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Wyświetlanie 1-15 z 30
Tytuł:
Spectral LFER studies in some N-(substituted phenyl) formamides
Autorzy:
Thirunarayanan, Ganesamoorthy
Muthuvel, Inasekaran
Sathiyendiran, Vasudevan
Powiązania:
https://bibliotekanauki.pl/articles/764126.pdf
Data publikacji:
2015
Wydawca:
Uniwersytet Marii Curie-Skłodowskiej. Wydawnictwo Uniwersytetu Marii Curie-Skłodowskiej
Tematy:
N-(Substituted phenyl)formamides
Sulphated titania(TiO2-SO4–-)
IR and NMR spectra
Anilines
Hammett correlations.
Opis:
A series of N-(substituted phenyl) formamides were synthesised by sulphated titania (TiO2-SO4 2-) catalyzed formylation of substituted anilines and formic acid in acetonitrile medium at room temperature. The synthesised formamide derivatives are characterized by their spectral data. The infrared νNH, CO (cm-1) stretches, chemical shifts(δ, ppm) of NH, COH and ipso carbons(Ar-C-NH) were assigned and correlated with Hammett substituent constants using single and multi-regression analysis. From the results of statistical analyses, the effect of substituents on the spectral data have been studied.
Źródło:
Annales Universitatis Mariae Curie-Skłodowska, sectio AA – Chemia; 2015, 70, 2
2083-358X
Pojawia się w:
Annales Universitatis Mariae Curie-Skłodowska, sectio AA – Chemia
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Spectral Quantitative Structure activity relationships in 3-(substituted phenyl) bicyclo[2.2.1]hept-5-en-2-yl-(pyrene-1-yl) methanone derivatives
Autorzy:
Thirunarayanan, Ganesamoorthy
Powiązania:
https://bibliotekanauki.pl/articles/1191973.pdf
Data publikacji:
2016
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
2
3-Diarylbicyclo[2.2.1]-hept-5-ene-2-yl methanones; Greener synthesis
Correlation analysis
Hammett equation
IR and NMR spectra
QSAR study
Opis:
About nine titled compounds were synthesized by greener method and the purities of these methanones have been examined using their analytical and spectral data reported in literature. The infrared and NMR spectral data of these methanones were assigned and correlated with Hammett substituent constants, F and R parameters using single and multi-linear regression analysis. From the results of statistical analyses, the effects of substituents in terms of spectral quantitative structure activity on the spectral frequencies were studied.
Źródło:
World Scientific News; 2016, 50; 74-94
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Study of IR and NMR spectral correlations and biological evaluation of 4-(6-ethyl-2-(substituted phenyl)-6H-pyrido[3,2-b]carbazol-4-yl) aniline derivatives
Autorzy:
Thirunarayanan, Ganesamoorthy
Powiązania:
https://bibliotekanauki.pl/articles/1189992.pdf
Data publikacji:
2016
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
IR and NMR spectra
Substituent effects
Hammett equation
Antibacterial activity
Antifungal activity
pyrido[3
2-b]carbazol-4-yl) aniline
Opis:
A series of seven titled compounds have been prepared and their purities were examined by literature method. The characteristic infrared stretching frequencies (, cm-1) and the NMR chemical shifts (, ppm) of these anilines were assigned. These assigned spectral data were correlated with Hammett substituent constants, F and R parameters using single and multi-regression analysis. From the statistical results the effect of substituents on the spectral data have been discussed. The antimicrobial activities of these aniline derivatives have been evaluated by Bauer-Kirby disc-diffusion method.
Źródło:
World Scientific News; 2016, 52; 228-246
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Ultrasonicated Synthesis of Bio-potent Sulphonamides
Autorzy:
Thirunarayanan, Ganesamooorthy
Powiązania:
https://bibliotekanauki.pl/articles/1075695.pdf
Data publikacji:
2019
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Antimicrobial activity
Antioxidant activity
Aryl sulfonamides
IR and NMR spectra
Sodium acetate
Ultrasonication
Opis:
About more than 85% yields of some aryl sulphonamides were synthesised by sodium acetate catalysed ultrasonication promoted condensation of aryl amines and benzene sulfonyl chlorides in room temperature. The synthesised sulfonamides were analysed with their physical constants, micro analysis and spectral techniques. The antioxidant potential of these sulfonamides were assessed by DPPH radical scavenging activity measurement using L-ascorbic acid as a standard. Antimicrobial activities of these sulfonamides have been assessed by disc diffusion method against their antimicrobial stains. Most of the sulfonamides shows antimicrobial activity. Many of the hydroxy and methoxy substituted sulfonamides showed significant antioxidant activity.
Źródło:
World Scientific News; 2019, 119; 125-138
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Application of Hammett equation on IR and NMR spectral data of (5-bromothiophen-2-yl) (3-(4-methoxyphenyl)bicyclo[2.2.1]hept-5-en-2-yl)methanones
Autorzy:
Thirunarayanan, G.
Powiązania:
https://bibliotekanauki.pl/articles/1182868.pdf
Data publikacji:
2016
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
(5-bromothiophen-2-yl)(3-substituted phenyl)bicyclo[2.2.1]hept-5-en-2-yl)methanones
ir and nmr spectra
hammett equation
hammett substituent constants
regression analysis
electronic effects
Opis:
More than 60% yield of the titled compounds, (5-bromothiophen-2-yl)(3-substituted phenyl) bicyclo[2.2.1]hept-5-en-2-yl)methanones were prepared and examined their purities by literature method. The characteristic infrared spectral frequencies (cm-1) and NMR chemical shifts (ppm) of these ketones were assigned. These spectral data were applied to Hammett equation with Hammett substituent constants for prediction of effects substituent using single and multi-regression analysis. From the results of statistical analysis, the electronic effect of substituents on the spectral data has been studied.
Źródło:
World Scientific News; 2016, 53, 3; 138-156
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Cu2+/Zeolite catalyzed synthesis and evaluation of antimicrobial activities of some chalcones
Autorzy:
Thirunarayanan, G.
Kumar, N. Dinesh
Powiązania:
https://bibliotekanauki.pl/articles/1179609.pdf
Data publikacji:
2017
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Antimicrobial activities
Aryl chalcones
Cu2+/Zeolite
IR and NMR spectra
Opis:
Some aryl chalcones have been synthesized by Cu2+/Zeolite catalyzed aldol condensation of aryl methyl ketones and substituted benzaldehydes under microwave irradiation conditions. The yields of the synthesized chalcones are more than 85%. These chalcones were characterized by their physical constants and spectroscopic data. The antimicrobial activities of synthesized chalcones were studied by Bauer-Kirby disc diffusion method.
Źródło:
World Scientific News; 2017, 74; 251-266
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Greener synthesis and Hammett spectral Linearity’s of some 1-{[3-(furan-2-yl)-5-phenyl-4,5-dihydro-1,2-oxazol-4-yl]methyl}-4-methyl piperazines
Autorzy:
Thirunarayanan, G.
Rajarajan, M.
Sekar, K. G.
Sathiyendiran, V.
Powiązania:
https://bibliotekanauki.pl/articles/1179600.pdf
Data publikacji:
2017
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Hammett equation and Regression analyses
Hammett substituent constants
IR and NMR spectra
Piperazines
Opis:
We have synthesized eleven numbers of 1-{[3-(furan-2-yl)-5-phenyl-4,5-dihydro-1,2-oxazol-4-yl]methyl}-4-methyl piperazines by hydroxyapatite catalyzed microwave assisted condensation method. The synthesized 1-{[3-(furan-2-yl)-5-phenyl-4,5-dihydro-1,2-oxazol-4-yl]methyl}-4-methyl piperazine compounds were characterized by means of their IR and NMR spectral data. The assigned infrared spectral νC=N, νC-O-C stretches(cm-1), NMR chemical shifts of isoxazoline (d) proton, isoxazoline (m) proton, N-CH3, C=N, C-NH2 and C-NH3 (δ, ppm) of these 1-{[3-(furan-2-yl)-5-phenyl-4,5-dihydro-1,2-oxazol-4-yl]methyl}-4-methyl piperazines were assigned and correlated with Hammett substituent constants, F and R parameters using single and multi linear regression analysis. From the results of statistical analyses, the effects of substituents on the above group frequencies were discussed.
Źródło:
World Scientific News; 2017, 74; 164-180
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Infrared and NMR spectral Hammett correlations in 4-(2-naphthyl)-5,6-dihydro-6-(substituted phenyl)-4H-1,3-oxazine-2-amines
Autorzy:
Thirunarayanan, G.
Pazhamalai, S.
Sekar, K. G.
Powiązania:
https://bibliotekanauki.pl/articles/411654.pdf
Data publikacji:
2014
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Oxazine-2-amines
IR and NMR spectra
Hammett equation
Correlation analysis
Opis:
A series containing ten titled compounds have been synthesised and recorded the IR and NMR spectra. From the spectra the infrared νNH, C=N, C-O-C stretches, NMR chemical shifts of (δ, ppm) NH and C=N were assigned and correlated with Hammett substituent constants, F and R parameters using single regression analysis. From the results, the effects of substituent on the above spectral frequencies were discussed.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2014, 8; 38-46
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Insect antifeedant potent unsaturated 1,3-oxazine-2-amines
Autorzy:
Thirunarayanan, G.
Renuka, V.
Sekar, K.G.
Lakshmanan, K.
Anbarasu, K.
Powiązania:
https://bibliotekanauki.pl/articles/412312.pdf
Data publikacji:
2014
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Insect antifeedant activity
4th instar larvae Achoea Janata L
Aryl 1,3-oxazine
Castor leaf discs
Green synthesis
IR and NMR spectra
Opis:
Insect antifeedant activities of some halo substituted aryl 1,3-oxazine-2-amines have been measured using 4th instar larvae Achoea Janata L by castor leaf discs-Dethler’s method. The highly halo substituted oxazine amines have shown good insect antifeedant activities. The 1,3-oxazine amines have been synthesised by greener method by solvent-free cyclization of aryl enones with urea under microwave irradiation. The yields of the oxazines were more than 80 %. The synthesised oxazines were characterized by their physical constants, analytical and spectroscopic data.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2014, 4; 66-81
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
IR & NMR spectral studies of some 7-substituted 9H-fluorenacyl bromides: Assessment of substituent effects
Autorzy:
Thirunarayanan, G.
Powiązania:
https://bibliotekanauki.pl/articles/412017.pdf
Data publikacji:
2013
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
9H-Fluorenacyl bromides
IR and NMR spectra
Hammett substituent constants
Correlation analysis
Opis:
A series of some 2-bromo-1-(2-substituted 9H-fluorene-7-yl)ethanones have been prepared. The purities of these ethanones have been checked by their physical constants and spectroscopic data. The spectral group frequencies of these enones have been assigned and correlated with Hammett substituent constants, F and R parameters. From the results of statistical analyses, the effects of substituent have been discussed.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2013, 9, 2; 152-161
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Solid acidic Bentonite/FeCl3 catalysed solvent-free cyclization of some aryl enones: Synthesis and assessment of antimicrobial potentials of some aryl pyrazolines
Autorzy:
Thirunarayanan, G.
Dineshkumar, N.
Rajarajan, M.
Powiązania:
https://bibliotekanauki.pl/articles/1076026.pdf
Data publikacji:
2019
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
1
3
5-Substituted pyrazolines
Antimicrobial activities
Bentonite/FeCl3
IR and NMR Spectra
Solvent-free synthesis
Opis:
Some aryl pyrazolines including 3-(substituted phenyl)-5-(naphthalen-1-yl)-1-phenyl-4,5-dihydro-1H-pyrazoles were prepared by microwave irradiation promoted cyclization of aryl enones and phenylhydrazine in the presence of solid acidic bentonite/FeCl3 catalyst under solvent-free conditions. In this cyclization the obtained yields are more than 75%. The structural analysis of these pyrazoline derivatives were confirmed through analytical and spectral techniques. The effect of catalyst and solvent on this cyclization also investigated through the obtained yields. The antimicrobial activities of these pyrazoline derivatives were assessed through measurement of mm of zone of inhibition against their micro stains using well known Bauer-Kirby disc diffusion method.
Źródło:
World Scientific News; 2019, 117; 14-28
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Solvent-free synthesis and spectral linearity of some (E)-2-(substituted benzylideneamino)-N-(3-chloro-4-fluorophenyl)-hexahydro-2H cyclopenta[b]thiophene-3-carboxamides
Autorzy:
Thirunarayanan, G.
Sekar, K. G.
Powiązania:
https://bibliotekanauki.pl/articles/412418.pdf
Data publikacji:
2013
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Solvent-free condensation
SiO2-H3PO4
Imine-carboximido derivatives
IR and NMR spectra
Hammett correlations
Opis:
Some (E)-2-(substituted benzylideneamino)-N-(3-chloro-4-fluorophenyl)-hexahydro-2H-cyclopenta[b]thiophene-3-carboxamide derivatives have been synthesized by SiO2:H3PO4 catalyzed solvent-free condensation of 2-amino-N-(3-chloro-4-fluorophenyl)-hexahydro-2H-cyclopenta [b]thiophene-3-carboxamide and various substituted benzaldehydes in microwave irradiation. The yield of the imine-carboximido derivatives has been found to be more than 85 %. The purity of all imine-carboximido derivatives has been checked using their physical constants and spectral data. The spectral data of the imine-carboximido derivatives such as infrared ? (cm-1) of CO, NH, C-N, C-Cl, C-F, C=N, and the NMR chemical shifts (?, ppm) of NH, CH, CO and C=N have been correlated with Hammett substituent constants, F and R parameters. From the results of statistical analysis, the effects of substituent on the above spectral group absorptions have been discussed.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2013, 8, 2; 160-174
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Spectral QSAR and QPR study of some (E)-4-(((2 hydroxy-6-(substituted phenyl)-1,6 dihydropyrimidin 4-yl)methyl)diazenyl)benzoic acid derivatives
Autorzy:
Thirunarayanan, G.
Sekar, K. G.
Powiązania:
https://bibliotekanauki.pl/articles/412619.pdf
Data publikacji:
2014
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Dihydropyrimidines
Diazenyl benzoic acids
IR spectra
NMR spectra
Hammett correlation
QSAR and QPR study
Opis:
A series of titled compounds were synthesized and recorded the infrared and NMR spectra. The assigned spectral group frequencies were correlated with Hammett substituent constants, F and R parameter. From the statistical analysis results, the effect of substituents on the spectral group frequencies has been studied.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2014, 17, 1; 10-20
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Insect antifeedant potent halogen substituted phenyl chalcones
Autorzy:
Sundararajan, R.
Arulkumaran, R.
Vijayakumar, S.
Kamalakkannan, D.
Suresh, R.
John, J. S.
Ranganathan, K.
Sakthinathan, S. P
Vanangamudi, G.
Thirunarayanan, G.
Powiązania:
https://bibliotekanauki.pl/articles/412081.pdf
Data publikacji:
2014
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Substituted styryl 2′,3′,4′-trichlorophenyl ketones
sulfated Titania
IR and NMR spectra
Insect antifeedant activities
Opis:
Some 2′,3′,4′-trichlorophenyl chalcones [(E)-1-(2,3,4-trichlorophenyl)-3-(substituted phenyl)-2-propen-1-ones] have been synthesised using sulfated Titania catalyzed solvent-free aldol condensation between 2,3,4-trichloroacetophenone and substituted benzaldehydes. The purities of synthesised chalcones were checked by their analytical, physical and spectroscopic data reported in literature. The insect antifeedant activities of these chalcones have been studied using 4th instar larvae Achoea Janata L by castor leaf disc bio-assay method. The chloro substituted chalcones shows significant insect antifeedant activity.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2014, 1; 67-73
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis, assessment of substituent effect and antimicrobial activities of some substituted (E)-Nbenzylidene- 5-bromopyridin-2-amines
Autorzy:
Senbagam, Rajamohan
Vanangamudi, Ganesan
Thirunarayanan, Ganesamoorthy
Powiązania:
https://bibliotekanauki.pl/articles/763969.pdf
Data publikacji:
2015
Wydawca:
Uniwersytet Marii Curie-Skłodowskiej. Wydawnictwo Uniwersytetu Marii Curie-Skłodowskiej
Tematy:
E-imines
UV
IR and NMR spectra
Spectral QSAR study
Antimicrobial activities
Opis:
A series of substituted (E)-N-benzylidene-5-bromopyridin-2-amine compounds have been synthesized from 5-bromo-2-aminopyridine with different substituted benzaldehydes. The structure of the adducts was confirmed by their physical constants, UV, IR and NMR spectral data. The observed UV absorption maximum λmaxC=N(nm), IR frequencies νC=N(cm-1), The 1H and 13C NMR δ(ppm) chemical shifts values have been correlated with Hammett substituent constants and F and R parameters using single and multi-linear regression analysis. From the results of statistical analysis, the effect of substituents on the spectral data has been studied. The antimicrobial activities of all synthesized imines have been studied using Bauer-Kirby method.
Źródło:
Annales Universitatis Mariae Curie-Skłodowska, sectio AA – Chemia; 2015, 70, 2
2083-358X
Pojawia się w:
Annales Universitatis Mariae Curie-Skłodowska, sectio AA – Chemia
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 30

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