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    Tytuł:
    Influence of gas detonation spraying parameters on the geometrical structure of Fe-Al intermetallic protective coatings
    Autorzy:
    Chrostek, Tomasz
    Bramowicz, Mirosław
    Rychlik, Kazimierz
    Wojtkowiak, Adam
    Senderowski, Cezary
    Powiązania:
    https://bibliotekanauki.pl/articles/298459.pdf
    Data publikacji:
    2019
    Wydawca:
    Uniwersytet Warmińsko-Mazurski w Olsztynie
    Tematy:
    GDS
    Detonation Gas Spraying
    Fe-Al
    intermetallic alloys
    fractal analysis
    RMS
    Opis:
    The paper presents the results of an analysis of the geometrical structure of Fe-Al intermetallic protective coatings sprayed under specified gun detonation spraying (GDS) conditions. Two barrel lengths, two powder injection positions (PIP) at the moment of spark detonation, and two numbers of GDS shots with 6.66 Hz frequency were applied as variable parameters in the GDS process. Surface profile measurements were conducted by contact profilometry with the use of the TOPO-01 system and the Mitutoyo SJ 210 profilometer. The measured parameters were used to analyze surface topography in two-dimensional (2D) and three-dimensional (3D) systems. It was assumed that roughness can be regarded as a non-stationary parameter of variance in surface amplitude which is highly dependent on the sampling rate and spraying distance. Therefore, changes in surface amplitude parameters and functional properties were analyzed across segments with a length (ln) of 1.25, 4 and 12.5 mm. The development of the geometric structure of the surface was analyzed with the RMS (Root Mean Square) fractal method, and the geometric structure of the surface stretched by several orders of magnitude was evaluated based on the correlation between roughness (Rq), segment length (ln) and fractal dimension (D). The RMS method and the calculated fractal dimension (D) supported the characterization of the geometric structure of intermetallic Fe-Al protective coatings subjected to GDS under the specified process conditions based on the roughness profiles of surface segments with a different length (ln).
    Źródło:
    Technical Sciences / University of Warmia and Mazury in Olsztyn; 2019, 22(3); 249-262
    1505-4675
    2083-4527
    Pojawia się w:
    Technical Sciences / University of Warmia and Mazury in Olsztyn
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Structural analysis of Fe-Al coatings applied by gas detonation spraying
    Autorzy:
    Chrostek, Tomasz
    Powiązania:
    https://bibliotekanauki.pl/articles/1835555.pdf
    Data publikacji:
    2020
    Wydawca:
    Uniwersytet Warmińsko-Mazurski w Olsztynie
    Tematy:
    gas detonation spraying
    GDS
    intermetallic FeAl alloys
    Opis:
    The article analyzes the formation of oxide phases in the structure of intermetallic FeAl coatings applied by gas detonation spraying (GDS). The structural properties of powder charge particles and FeAl coating formed during GDS were determined. The effect of the GDS process on phase changes in FeAl coating applied under controlled conditions was examined. The results indicate that at specific process parameters, FeAl powder particles are strongly oxidized in a hot stream of gases produced during supersonic combustion. Powder particles undergo very strong plastic deformation during the process, and the resulting multiphase coating contains oxide phases that form thin membranes along grain boundaries. The results of structural analyses and microanalyses of chemical composition (SEM/EDS) and phase composition (XRD) indicate that strongly heated FeAl particles undergo surface oxidation during GDS and are transformed into grains (splats) when they collide with a steel substrate. The produced FeAl coating has a multi-layered and multi-phase structure characteristic of the sprayed material, and it contains thin oxide layers, mainly Al2O3.
    Źródło:
    Technical Sciences / University of Warmia and Mazury in Olsztyn; 2020, nr 23(3); 221-232
    1505-4675
    2083-4527
    Pojawia się w:
    Technical Sciences / University of Warmia and Mazury in Olsztyn
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Tribological wear of Fe-Al coatings applied by gas detonation spraying
    Autorzy:
    Chrostek, Tomasz
    Powiązania:
    https://bibliotekanauki.pl/articles/2069744.pdf
    Data publikacji:
    2021
    Wydawca:
    Uniwersytet Warmińsko-Mazurski w Olsztynie
    Tematy:
    gas detonation spraying
    GDS
    coating
    Fe-Al
    intermetallic alloys
    tribology
    Opis:
    Comparative tests of gas detonation (GDS) coatings were carried out in order to investigate the influence of spraying parameters on abrasive wear under dry friction conditions. The tests were carried out using the pin-on-disc (PoD) method at room temperature. The microstructure of the coatings was analysed by X-ray diffraction (XRD) and scanning electron microscopy (SEM/EDS) methods. The results showed that with certain parameters of the GDS process, the main phase of the produced coatings is the FeAl phase with the participation of thin oxide layers, mainly Al2O3. The tribological tests proved that the coatings sprayed with the shorter barrel of the GDS gun showed higher wear resistance. The coefficient of friction was slightly lower in the case of coatings sprayed with the longer barrel of the GDS gun. During dry friction, oxide layers form on the surface, which act as a solid lubricant. The load applied to the samples during the tests causes shear stresses, thus increasing the wear of the coatings. During friction, the surface of the coatings is subjected to alternating tensile and compressive stresses, which lead to delamination and is the main wear mechanism of the coatings.
    Źródło:
    Technical Sciences / University of Warmia and Mazury in Olsztyn; 2021, 24(1); 245--256
    1505-4675
    2083-4527
    Pojawia się w:
    Technical Sciences / University of Warmia and Mazury in Olsztyn
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
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