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Wyświetlanie 1-15 z 42
Tytuł:
$BiFeO_3$ Crystal Structure at Low Temperatures
Autorzy:
Palewicz, A.
Sosnowska, I.
Przeniosło, R.
Hewat, A.
Powiązania:
https://bibliotekanauki.pl/articles/1538869.pdf
Data publikacji:
2010-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.05.fm
61.66.Fn
75.50.Ee
77.84.Bw
Opis:
The crystal and magnetic structure of $BiFeO_3$ have been studied with the use of high resolution neutron diffraction between 5 K and 300 K. The atomic coordinates in $BiFeO_3$ are almost unchanged between 5 K and 300 K.
Źródło:
Acta Physica Polonica A; 2010, 117, 2; 296-301
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A System of B-C-N-O: Synthesis, Characterization and Determination of Unit Cell Parameters
Autorzy:
Gül, G.
Kurtuluş, F.
Powiązania:
https://bibliotekanauki.pl/articles/1033375.pdf
Data publikacji:
2017-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
33.20.Ea
61.66.-f
61.66.Fn
84.40.-x
Opis:
Boron-rich solids are good candidates to apply instead of diamond. Boron has a unique crystal structure and compounds of it are resistant to heat treatment. These structures have light density, high hardness, and chemically inertness. Also, boron compounds display thermal and electronic properties as a thermoelectric power at high temperatures. A boron, carbon, nitrogen, and oxygen containing compound was synthesized for the first time by classical microwave method using elemental amorphous boron, active carbon, and urea with 1:1:1 molar ratio. The compound is crystallized in monoclinic system with unit cell parameters a=12.9575 Å, b=9.3264 Å, c=9.6529 Å, β =113.277° which are calculated by POWD indexing program. The X-ray diffraction, POWD, the Fourier transform infrared, scanning electron microscopy/energy X-ray diffraction spectroscopy and thermogravimetric/different thermal analysis were achieved.
Źródło:
Acta Physica Polonica A; 2017, 131, 1; 36-38
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Analysis of Secondary Interactions and Structure-Activity-Relationship of Two Benzoic Acids
Autorzy:
Dinesh, J.
Powiązania:
https://bibliotekanauki.pl/articles/1400141.pdf
Data publikacji:
2013-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.66.Fn
Opis:
Two benzoic acids, 2-[3-(o-methylphenoxymethyl)-5-phenyl-[1,2,4]triazol-4-yl]-benzoic acid [I] and 2-[3-(m-methylphenoxymethyl)-5-phenyl-[1,2,4]triazol-4-yl]-benzoic acid [II] were synthesized and their crystal structures have been analyzed to the reliability factor of 4.2% [I] and 4.8% [II]. Different structural motifs (i.e. chains, dimmers, rings, etc.) bonded through C-H...π, ı...ı and hydrogen interactions have been analyzed. Structure-activity-predictions have been identified on the basis of structural fragments and variation in activities has been observed in both the compounds. The detailed analysis of non-covalent interactions illustrates that the shifting of methyl group from ortho-to-para increases the bioactivity-predictions of "Endothelin B receptor antagonist".
Źródło:
Acta Physica Polonica A; 2013, 123, 4; 704-708
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Analytic Equation of State and Thermodynamic Properties, for α-, β-, and γ-Si₃N₄ Based on Analytic Mean Field Approach
Autorzy:
Wang, L.
Sun, J.
Yang, W.
Tian, R.
Powiązania:
https://bibliotekanauki.pl/articles/1812044.pdf
Data publikacji:
2008-10
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
64.10.+h
65.40.-b
61.66.Fn
Opis:
The analytic mean field potential approach is applied to α-, β-, and γ-Si₃N₄. The analytic expressions for the Helmholtz free energy, internal energy, and equation of state were derived. The formalism for the case of the Morse potential is used in this work. Its six potential parameters are determined through fitting the compression experimental data of α-, β-, and γ-Si₃N₄. The calculated compression curves of α-, β-, and γ-Si₃N₄ are in good agreement with the available experimental data. This suggests that the analytic mean field potential approach is a very useful approach to study the thermodynamic properties of Si₃N₄. Furthermore, we predict the variation of the free energy and internal energy with the molar volume at several higher temperatures and calculate the temperature dependence of the molar volume, bulk modulus, thermal expansion coefficient and isochoric heat capacity at zero pressure.
Źródło:
Acta Physica Polonica A; 2008, 114, 4; 807-818
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Carbonaceous Materials Obtained from Sewage Sludge for $NO_2$ Removal under Wet Conditions at Room Temperature
Autorzy:
Pietrzak, R.
Powiązania:
https://bibliotekanauki.pl/articles/1536471.pdf
Data publikacji:
2010-09
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.66.Fn
81.05.-t
81.05.Rm
82.65.+r
89.60.-k
Opis:
The effect of the processes of carbonisation and activation on adsorbents obtained from sewage sludge and their sorption properties towards $NO_2$ were studied. Carbonaceous adsorbents were obtained by carbonisation of sewage sludge at 600°C for four different times 30, 60, 90 and 120 min followed by activation of the carbonisates by $CO_2$ at 800°C for 60 min. Adsorption of $NO_2$ was carried out in wet air. It has been shown that by appropriate thermal and chemical treatment of sludge, mesoporous adsorbents capable of $NO_2$ removal can be obtained. The sorption abilities of the carbonised and activated samples to adsorb $NO_2$ have been shown to increase with increased time of carbonisation and reach maximum for the carbonisation maintained for 90 min. Further increase in this time causes a decrease in the adsorption abilities of the samples. The sorption properties of the carbonisates have been proved to be determined by the chemical character of the surface, while those of the activated samples - by the porous structure.
Źródło:
Acta Physica Polonica A; 2010, 118, 3; 487-492
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Cobalt Additives Influence on Phase Composition and Defect Structure of Manganese Dioxide Prepared from Fluorine Containing Electrolytes
Autorzy:
Sokolsky, G.
Ivanov, S.
Ivanova, N.
Boldurev, Ye.
Kobulinskaya, O.
Demchenko, M.
Powiązania:
https://bibliotekanauki.pl/articles/1550089.pdf
Data publikacji:
2010-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.66.Fn
61.72.-y
85.40.Ry
Opis:
Manganese dioxide samples were prepared from fluorine containing electrolytes with additives of $Co^{2+}$ ions. Atomic absorption spectroscopy, thermogravimetric analysis, X-ray diffraction, scanning electron microscopy with energy dispersive X-ray analysis were the methods of the samples characterisation. Manganese dioxide at the presence of cobalt forms nanosized ramsdellite structure crystallites of mostly needle-like morphology with significant content of hydroxide groups. The main phase state in manganese dioxide samples obtained at the presence of cobalt is $γ-MnO_{2}$ with ramsdellite structure and low content of intergrowth defects. The sample doped both with lithium and cobalt can be indexed to a hollandite-type structure (tetragonal; space group I4/m) of $α-MnO_{2}$.
Źródło:
Acta Physica Polonica A; 2010, 117, 1; 86-90
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Combined X-Ray Diffraction and Absorption Study οf Crystalline Vanadium-Doped Lithium Disilicate
Autorzy:
Paszkowicz, W.
Wolska, A.
Klepka, M.
abd el All, S.
Ezz-Eldin, F.
Powiązania:
https://bibliotekanauki.pl/articles/1538928.pdf
Data publikacji:
2010-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.43.Fs
61.66.Fn
71.20.Ps
81.05.Je
Opis:
Structure of vanadium-doped lithium disilicate, $Li_{2}Si_{2}O_{5}$ (Ccc2 space group) is studied. This crystalline phase is obtained by annealing of the doped lithium disilicate glass for 4 h at 550°C. X-ray diffraction and X-ray absorption near-edge structure analysis indicate location of vanadium atoms at Si sites. the lattice parameters are found to increase isotropically with increasing vanadium content. the valency of vanadium ions is discussed on the basis of X-ray absorption near-edge structure results.
Źródło:
Acta Physica Polonica A; 2010, 117, 2; 315-318
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Crystal Structure and Magnetic Properties of Pyrrhotite-Type Compounds $Fe_{7-y}V_{y}S₈$
Autorzy:
Selezneva, N.
Ibrahim, P.
Toporova, N.
Sherokalova, E.
Baranov, N.
Powiązania:
https://bibliotekanauki.pl/articles/1397027.pdf
Data publikacji:
2018-03
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.66.Fn
75.30.Kz
75.50.Gg
Opis:
The pyrrhotite-type compounds $Fe_{7-y}V_{y}S₈$ have been synthesized and studied by means of the X-ray diffraction and magnetization measurements in order to reveal how the substitution of V for Fe affects the crystal structure, phase transition and magnetic properties. The growth of the V content in $Fe_{7-y}V_{y}S₈$ results in changes of the crystal structure and leads to a sharp decrease in the resultant magnetization, non-monotonous change of the coercive field and reduction of the magnetic ordering temperature. Unlike ferrimagnetic ordering in pyrrhotite Fe₇S₈ the compound V₇S₈ is observed to exhibit a Pauli-paramagnetic behaviour.
Źródło:
Acta Physica Polonica A; 2018, 133, 3; 450-452
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Crystal Structure of K$\text{}_{3}$Na(SeO$\text{}_{4}$)$\text{}_{2}$ at 340 K
Autorzy:
Fukami, T.
Chen, R. H.
Powiązania:
https://bibliotekanauki.pl/articles/1993089.pdf
Data publikacji:
1998-11
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.66.Fn
64.60.Fr
Opis:
The crystal structure of tripotassium sodium diselenate, K$\text{}_{3}$Na(SeO$\text{}_{4}$)$\text{}_{2}$, at 340 K is studied by single-crystal X-ray diffraction. The space group symmetry (trigonal P3̅) and structure parameters are determined. It is found that there exists the difference of the direction and the magnitude of the atomic displacement at the two phase transitions of 346 K and 334 K.
Źródło:
Acta Physica Polonica A; 1998, 94, 5-6; 795-801
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Crystalline Structure of Potassium Holmium Double Tungstate
Autorzy:
Borowiec, M.
Dyakonov, V.
Woźniak, K.
Dobrzycki, Ł.
Majchrowski, A.
Michalski, E.
Zubov, E.
Khatsko, E.
Zayarnyuk, T.
Szewczyk, A.
Gutowska, M.
Rykova, A.
Barański, M.
Domukhovski, V.
Shtyrkhunova, V.
Iwanowski, P.
Żmija, J.
Szymczak, H.
Powiązania:
https://bibliotekanauki.pl/articles/1505085.pdf
Data publikacji:
2011-06
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.66.Fn
Opis:
The potassium holmium double tungstate was prepared by using top seeded solution growth technique. Structural investigations have been performed at room temperature. The $KHo(WO_4)_2$ single crystal belongs to the monoclinic space group C2/c with the unit-cell parameters: a = 10.624(2) Å, b = 10.352(2) Å, c = 7.5434(15) Å, β = $130.78(3)^{o}$, and Z = 4. The atomic coordinates, isotropic and anisotropic displacement parameters and interionic distances for the studied structure were determined.
Źródło:
Acta Physica Polonica A; 2011, 119, 6; 835-837
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Annealing on the Crystal Structure and Microstructure of Pr Doped $ZrO_{2}-Y_{2}O_{3}$ Nanocrystals
Autorzy:
Werner-Malento, E.
Paszkowicz, W.
Fidelus, J.
Godlewski, M.
Yatsunenko, S.
Powiązania:
https://bibliotekanauki.pl/articles/1550117.pdf
Data publikacji:
2010-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.46.-w
61.66.Fn
81.40.-z
Opis:
Rare-earth doped nanocrystalline yttria-stabilized zirconia (YSZ, $ZrO_{2}-Y_{2}O_{3}$) is, recently, a subject of studies because of its luminescent properties. The luminescence may be strongly influenced by the crystal structure and microstructure of the material. In this work, the X-ray diffraction study for Pr doped YSZ nanocrystals is presented. The phase composition dependence on the $Y_{2}O_{3}$ content and on heat treatment conditions is quantitatively determined using the Rietveld method and the similarities and differences between the present data for doped samples and earlier reported data for undoped material are discussed. A formation of high symmetry phases (cubic and tetragonal) is observed for high yttria content in agreement with general tendencies observed in literature for undoped samples.
Źródło:
Acta Physica Polonica A; 2010, 117, 1; 91-97
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Electronic Constitution of Paramagnetic 3d Complexes and Positronium Conversion Rate Constants
Autorzy:
Fantola Lazzarini, A. L.
Lallarini, E.
Powiązania:
https://bibliotekanauki.pl/articles/1929063.pdf
Data publikacji:
1993-03
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
36.10.Dr
61.66.Fn
71.70.Ch
78.40.Dw
78.70.Bj
Opis:
The rate constants, k$\text{}_{SE}$, of ortho- into para-positronium spin conversion reactions promoted by paramagnetic 3d complexes may be correlated with their electronic constitution as it is described by the spin-orbit coupling and interelectronic repulsion parameters. The correlation is explained in terms of unpaired metal-electron delocalization towards the complex boundaries.
Źródło:
Acta Physica Polonica A; 1993, 83, 3; 297-302
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Experimental and Theoretical Study of Zircon and Scheelite Phases of $DyVO_4$
Autorzy:
Ermakova, O.
Paszkowicz, W.
López-Solano, J.
Muñoz, A.
Dabkowska, H.
Powiązania:
https://bibliotekanauki.pl/articles/1431671.pdf
Data publikacji:
2012-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
42.70.Hj
61.43.Bn
61.66.Fn
Opis:
Polycrystalline zircon-type dysprosium orthovanadate, $DyVO_4,$ prepared from a single crystal grown by slow cooling from $PbO//PbF_2$ flux, was studied by X-ray diffraction. Rietveld refinement provided the following unit cell size and oxygen atom coordinates: a=7.14811(4) Å; c=6.30825(4) Å, V=322.323(3) Å3, y($O^{2-}$)=0.4300(4); z($O^{2-}$)=0.2082(4) which are of a particularly high accuracy and show consistency with earlier reported values. Density functional theory calculations within the generalized gradient approximation for the exchange-correlation energy were also performed, providing values of structure parameters which differ by less than 2% from the experimental ones. The agreement between theory and experiment demonstrates the value of these calculations for understanding the structure of compounds of $RVO_4$ family. In addition, density functional theory calculations were performed for the scheelite-type $DyVO_4$; also for this polymorph the discrepancy with the only known set of lattice parameters is less than 2%. Values of oxygen atom coordinates have not been reported yet for this polymorph; here, the calculated ones are quoted.
Źródło:
Acta Physica Polonica A; 2012, 121, 4; 920-927
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Growth by LHPG, Structure and Spectroscopy of Nd$\text{}^{3+}$-Doped Ba$\text{}_{2}$NaNb$\text{}_{5}$O$\text{}_{15}$ Nonlinear Single-Crystal Fibres
Autorzy:
Foulon, G.
Ferriol, M.
Brenier, A.
Cohen-Adad, M. T.
Boulon, G.
Powiązania:
https://bibliotekanauki.pl/articles/1945469.pdf
Data publikacji:
1996-07
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.66.Fn
78.20.-e
Opis:
The renewal of the second order nonlinear crystals is very strong in laser materials optics. We are involved in the search for new systems based upon highly nonlinear niobate crystal family. Among these crystals, Ba$\text{}_{2}$NaNb$\text{}_{5}$O$\text{}_{15}$ is characterized by the highest nonlinear parameters but, unfortunately, it is difficult to grow crackless samples. The obtention of good quality and crackless Ba$\text{}_{2}$NaNb$\text{}_{5}$O$\text{}_{15}$ single crystals doped with different concentrations of Nd$\text{}_{2}$O$\text{}_{3}$ is reported. The crystals were grown as monocrystalline fibres by the laser heated pedestal growth technique. A new determination of the crystallographic structure of Ba$\text{}_{2}$NaNb$\text{}_{5}$O$\text{}_{15}$ has been performed. The structure of fibres doped with 1 at.% Nd$\text{}^{3+}$ was found orthorhombic with the new space group Pba2 instead of Cmm2. The well-known twinning of Ba$\text{}_{2}$NaNb$\text{}_{5}$O$\text{}_{15}$ due to the exchange of the a and b axes of the unit cell, which disturbs the optical properties, decreases as the Nd$\text{}^{3+}$ content of the fibre increases. Above 3%Nd$\text{}^{3+}$ ions, such monocrystalline fibres were found to be of tetragonal structure. Low temperature spectroscopy reveals that Nd$\text{}^{3+}$ ions substitute probably both Ba$\text{}^{2+}$ and Na$\text{}^{+}$ ions. The stimulated emission cross-section near 1060 nm of the $\text{}^{4}$F $\text{}_{3}\text{}_{/}\text{}_{2}$ → $\text{}^{4}$I$\text{}_{11}\text{}_{/}\text{}_{2}$ channel and its branching ratios are determined with the help of Judd-Ofelt analysis. This work shows that b-axis grown monocrystalline fibres are potentially self-doubling laser materials.
Źródło:
Acta Physica Polonica A; 1996, 90, 1; 63-72
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of Simultaneous Doping of $Li^+$ and $Fe^{3+}$ Ions in the $LiMn_2O_4$ Spinel Structure
Autorzy:
Nowicki, W.
Powiązania:
https://bibliotekanauki.pl/articles/1812247.pdf
Data publikacji:
2008-08
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.66.Fn
75.47.Lx
68.18.Jk
73.21.Cd
Opis:
A series of compounds $Li_xMn_{3-x-y}Fe_yO_4$ (x=1.0125;0≤y≤0.05) were synthesized by solid state reaction of $Li_2CO_3$ with the manganese oxide or iron-manganese oxide precursors. Investigations of the structure transformation effect of double substitution with $Li^+$ and $Fe^{3+}$ ions in $LiMn_2O_4$, in the temperature range of 10-300 K, were undertaken using high-resolution X-ray powder diffraction at the HASYLAB (DESY) synchrotron. The $Li_{1.0125}Mn_{1.9625}Fe_{0.025}O_4$ transforms from cubic (Fd3̅ m) to orthorhombic (Fddd) below 250 K, and is stable to 10 K. Whereas in the $Li_{1.0125}Mn_{1.9375}Fe_{0.05}O_4$ oxide no phase transition was observed, this spinel remains in cubic structure down to the temperature of 10 K.
Źródło:
Acta Physica Polonica A; 2008, 114, 2; 375-382
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 42

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