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Wyświetlanie 1-15 z 60
Tytuł:
Assessment of substituent effects on β-naphthyl based isoxazoles by IR and NMR spectra
Autorzy:
Thirunarayanan, G.
Sathiyendiran, V.
Arulkumarn, R.
Sundararrajan, R.
Manikandan, R.
Vanangamud, G.
Powiązania:
https://bibliotekanauki.pl/articles/1194022.pdf
Data publikacji:
2015
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Correlation analysis
IR spectra
NMR spectra
β-naphthyl dihydroisoxazoles
Opis:
A series containing thirteen 3-(2-naphthyl)-5-(substituted phenyl)-4,5-dihydroisoxazole have been synthesized and examined their purities by their data reported earlier. The characteristic infrared νC=N (cm-1) stretches, NMR chemical shifts (δ, ppm) of H4,4׳, H5 protons, C3-5 carbons were assigned and correlated with Hammett substituent constants and Swain-Lupton’s parameters using single and multi- regression analysis. From the results of regression analysis the effect of substituents on the spectral data have been studied.
Źródło:
World Scientific News; 2015, 9; 35-58
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structure parameter correlation of some quinoxaline derivatives through IR and 13C NMR spectra
Autorzy:
Thirunarayanan, G.
Muthuvel, I.
Sathiyendiran, V.
Powiązania:
https://bibliotekanauki.pl/articles/412003.pdf
Data publikacji:
2014
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Quinoxalines
IR spectra
NMR spectra
Hammett Correlation
substituent effects
Opis:
A series of 6-substituted quanoxaline derivatives have been synthesized and examined their purities by literature method. The infrared and 13>/Sup>C NMR spectral data of these quinoxalines were correlated with Hammett substituent constants, F and R parameters using single and multi-regression analysis. From the results of statistical analysis, the effect of substituents on the spectral frequencies has been studied.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2014, 19, 2; 198-207
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis, spectroscopic characterization and antimicrobial evaluation of some (E)-N-(4-substitutedbenzylidene)-4-fluorobenzenesulfonamides
Autorzy:
Jayanthi, P.
Jesu Retna Raj, G.
Sekar, M.
Thanikachalam, V.
Powiązania:
https://bibliotekanauki.pl/articles/1113828.pdf
Data publikacji:
2017
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
4-fluorobenzenesulfonamide
Bauer-Kirby
IR spectra
NMR spectra
antimicrobial activities
Opis:
In the present study, six numbers of Schiff bases (1-6) have been synthesized by the condensation of 4-fluorobenzenesulfonamide and substituted aromatic aldehyde. The purities of these Schiff bases have been checked by their physical constants, IR, 1H NMR and 13CNMR spectral data. The antimicrobial activities of these Schiff bases have been evaluated using Bauer-Kirby method.
Źródło:
World News of Natural Sciences; 2017, 13; 101-112
2543-5426
Pojawia się w:
World News of Natural Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Hammett spectral correlations in benzofuranyl flavonols
Autorzy:
Thirunarayanan, G.
Sekar, K. G.
Powiązania:
https://bibliotekanauki.pl/articles/412326.pdf
Data publikacji:
2014
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Benzofuranyl flavonols
Hammett equation
IR spectra
NMR spectra
Regression analysis
Opis:
A series containing eleven benzofuranyl flavonols have been prepared by cyclization of 3-hydroxybenzofuranyl chalcones with 30 % hydrogen peroxide in the presence of sodium bicarbonate. The synthesized flavonols were characterized by their physical constants, analytical and spectroscopic data. The infrared spectral νOH, CO stretches(cm-1), NMR chemical shifts of OH, CO(δ, ppm) of these flavonols were assigned and correlated with Hammett substituent constants, F and R parameters using single and multi linear regression analysis. From the results of statistical analyses, the effects of substituents on the above group frequencies were discussed.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2014, 6; 39-47
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
IR and NMR spectral studies of some 4-(6-methoxy-2-naphthyl)-5,6-dihydro-6-(substituted phenyl)-4H-1,3-oxazine-2-amines: Assessment of substituent effects
Autorzy:
Thirunarayanan, G.
Powiązania:
https://bibliotekanauki.pl/articles/412242.pdf
Data publikacji:
2014
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Oxazine-2-amines
IR spectra
NMR spectra
Hammett correlation
Substituent constans
Opis:
A series containing thirteen title compounds were synthesized and recorded IR and NMR spectra. The infrared νNH, C=N(cm-1)stretches, 1H NMR δNH, 13C NMR δC=N(ppm) chemical shifts of synthesized oxazine amines were assigned and correlated with Hammett substituent constants, F and R parameters. From the results of statistical analyses, the effect of substituents on the above spectral frequencies can be discussed.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2014, 4; 109-116
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis, spectral studies and antimicrobial activities of some substituted (E)-1-benzylidene-2-(4-bromophenyl)hydrazines
Autorzy:
Rajarajan, M.
Senbagam, R.
Vijayakumar, R.
Manikandan, V.
Balaji, S.
Vanangamudi, G.
Thirunarayanan, G.
Powiązania:
https://bibliotekanauki.pl/articles/1194024.pdf
Data publikacji:
2015
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Antimicrobial study
Hammett equation
Hydrazone
IR spectra
NMR spectra
Synthesis
UV
Opis:
A series of nine number of (E)-1-benzylidene-2-(4-bromophenyl)hydrazine compounds have been synthesized by the condensation reaction of 4-bromo phenylhydrazine with varies m- and p- substituted benzaldehydes using acetic acid catalyst were refluxed for 4h with 20 mL of absolute ethanol. The yield of synthesized (E)-1-benzylidene-2-(4-bromophenyl)hydrazine compounds are more than 80%. The synthesized (E)-1-benzylidene-2-(4-bromophenyl)hydrazines have been characterized by UV, IR, 1H and 13C spectral data. These UV, IR and NMR spectral data have been correlated with varies Hammett substituted constant and Swain-Lupton F and R parameters using single and multi- regression analysis. From the results of statistical analysis, the effects of substituent have been studied. The antimicrobial activity of all the synthesized substituted (E)-1-benzylidene-2-(4-bromophenyl)hydrazines have been evaluated using Bayer-Kirby method.
Źródło:
World Scientific News; 2015, 9; 144-160
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Spectral studies of some (5-substituted phenyl) isoxazole based sydnones: Assessment of substituent effects
Autorzy:
Thirunarayanan, G.
Vanangamudi, G.
Sathiyendiran, V.
Powiązania:
https://bibliotekanauki.pl/articles/1194034.pdf
Data publikacji:
2015
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Hammett substituent constants
IR spectra
NMR spectra
Spectral LFER
Sydnone isoxazole
Opis:
About ten 4-(N-(4-(5-phenylisoxazol-3-yl)phenylsufamyl)-3-(p-tolyl)-1,2,3,-oxadiazol-3-ium-5-olates were synthesised and examined their purities by literature method. The infrared and NMR spectral data of above synthesised isoxazoles were assigned and correlated with Hammett substituent constants and Swain-Lupton’s constants using regression analysis. From statistical analyses results, the effects of substituents on the spectral data have been discussed.
Źródło:
World Scientific News; 2015, 11; 44-64
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis, spectral correlations and biological activities of some (E)-[4-(substituted benzylidene amino)phenyl] (phenyl) methanones
Autorzy:
Mayavel, P.
Thirumurthy, K.
Dineshkumar, S.
Thirunarayanan, G.
Powiązania:
https://bibliotekanauki.pl/articles/412136.pdf
Data publikacji:
2014
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Schiff's bases
fly-ash
PTS
IR spectra
NMR spectra
Hammett correlation
Opis:
A series of Schiff’s bases have been synthesized by fly-ash:p-toluenesulfonic acid (fly-ash:PTS) catalyzed microwave assisted oxidative coupling of arylamines and substituted benzaldehydes under solvent-free condition. The synthesized Schiff’s bases are characterized by their physical constants, analytical and spectroscopic data. The group frequencies of imines such as IR (v, cm–1) and NMR (δ, ppm) spectral data was correlated with Hammett substituent constants, F and R parameters using single and multi-linear regression analysis. The antimicrobial activities of these Schiff’s bases have been studied using Bauer-Kirby method.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2014, 20, 2; 145-159
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
NMR Spectral correlations in some Tröger’s bases
Autorzy:
Thirunarayanan, G
Suresh, M.
Powiązania:
https://bibliotekanauki.pl/articles/412650.pdf
Data publikacji:
2014
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
tröger’s bases
NMR spectra
hammett correlations
substituent effects
Opis:
Some Tröger’s bases have been synthesised from substituted anilines and paraformaldehyde in presence of Lewis acid catalyst such as anhydrous AlCl3, through electrophilic substitution reaction. The purities of these Tröger’s bases have been checked by their physical constants and spectroscopic data published earlier in the literature. The NMR chemical shift (δ, ppm) of methylene protons and carbon were assigned. The assigned methylene protons and carbon chemical shifts (δ, ppm) of synthesised Tröger’s bases have been correlated with Hammett substituent constants, F and R parameters using single and multi-regression analyses. From the results of statistical analyses, the effects of substituent on methylene protons and carbon were discussed.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2014, 4; 1-11
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis, spectral correlation analysis and evaluation of biological activities of some substituted hydrazones
Autorzy:
Vijayakumar, Renganathan
Senbagam, Rajamohan
Rajarajan, Murugan
Balaji, Selvaraj
Manikandan, Venkatesan
Vanangamudi, Ganesan
Thirunarayanan, Ganesamoorthy
Powiązania:
https://bibliotekanauki.pl/articles/764124.pdf
Data publikacji:
2015
Wydawca:
Uniwersytet Marii Curie-Skłodowskiej. Wydawnictwo Uniwersytetu Marii Curie-Skłodowskiej
Tematy:
Hydrazones
UV
IR & NMR spectra
Correlation analysis
Antimicrobial activities
Opis:
Some novel substituted hydrazone derivatives of amino guanidine have been synthesized with different substituted benzaldehydes by condensation method. The synthesized hydrazones were characterized by their physical constants, UV, IR and NMR spectra. The spectral data have been correlated with Hammett substituent constants and Swain–Lupton parameters. From the result of statistical analysis, the effects of substituents on the spectral data have been predicted. The antimicrobial activities of these synthesized hydrazone compounds have been screened by Bauer-Kirby method using human pathogenic bacteria and fungal species. The antimicrobial activities of all synthesized hydrazone compounds have shown significant activity.
Źródło:
Annales Universitatis Mariae Curie-Skłodowska, sectio AA – Chemia; 2015, 70, 2
2083-358X
Pojawia się w:
Annales Universitatis Mariae Curie-Skłodowska, sectio AA – Chemia
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Spectral LFER in some aryl azine derivatives
Autorzy:
Thirunarayanan, G.
Powiązania:
https://bibliotekanauki.pl/articles/1191375.pdf
Data publikacji:
2016
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Aryl hydrazines
Hammett correlations
IR spectra
NMR spectra
Swain-Lupton’s parameters
Opis:
About ten (Z)-1-(1-(substitutedphenyl)ethylidene)-2-(diphenylmethylene)hydrazines were prepared and their purities were examined by literature method. The infrared and NMR spectra of these hydrazines were recorded. The characteristics C=N and N-N stretches (ν, cm-1) and the chemical shifts (δ, ppm) of methyl protons and carbons were assigned. These spectral have been correlated with Hammett substituent constants, F, R and Swain-Lupton’s parameters using single and multi-regression analysis. From the results of statistical analyses, the effects of substituent on the spectral data have been studied.
Źródło:
World Scientific News; 2016, 33; 79-95
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis, spectral (FT-IR, 1H and 13C NMR) and antimicrobial studies some of (E)-2-(2-((aryl)(phenyl)methylene)hydrazinyl)benzo[d] thiazole
Autorzy:
Manikandan, S.
Thirunarayanan, G.
Powiązania:
https://bibliotekanauki.pl/articles/1177421.pdf
Data publikacji:
2018
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Aryl hydrazone
IR and NMR spectra
antibacterial and antifungal activities
Opis:
A series of (E)-2-(2-((aryl)(phenyl)methylene)hydrazinyl)benzo[d] thiazole compounds by condensation of substituted benzophenone with 2-hydrazinobenzothizol in the presence acetic acid. The synthesized compounds 1-6 were characterized by elemental, FT-IR, 1H and 13C NMR spectral data. From the IR and NMR spectra, the characteristic frequencies were assigned and the data used for confirmation of the formation hydrazones 1-6. All compounds were screened for their preliminary antibacterial and antifungal activities. The methoxy substituted compound 6 shows good antibacterial activity against their bacterial strains within the agreed mm of zone of inhibition. The methyl (5) and methoxy (6) substituted hydrazones show good antifungal activities against their fungal strains.
Źródło:
World Scientific News; 2018, 103; 1-18
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Hammett spectral correlations in some aryl 1,3-oxazine-4-thione derivatives
Autorzy:
Thirunarayanan, G.
Sekar, K. G.
Powiązania:
https://bibliotekanauki.pl/articles/412394.pdf
Data publikacji:
2014
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
1,3-oxazine-4-thiones
IR spectra
13C NMR spectra
Hammett correlation
Opis:
A series of some aryl 1,3-oxazine-4-thione derivatives have been synthesized by 1-methyl imidazole catalyzed three component one pot synthetic method in room temperature. The purities of these thiones were studied by their physical constants and spectroscopic data. The infrared and 13C NMR spectral data of CN and CS were correlated with Hammett substituent constants, F and R parameters using single and multi-linear regression analysis. From the results of statistical analysis, the effect of substituent on the spectral data was studied.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2014, 17, 2; 193-200
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Infrared and ¹³C NMR spectral studies of some aryl hydrazides: Assessment of substituent effects
Autorzy:
Thirunarayanan, G.
Sekar, G. K.
Lakshmi Narayanan, R.
Powiązania:
https://bibliotekanauki.pl/articles/412577.pdf
Data publikacji:
2014
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
substituted aryl benzohydrazide
IR spectra
NMR spectra
hammett equation
substituent constants
correlation analysis
Opis:
A series of some aryl hydrazides have been synthesized. These hydrazides purities were analyzed by physical constants and spectral data. The assigned spectral group frequencies were correlated with Hammett substituent constants and Swain-Lupton parameters using single and multi-linear regression analysis. From the results of statistical analysis, the effect of substituents on the spectral group frequencies has been discussed.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2014, 13, 1; 88-94
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
IR and NMR spectral LFER study on 3-benzoicacid based sulfonamides
Autorzy:
Dineshkumar, Selvakumar
Thirunarayanan, Ganesamoorthy
Powiązania:
https://bibliotekanauki.pl/articles/1182898.pdf
Data publikacji:
2016
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
3-(substituted phenylsulfonamido)benzoic acids
ir and nmr spectra
correlation analysis
Opis:
A series containing nine 3-(substituted phenylsulfonamido)benzoicacids) have been synthesized and examined their purities by their data reported earlier. The characteristic infrared (NH, SO(as), SO(sym) and CO(as) cm-1) stretches, NMR chemical shifts (δ, ppm) of NH protons, CO carbons were assigned and correlated with Hammett substituent constants and Swain-Lupton’s parameters using single and multi-regression analysis. From
Źródło:
World Scientific News; 2016, 53, 3; 367-384
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 60

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