, 123; 87-101
    2392-2192
    Pojawia się w:
    World Scientific News
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    ZrO2-CeO2 ceramic powders obtained from a sol-gel process using acetylacetone as a chelating agent for potential application in prosthetic dentistry
    Autorzy:
    Nakonieczny, D.
    Paszenda, Z.
    Drewniak, S.
    Radko, T.
    Lis, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/306436.pdf
    Data publikacji:
    2016
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    proces zol-żel
    metody rentgenowskie
    analiza termiczna
    ZrO2
    protetyka
    sol-gel process
    X-ray Methods
    Thermal Analysis
    Prosthetic Dentistry
    Opis:
    Purpose: The main objective of this study was to obtain single-phase β-ZrO2 powders with so-called soft agglomerates reproducibile morphology with acetyl-acetone as a chelating-agent. To the best of our knowledge there is no avaiable data which determine the effect of acetyl acetone on the phase composition and morphology of ceria-doped ZrO2 powders for biomedical applications. Methods: Twenty variants of powders with different water to zirconia precursor and acetylacetone to zirconia precursor molar ratios were prepared. 0.9ZrO20.1CeO2 powders were obtained by a hydrolysis and condensation and further calcination of zirconium n-propoxide in a simple one-step sol-gel process. Influence of acetyloacetone to zirconia precursor on the phase composition ratio and water to zirconia precursor was investigated. Samples have been characterized by X-ray diffraction (XRD), Raman spectroscopy (RS), thermal analysis (TGA/DTA) and scanning electron microscopy (SEM) measurements. Results: Ceramic powders prepared by sol-gel process, according to the various concentration of chelating agent and water show different morphology and phase composition. Conclusions: Higher molar ratios of AcAc in range with smaller amounts of water cause hard agglomerates, obtained powders are characterized by highly thermally stable behaviour and various phase composition. With higher molar ratios of water to zirconium-n-propoxide so-called soft agglomerates and one phase powders are obtained.
    Źródło:
    Acta of Bioengineering and Biomechanics; 2016, 18, 3; 53-60
    1509-409X
    2450-6303
    Pojawia się w:
    Acta of Bioengineering and Biomechanics
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-6 z 6

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