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Tytuł:
An Electrochemical Study of the Corrosion Resistance of Niobium-Aluminum Carbonitride Coating Produced on Steels by Thermo-Reactive Diffusion Technique
Autorzy:
Abakay, E.
Durmaz, M.
Sen, S.
Sen, U.
Powiązania:
https://bibliotekanauki.pl/articles/1031643.pdf
Data publikacji:
2017-09
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.65.Lp
81.65.Kn
87.64.Ee
Opis:
Thermo-reactive diffusion/deposition technique is an alternative to physical vapor deposition and chemical vapor deposition techniques for obtaining wear and corrosion resistant coatings on steel parts. In this work, thermo-reactive diffusion/deposition technique was used to produce niobium aluminum carbonitride-based coatings on AISI M2 steel. Characterization of the coatings was done by X-ray diffraction analysis, scanning electron microscopy and energy dispersive spectroscopy. The corrosion resistance of the produced coatings was investigated by using potentiodynamic polarization in a solution of 0.5 M NaCl. Hard, compact and adherent coatings, mainly consisting of NbC and NbN phases were obtained. The corrosion behavior of the samples was investigation by potentiodynamic polarization measurements.
Źródło:
Acta Physica Polonica A; 2017, 132, 3; 682-684
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Wear Properties of TIG Surface Alloyed Steel with 50%Fe-10%W-40%B Alloy
Autorzy:
Abakay, E.
Kilinc, B.
Sen, S.
Sen, U.
Powiązania:
https://bibliotekanauki.pl/articles/1401223.pdf
Data publikacji:
2015-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.20.Vj
81.05.Bx
81.40.Pq
81.65.Lp
Opis:
In the present study, AISI 1020 plain carbon steel was surface alloyed with preplaced 50%Fe-10%W-40%B alloying powders using a tungsten-inert gas (TIG) heat source. Microstructure, hardness, and wear resistance of the surface alloyed layer were investigated. Following the surface alloying, conventional characterization techniques such as optical microscopy (OM), scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDS), and X-ray diffraction analysis (XRD) were used to study the phase and microstructural examinations of the alloyed surfaces. Hardness measurements were performed across the alloyed zones, and wear properties of the alloyed surfaces were evaluated using a ball-on-disc wear test method. Hardness values of the phases formed in the alloyed layer are changing between 620±30 $HV_{0.1}$ and 2095±254 $HV_{0.1}$. The major phases formed in the surface alloyed layer were Fe₂B, FeB and FeW₂B₂. Wear test were realized against Alumina ball under the loads of 2.5 N, 5 N and 10 N at the sliding speed of 0.1 m/s for 250 m sliding distance. The friction coefficient of the 50%Fe-10%W-40%B alloyed steel surface is changing between 0.70 and 0.79 depending on applied loads. The wear rates of the surface alloyed steel ranged from $4.01 \times 10^{-5}$ mm³/m to $4.14 \times 10^{-4}$ mm³/m.
Źródło:
Acta Physica Polonica A; 2015, 127, 4; 957-960
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Double Stage Nitriding on 34CrAlNi7-10 Nitriding Steel
Autorzy:
Altinsoy, İ.
Çelebı Efe, G.
Yener, T.
Önder, K.
Bindal, C.
Powiązania:
https://bibliotekanauki.pl/articles/1031228.pdf
Data publikacji:
2017-09
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.05.BX
81.65.LP
81.70.BT
Opis:
In this study, effect of double stage gas nitriding of 34CrAlNi7-10 steel was analyzed. Nitriding processes were carried out in two stages. in the first stage, samples were nitridied at 500°C for 10 h and then in second stage nitriding process was continued at 530 and 550°C for 20 h. During both stages, the nitrogen activity on surface was controlled by the nitriding potential, which is a thermodynamical control parameter for controlled gas nitriding process. The nitriding potential was kept constant, at value of 10, during the first stage and was varied in the range of 3.2-0.2, for both nitriding temperatures, in the second stage. The presence of nitrides, formed on the surface of test materials was determined by XRD analysis technique. The morphology of nitrided layer was studied by optical microscopy. The microhardness of the surfaces of nitrided samples in HV1 was between 955 and 1029. The measurements have shown that the thickness of the compound layer (white layer) has varied between 6.85-23.90 μm and that the growth of the white layer and microhardness gradient were strongly affected by the nitriding potential and the temperature. Diffusion depths as Nht(HV) for Vickers Hardness were determined and compared.
Źródło:
Acta Physica Polonica A; 2017, 132, 3; 663-666
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Gas Nitriding Behaviour of 34CrAlNi7 Nitriding Steel
Autorzy:
Altinsoy, I.
Onder, K.
Celebi Efe, F.
Bindal, C.
Powiązania:
https://bibliotekanauki.pl/articles/1219733.pdf
Data publikacji:
2014-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.05.Bx
81.65.Lp
Opis:
In this study, gas nitriding behavior of 34CrAlNi7-10 steel was investigated. Single stage processes were carried out at 500°C, 520C and 540C for 10, 20, 30 h, respectively. Nitrogen activity on surface was controlled by the nitriding potential $K_{N}$ which is known as thermodynamical control parameter for controlled gas nitriding process. The presence of nitrides formed on surface of test material was determined by X-ray diffraction analysis technique. The morphology of nitrided layer was studied by optical microscope. The microhardness of surface of nitrided sample in $HV_1$ was observed between 975 and 1132. Choosing the right nitriding potentials for each temperature, which give the same nitrogen concentration and activity on surface by using the Lehrer diagram, showed that all the samples had almost the same surface roughness of $R_{a}$ = 0.28-0.32 μm after gas nitriding cycles. The measurements showed that the white layer thickness varies between 4.38 μm and 28.80 μm and the growth of the layer was strongly affected by process time and temperature. Diffusion depths as Nht (HV) for each experiment were determined and compared.
Źródło:
Acta Physica Polonica A; 2014, 125, 2; 414-416
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Study of the Nickel-Tungsten and Nickel-Cobalt Coatings Plated on Ductile Iron
Autorzy:
Ayday, A.
Skulev, H.
Powiązania:
https://bibliotekanauki.pl/articles/1187269.pdf
Data publikacji:
2016-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.05.Bx
81.40.Pq
81.65.Lp
Opis:
Hard coatings such as nickel, chromium and tungsten can improve the surface properties of the substrate. The coating surfaces have been developed for increase of the wear resistance, hardness or corrosion resistance for industrial applications. Electroplating methods generally used to obtain producing these hard coatings and a novel brush plating process has the potential as an alternative of electroplating for industrial applications. In the present work, nickel-tungsten and nickel-cobalt alloys are coated on ductile iron by brush plating for surface characterization. Scanning electron microscopy and energy dispersive spectrometry were used to investigate the coating microstructures, surface morphology. The hardness of plating layers was measured. The results indicated that the nickel-tungsten coating was harder than nickel-cobalt coating. Excellent adhesion was obtained after nickel-cobalt plating. The tribological resistances were also significantly improved, as confirmed by the decrease friction coefficient and wear rate.
Źródło:
Acta Physica Polonica A; 2016, 129, 4; 455-458
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A Comparative Study on Boride Layer Morphology of Fe-4Co, Fe-4V and Fe-4W Binary Alloys
Autorzy:
Azakli, Y.
Gunduz, K.
Tarakci, M.
Gencer, Y.
Powiązania:
https://bibliotekanauki.pl/articles/1401369.pdf
Data publikacji:
2015-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.65.Lp
81.05.Je
81.05.Bx
Opis:
In this study, the pack boronizing behavior of Fe-4M alloys (at.% M=W, V, Co) along with pure iron was investigated. The boronizing process was carried out at 1100°C for 3 h. The morphology, microstructure, boride layer thickness and surface properties of the formed boride layers were characterized by XRD, SEM-EDS and profilometry. The average boride layer thicknesses were 85 μm, 130 μm, 275 μm and 280 μm for Fe-4W, Fe-4V, Fe-4Co binary alloys and pure Fe, respectively. The surface roughness was not changed with the addition of alloying element into the substrate. FeB and Fe₂B phases exist on all boronized samples, but their ratio changes owing to alloying elements in the substrate. The saw-tooth morphology has transformed to a smoother boride layer with the addition of alloying elements of W and V, though Co addition was ineffective on saw tooth morphology. In addition, a transition zone under the boride layer was observed for the boronized Fe-W and Fe-V alloys. The formation of precipitates of boride of alloying elements was evident in the boride layer and in the transition zone for borided Fe-4V and Fe-4W alloys. Co has made a solid solution with iron in boride by replacing iron in the boride lattice.
Źródło:
Acta Physica Polonica A; 2015, 127, 4; 1326-1330
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Improvement of Surface Properties of Low Carbon Steel by Nitriding Treatment
Autorzy:
Benlahreche, F.
Nouicer, E.
Powiązania:
https://bibliotekanauki.pl/articles/1030365.pdf
Data publikacji:
2017-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.65.Lp
Opis:
This work aimed to improve the physicochemical properties of a low carbon steel C15 by a nitriding treatment in a salt bath at 580°C. The micrographs of treated sample show that the nitriding treatment causes significant structural changes, it is allowed to delineate the nitriding layer. The X-ray diffraction and the Raman spectroscopy of the treated samples permitted to identify different nitrides (Fe_{2-3}N, Fe₄N) formed. The obtained hardness profile determines the nitriding depth. Potentiodynamic curves show that the corrosion current density of treated C15 is the 10 times lower than untreated specimen. The values of impedance parameters obtained after nitriding treatment indicate that the resistance values and exponent n increase, whereas the capacitance decreases. We concluded that the nitriding treatment is an effective method for improvement of the corrosion behavior and surface properties of the low alloy steel C15.
Źródło:
Acta Physica Polonica A; 2017, 131, 1; 20-23
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Phase Composition of the Surface Zone of Nitrided Cast Steels and Their Mechanical Properties
Autorzy:
Brzózka, K.
Budzynowski, T.
Górka, B.
Powiązania:
https://bibliotekanauki.pl/articles/1506569.pdf
Data publikacji:
2011-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.66.Dk
81.65.Lp
81.40.-z
76.80.+y
61.05.cp
68.37.-d
81.40.Pq
Opis:
Conversion electron Mössbauer spectroscopy and structural X-ray diffractometry have been used to study nitrides formation in the surface layer of cast steels subjected previously to low-temperature nitriding. It has been found that creation of iron-nitrogen phases strongly depends on sample composition. Nitrides: $γ^\prime-Fe_{4}N$ and $\epsilon-Fe_{2-3}N$ arise in the course of the nitriding procedure in most investigated cast steels. Moreover, considerable changes in their microstructure and tribological properties occur. The depth profile of nitrides has been derived for selected cast steel.
Źródło:
Acta Physica Polonica A; 2011, 119, 1; 28-32
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A Study on Modification of Micro-Alloy Steel Surfaces with Different Hard Materials Via Electro-Spark Deposition Method
Autorzy:
Çakir, A.
Yilmaz, M.
Ribalko, A.
Korkmaz, K.
Powiązania:
https://bibliotekanauki.pl/articles/1401438.pdf
Data publikacji:
2015-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.05.Bx
82.45.Fk
81.65.Lp
Opis:
In this study, micro alloy steel (St 35) surfaces, which were coated with different hard alloy electrode materials via Electro Spark Deposition (ESD) method, have been characterized. The electrode materials were chosen among hard alloys such as; TiCN(Ni), CrC-NiCr, WC(Co) and TiWC(Co). During the ESD experiments, the following pulse parameters in a group were used: pulse current amplitude, pulse duration, electrical charge of 100-200 A, 100 μs, 1000 mC respectively. The surface roughness, thickness of coatings, cross sectional microstructure analysis, phase analysis, micro hardness and adhesion properties of the coated samples were characterized by profilometer, SEM (EDX), XRD, micro hardness tester and scratch adhesion tester respectively.
Źródło:
Acta Physica Polonica A; 2015, 127, 4; 1410-1413
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Pack Siliconizing of Ti6Al4V Alloy
Autorzy:
Celebi Efe, G.
İpek, M.
Bindal, C.
Zeytin, S.
Powiązania:
https://bibliotekanauki.pl/articles/1031464.pdf
Data publikacji:
2017-09
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.65.Lp
81.65.-b
Opis:
In this study, it was aimed to produce titanium silicide layer on Ti6Al4V by a simple, cheap and efficient method of pack siliconizing. Siliconizing was performed in a pack containing a mixture composed of SiO₂ powder as siliconizing source, pure Al powder as a reducer for siliconizing, NH₄Cl as an activator and Al₂O₃ powder as filler, at 1000°C for 8, 10 and 12 hours in open atmospheric furnace. Optical microscope and SEM-EDS studies indicate that the morphology of silicide layers has smooth, dense and layered nature. The presence of phases, confirmed by XRD analyses, reveals that the silicide layers formed at 1000°C are composed of TiSi₂, Ti₃Si₅, TiN, TiO₂ and SiO₂ compounds. Silicide layer thickness was increased with increasing process time and ranged from 7.5 to 9.0 μm. Hardness of silicide layers, measured by Vickers indentation, is over 2100 HV.
Źródło:
Acta Physica Polonica A; 2017, 132, 3; 760-762
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Cathodic Electrolytic Plasma Hardening of Steel and Cast Iron Based Automotive Camshafts
Autorzy:
Dayanç, A.
Karaca, B.
Kumruoğlu, L.
Powiązania:
https://bibliotekanauki.pl/articles/1030309.pdf
Data publikacji:
2017-03
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.65.Lp
82.45.Hk
81.40.Pq
Opis:
Cathodic electrolytic plasma hardening is a novel thermochemical surface modification and hardening process, used to increase wear resistance and surface hardness of metallic components in a local area of interest. The heating efficiency is related with the plasma nozzle design, applied current and electrolyte. The nozzle design is also a critical factor for the hardening of complex shapes, such as gears and camshafts. In this work, lobes of camshafts, fabricated from several cast iron and steel grades were hardened by cathodic electrolytic plasma hardening in aqueous carbonate electrolyte, using a specific plasma nozzle. The camshafts were attached to CNC lathe for turning them in the horizontal axis. In order to optimise heating and to achieve the ideal flowing and wetting by the electrolyte of the lobe case, the ceramic ellipse-shaped nozzle outlet was designed. As a result of preliminary studies, external surface of lobes was heated and subsequently quenched by electrolyte. The hardness of processed surface was in the range of 50-60 HRc for the different camshafts. No distortion was observed on the surface of lobes. Hardness depth was measured to be from 0.1 mm to 5 mm for several lobes.
Źródło:
Acta Physica Polonica A; 2017, 131, 3; 374-378
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Morphology and Selected Properties of Core/Shell ZnTe-Based Nanowire Structures Containing ZnO
Autorzy:
Gas, K.
Janik, E.
Zaleszczyk, W.
Pasternak, I.
Dynowska, E.
Fronc, K.
Kolkovsky, V.
Kret, S.
Morhange, J. F.
Reszka, A.
Wiater, M.
Caliebe, W.
Karczewski, G.
Kowalski, B. J.
Szuszkiewicz, W.
Wojtowicz, T.
Powiązania:
https://bibliotekanauki.pl/articles/2047950.pdf
Data publikacji:
2011-05
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
68.37.Hk
68.37.Lp
68.65.La
81.07.Vb
Opis:
We report on an approach to fabricate ZnTe-based core/shell radial heterostructures containing ZnO, as well as on some of their physical properties. The molecular beam epitaxy grown ZnTe nanowires constituted the core of the investigated structures and the ZnO shells were obtained by thermal oxidation of ZnTe NWs. The influence of the parameters characterizing the oxidation process on selected properties of core/shell NWs were examined. Scanning electron microscopy revealed changes of the NWs morphology for various conditions of the oxidation process. X-ray diffraction, high resolution transmission electron microscopy, and Raman scattering measurements were applied to reveal the presence of ZnTe single crystal core and polycrystalline ZnO-shell of investigated structure.
Źródło:
Acta Physica Polonica A; 2011, 119, 5; 612-614
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structural Properties of Co and CoFe Electrodes Forming a Magnetic Tunnel Junction
Autorzy:
Gładczuk, L.
Pankowski, P.
Paszkowicz, W.
Dłużewski, P.
Wójcik, M.
Przysłupski, P.
Powiązania:
https://bibliotekanauki.pl/articles/2047237.pdf
Data publikacji:
2007-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.15.Hi
68.65.Ac
61.10.Nz
76.60.Lz
68.37.Lp
Opis:
The M$\text{}_{1}$/MgO/M$\text{}_{2}$ trilayer tunnel magnetoresistance systems are studied by means of X-ray diffraction, NMR, and transmission electron microscopy techniques. As M$\text{}_{1}$ and M$\text{}_{2}$ electrodes we used Co, Fe, and CoFe layers. The growth mechanism and structural quality of both electrodes and of the epitaxial MgO barrier forming the magnetic tunnel junctions are experimentally examined. It is shown that the crystallographic coherence of magnetic tunnel junctions across the MgO barrier is significantly disturbed by imperfect crystal structure of magnetic electrodes. The NMR results indicate a difference in short-range order between bottom and top electrodes.
Źródło:
Acta Physica Polonica A; 2007, 111, 1; 135-140
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Detection of Shallow Dislocations on 4H-SiC Substrate by Etching Method
Autorzy:
Ishikawa, Y.
Yao, Y.
Sato, K.
Sugawara, Y.
Danno, K.
Suzuki, H.
Bessho, T.
Kawai, Y.
Shibata, N.
Powiązania:
https://bibliotekanauki.pl/articles/1492539.pdf
Data publikacji:
2011-12
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.72.uj
81.65.Cf
68.37.Lp
Opis:
Correlation between dislocation types in epitaxial 4H-SiC and etch pit types on the 4H-SiC wafer surface were investigated by etch pit method and transmission electron microscope. Shallow dislocation on the wafer was found to form round pit without core. The shallow dislocation was estimated half-loop type in wafer and this estimation explains that step-flow growth converts half-loop dislocation into complex dislocation composed by threading dislocation and basal plane dislocation.
Źródło:
Acta Physica Polonica A; 2011, 120, 6A; A-025-A-027
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Characterization of Fe-Nb-B Base Hardfacing of Steel
Autorzy:
Kilinc, B.
Cegil, O.
Abakay, E.
Sen, U.
Sen, S.
Powiązania:
https://bibliotekanauki.pl/articles/1311693.pdf
Data publikacji:
2014-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.65.Kn
68.55.J-
81.65.Lp
Opis:
Recently hardfacing by welding has become a commonly used technique for improvement of material performance in extreme (high temperature, impact/abrasion, erosion, etc.) conditions. In the present study, three different alloy compositions of the Fe-Nb-B were used for hardfacing of the AISI 1020 steel by tungsten inert gas welding process and analyzed. The coatings were produced from a mixture of ferrous niobium, ferrous boron and iron powders in the range of - 45 μm particle size with different ratio. The coatings' thickness was set to 2-3 mm on the substrate. Microstructure, phase analysis and hardness of the manufactured hardfacing alloys were characterized. Deposition results indicate good quality thick coating and porosity free of the hardfacings. X-ray diffraction analyses showed that the alloyed layers include iron borides, FeNbB and iron phases. It was shown that surface alloyed layer has composite structure including steel matrix and well distributed boride phases.
Źródło:
Acta Physica Polonica A; 2014, 125, 2; 656-658
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 25

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