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Wyświetlanie 1-15 z 35
Tytuł:
Migracja danych ewidencyjnych w polskim okresie powojennym
Autorzy:
Surowiec, S.
Konieczna, J.
Surowiec, M.
Powiązania:
https://bibliotekanauki.pl/articles/129755.pdf
Data publikacji:
2001
Wydawca:
Stowarzyszenie Geodetów Polskich
Tematy:
migracja danych
zbieranie danych
ewidencja gruntów
data migration
collecting data
land registry
Źródło:
Archiwum Fotogrametrii, Kartografii i Teledetekcji; 2001, 11; 1-7-1-16
2083-2214
2391-9477
Pojawia się w:
Archiwum Fotogrametrii, Kartografii i Teledetekcji
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Evolution of the β Phase Flux Dissolution during Quasicrystal Formation
Autorzy:
Surowiec, M.
Bogdanowicz, W.
Sozańska, M.
Powiązania:
https://bibliotekanauki.pl/articles/1373540.pdf
Data publikacji:
2014-08
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.10.Fq
61.44.Br
Opis:
This study focuses mainly on the verification of a peritectic reaction during the crystallization of quasicrystals. The β and λ phases apparently provide the necessary material for crystallization of the quasicrystalline ψ phase. We present results of an experimental visualization of the evolution of the flux dissolution process of the high temperature β phase. Solidified droplets of the β phase, formed primarily by the surface tension of the liquid within a bubble or a shrinkage, after crumbling during the flux dissolution may contribute to the quasicrystal formation process according to a peritectic reaction: $β_{c}$ + λ + L → ψ, where $β_{c}$ denotes the crumbled β phase immersed in the liquid.
Źródło:
Acta Physica Polonica A; 2014, 126, 2; 594-596
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Surface Decorations of Al-Cu-Fe and Al-Cu-Co Single Quasicrystals
Autorzy:
Surowiec, M.
Bogdanowicz, W.
Krawczyk, J.
Sozańska, M.
Powiązania:
https://bibliotekanauki.pl/articles/1373609.pdf
Data publikacji:
2014-08
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.44.Br
Opis:
We studied surface decorations of faceted icosahedral Al-Cu-Fe and decagonal Al-Cu-Co single quasicrystals by the scanning electron microscopy using primary and secondary electrons. Both types of single quasicrystals exhibited decorations on their facets, however the character of the decorations was totally different. Three kinds of decorations has been developed. On icosahedral $Al_{60}Cu_{26}Fe_{14}$ quasicrystals we found three kinds of decorations: cellular, cavity type and fractal-like. There was no evident difference in chemical composition between the inner dodecahedra and the decorations of all types. Surface decorations found on decagonal $Al_{73.5}Cu_{17.5}Co_9$ quasicrystals formed a kind of irregular dendritic stars on the separate bright islands.
Źródło:
Acta Physica Polonica A; 2014, 126, 2; 597-598
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Investigation of magnetite Fe3O4 nanoparticles for magnetic hyperthermia
Autorzy:
Surowiec, Z.
Miaskowski, A.
Budzyński, M.
Powiązania:
https://bibliotekanauki.pl/articles/147118.pdf
Data publikacji:
2017
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
Mössbauer effect
superparamagnetic nanoparticles
hyperthermia
Opis:
The paper presents the investigation of magnetic nanoparticles (MNPs) dedicated to hyperthermia application. The crystal structure and size distributions have been determined by means of transmission electron microscope (TEM) and X-ray diffraction (XRD). Magnetic properties of the nanoparticles were tested by Mössbauer spectroscopy together with calorimetric experiments. The Mössbauer spectroscopic study of MNPs revealed the existence of a superparamagnetic phase. The relative contribution of the relaxing component to the total spectrum at room temperature was about 10%. The heating effect of these MNPs under alternating magnetic field was examined. The temperature increase has reached 5°C in 10 min. The preliminary temperature rise suggests that the investigated materials are applicable for hyperthermia.
Źródło:
Nukleonika; 2017, 62, 2; 183-186
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Synthesis and Properties of High Surface Area $Fe_{2}O_{3}$ Materials
Autorzy:
Surowiec, Z.
Gac, W.
Wiertel, M.
Powiązania:
https://bibliotekanauki.pl/articles/1506442.pdf
Data publikacji:
2011-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
76.80.+y
78.67.Bf
78.67.Rb
75.20.-g
Opis:
Two types of the silica materials were used for the preparation of iron oxides. The MCM-48 type silica support and wide-pore silica gel were impregnated with iron nitrates. The samples were investigated by the nitrogen adsorption/desorption method, X-ray diffraction, scanning electron microscopy, and $\text{}^{57}Fe$ Mössbauer spectroscopy. Redox properties were studied by the temperature programmed reduction method. Strongly dispersed hematite was evidenced on the supports. An application of the MCM-48 silica mesoporous materials led to the development of the oxide phases within the ordered porous structure. The detailed temperature programmed reduction studies evidenced slight differences of the redox properties of the species located within the silica templates and after their removal. Magnetic properties of iron oxides were related to the porous structure of the silica supports. The Mössbauer study of high surface area materials Fe/$SiO_{2}$ and Fe/MCM-48 type silicate templates revealed existence of ferro- and superparamagnetic phases. The relative contribution of the superparamagnetic doublet component in Mössbauer spectra is 15% and 80% for Fe/$SiO_{2}$/c and Fe/MCM-48/c samples, respectively.
Źródło:
Acta Physica Polonica A; 2011, 119, 1; 18-20
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of annealing temperature on structural and magnetic properties of MnFe2O4 nanoparticles
Autorzy:
Surowiec, Z.
Wiertel, M.
Gac, W.
Budzyński, M.
Powiązania:
https://bibliotekanauki.pl/articles/146127.pdf
Data publikacji:
2015
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
manganese ferrite
MCM-41 porous silica
Mössbauer effect
superparamagnetic nanoparticles
Opis:
Nanoparticles of manganese ferrite were obtained by the impregnation of highly ordered mesoporous MCM-41 silica support. The investigated sample contained 20% wt. Fe. The obtained nanocrystallites were strongly dispersed in silica matrix and their size was about 2 nm. The sample annealing at 500°C led to increase of particle size to about 5 nm. The Mössbauer spectroscopy investigations performed at room temperature show on occurrence of MnFe2O4 nanoparticle in superparamagnetic state for the sample annealed in all temperatures. The coexistence of superparamagnetic and ferromagnetic phase was observed at liquid nitrogen temperature. The sample annealed at 400°C and 500 °C has bigger manganese ferrite particle and better crystallized structure. One can assign them the discrete hyperfi ne magnetic field components.
Źródło:
Nukleonika; 2015, 60, 1; 137-141
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Study on the effect of atmospheric gases adsorbed in MnFe2O4/MCM-41 nanocomposite on ortho-positronium annihilation
Autorzy:
Wiertel, M.
Surowiec, Z.
Budzyński, M.
Gac, W.
Powiązania:
https://bibliotekanauki.pl/articles/146949.pdf
Data publikacji:
2015
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
manganese ferrite
MCM-41 silica
nanocomposite
o-Ps quenching
positronium annihilation
Opis:
In this paper, results of positron annihilation lifetime spectroscopy (PALS) studies of MnFe2O4/MCM- -41 nanocomposites in N2 and O2 atmosphere have been presented. In particular, the influence of manganese ferrite loading and gas filling on pick-off ortho-positronium (o-Ps) annihilation processes in the investigated samples was a point of interest. Disappearance of the longest-lived o-Ps component with τ5 present in the PAL spectrum of initial MCM-41 mesoporous material in the PAL spectra of MnFe2O4-impregnated MCM-41 measured in vacuum is a result of either a strong chemical o-Ps quenching or the Ps inhibition effects. The intensity I4 of the medium-lived component initially increases, reaching a maximum value for the sample with minimum manganese ferrite content, and then decreases monotonically. Analogous dependence for the intensity I3 of the shortest-lived component shows a maximum at higher MnFe2O4 content. Filling of open pores present in the studied nanocomposites by N2 or O2 at ambient pressure causes partial reappearance of the τ4 and τ5 components, except a sample with maximum ferrite content. The lifetimes of these components measured in O2 are shortened in comparison to that observed in N2 because of paramagnetic quenching. Anti-inhibition and anti-quenching effects of atmospheric gases observed in the MnFe2O4/MCM-41 samples are a result of neutralization of some surface active centers acting as inhibitors and weakening of pick-off annihilation mechanism, respectively.
Źródło:
Nukleonika; 2015, 60, No. 4, part 1; 783-787
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Positron Annihilation in $MnFe_2O_4$/MCM-41 Nanocomposite
Autorzy:
Wiertel, M.
Surowiec, Z.
Gac, W.
Budzyński, M.
Powiązania:
https://bibliotekanauki.pl/articles/1339369.pdf
Data publikacji:
2014-03
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
78.70.Bj
34.80.Lx
78.67.Bf
62.23.Pq
68.43.-h
75.50.Gg
78.47.D-
Opis:
In the paper results of studies of $MnFe_2O_4$/MCM-41 nanocomposites have been presented. The influence of manganese ferrite loading on changes of porous properties of mesoporous MCM-41 structure was studied by means of $N_2$ sorption/desorption method and positron annihilation lifetime spectroscopy. Disappearance of the longest-lived ortho-positronium component ($τ_5$) of pure MCM-41 mesoporous material in the positron annihilation lifetime spectra of $MnFe_2O_4$/MCM-41 measured in vacuum is a result of either o-Ps quenching or the Ps inhibition mechanism. Filling of pores in the studied nanocomposites by air at ambient pressure causes partial reappearance of the ($τ_5$) component except for the sample with maximum ferrite content. Both the ($τ_5$) component lifetime and intensity are suppressed together with increasing $MnFe_2O_4$ content by chemical quenching and inhibition of Ps formation occur. Observed anti-quenching effect of air is a result of two processes: neutralization of some surface active centres acting as inhibitors and considerably weaker paramagnetic quenching by $O_2$ molecules.
Źródło:
Acta Physica Polonica A; 2014, 125, 3; 793-797
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Influence of Reduction Process on the Iron-Molybdenum Nanoparticles in Modified MCM-41 Silica
Autorzy:
Surowiec, Z.
Wiertel, M.
Gac, W.
Budzyński, M.
Powiązania:
https://bibliotekanauki.pl/articles/1381974.pdf
Data publikacji:
2014-03
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
76.80.+y
78.67.Bf
78.67.Rb
75.20.-g
Opis:
Iron-molybdenum silica mesoporous materials were obtained by the application of direct hydrothermal method. The influence of high temperature samples reduction in the $H_2$ flow on their structural and magnetic properties was studied. Four samples with different metal contents relative to silica were investigated. The study was carried out by means of X-ray diffraction, $\text{}^{57}Fe$ Mössbauer spectroscopy and the temperature programmed reduction method. With an increasing metals content, primary pores of MCM-41 transformed into the bottle-like pores, and then into the slit-like ones. Reduction and heat treatment caused the α-Fe, $Fe_2Mo$, and Fe-Mo alloy formation. Iron and molybdenum atoms after being released into the silica matrix, where they were embedded, create clusters or crystallites. It was observed that the high temperature reduction caused partial transformation of highly dispersed Fe-Mo oxides species initially embedded in silica walls into crystallites big enough to give magnetic sextet component in the Mössbauer spectra.
Źródło:
Acta Physica Polonica A; 2014, 125, 3; 846-849
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Mössbauer and X-ray Diffraction Studies of Zr$\text{}_{1-x}$Ti$\text{}_{x}$Fe$\text{}_{2}$ Laves Phase Compounds
Autorzy:
Budzyński, M.
Sarzyński, J.
Surowiec, Z.
Wiertel, M.
Powiązania:
https://bibliotekanauki.pl/articles/2028966.pdf
Data publikacji:
2001-11
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
31.30.Gs
77.80.Bh
75.30.Kz
Opis:
Mössbauer spectroscopy of $\text{}^{57}$Fe and X-ray diffraction measurements in the Zr$\text{}_{1-x}$Ti$\text{}_{x}$Fe$\text{}_{2}$ phase have been made. Our X-ray diffraction spectra revealed that the samples have the cubic C15 crystal structure for low Ti concentration and the hexagonal C14 structure for high Ti concentration. In the range of 0.2≤x≤0.5 a mixture of both structures occurs. The investigated compounds are paramagnetic at RT for x>0.80 and magnetic for x
Źródło:
Acta Physica Polonica A; 2001, 100, 5; 717-722
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of the substitution of Ti for Y on structural properties and hyperfine interactions in Y1-xTixFe2 compounds
Autorzy:
Surowiec, Z.
Sarzyński, J.
Budzyński, M.
Wiertel, M.
Powiązania:
https://bibliotekanauki.pl/articles/971534.pdf
Data publikacji:
2004
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
hyperfine interactions
Mössbauer effect
quasibinary Laves phase
Y1 xTixFe2
Opis:
Abstract Room temperature 57Fe Mössbauer spectroscopy and X-ray diffraction measurements are reported for a series of Y1 xTixFe2 polycrystalline samples. Our research shows that except for x = 0 and x = 1, the samples are a mixture of two C15 and C14 pseudobinary Laves phases. Some Ti atoms occupy the crystallographic positions 8a characteristic of the Y atoms in the cubic C15 structure while the rest of them form the hexagonal C14 phase. However, the lattice constant dependencies on concentration x suggest the occurrence of Y atoms in the positions 4f characteristic of Ti atoms in the hexagonal C14 structure. The partial substitution of Ti atoms for Y atoms is responsible for the HMF changes in the cubic phase. Contrary to the situation taking place in the Zr1 xTixFe2 compounds, magnetic arrangement in the pseudobinary hexagonal phases is not observed at room temperature.
Źródło:
Nukleonika; 2004, 49,suppl.3; 17-21
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structural and magnetic properties of Sc(Fe1-xCux)2 compounds studied by means of Mössbauer effect and neutron diffraction
Autorzy:
Wiertel, M.
Surowiec, Z.
Budzyński, M.
Sarzyński, J.
Powiązania:
https://bibliotekanauki.pl/articles/147830.pdf
Data publikacji:
2013
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
hyperfine fields
Mössbauer effect
neutron diffraction
quasibinary Laves phase
Opis:
The subject of the investigations were quasibinary Sc(Fe1-xCux)2 Laves phases in which structural and magnetic properties depend on replacement of Fe atoms by Cu atoms. Powder X-ray diffraction and neutron diffraction measurements carried out at room temperature revealed that samples were a mixture of two phases: the quasibinary Sc(Fe1-xCux)2 compounds with cubic C15 structure and ScCu2 with tetragonal structure. 57Fe Mossbauer spectroscopy revealed that the Sc(Fe1-xCux)2 compounds are ferrimagnetic up to an actual concentration xact less than 0.30. A decreasing of mean values of hyperfine magnetic fields was observed. On the basis of analysis of the neutron diffraction spectra the mean values of Fe magnetic moments were determined, considering the component connected with the quasibinary Sc(Fe1-xCux)2 phases. These moments change from 1.45(29) �ĘB in the Sc(Fe0.92Cu0.08)2 to 1.18(32)mi B in Sc(Fe0.72Cu0.28)2 phase at 8 K. From the results of independent hyperfine magnetic field on 57Fe probes and magnetic Fe moments measurements, the hyperfine coupling constant in quasibinary ferrimagnetic Sc(Fe1.xCux)2 phases is estimated as equal to 13 T/mi B at room temperature.
Źródło:
Nukleonika; 2013, 58, 1; 173-178
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis and characterization of iron - cobalt nanoparticles embedded in mesoporous silica MCM - 41
Autorzy:
Surowiec, Z.
Wiertel, M.
Budzyński, M.
Gac, W.
Powiązania:
https://bibliotekanauki.pl/articles/147878.pdf
Data publikacji:
2013
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
cobalt
iron
MCM-41 porous silica
Mössbauer effect
superparamagnetic nanoparticles
Opis:
Fe1.xCox/MCM-41 nanocomposite materials were prepared by wet impregnation of the silica mesoporous support with aqueous solution of iron and cobalt salt mixtures. Samples, after calcination, were reduced at 573 K in order to obtain homogeneous distribution of (Fe-Co)3O4 oxide species over the MCM-41 support. Bimetallic systems were achieved through high temperature reduction, carried out at 1073 K. The temperature-programmed reduction studies indicated complex nature of the oxide species. The phase analysis of the obtained samples after low temperature reduction process carried out by means of X-ray diffraction method and using 57Fe Mossbauer spectroscopy revealed the presence of nanostructured magnetite- and maghemite-like phases. The samples with higher cobalt contents (x . 0.2) contained additionally bimetallic phases. The complete transformation of oxide phases to bimetallic Fe-Co systems occurred during reduction process in hydrogen at 1073 K. It was observed that high temperature processing caused partial transformation of highly dispersed iron oxide nanocrystallites into fayalite species embedded in the silica walls.
Źródło:
Nukleonika; 2013, 58, 1; 87-92
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Positron annihilation studies of mesoporous iron modified MCM-41 silica
Autorzy:
Wiertel, M.
Surowiec, Z.
Budzyński, M.
Gac, W.
Powiązania:
https://bibliotekanauki.pl/articles/147950.pdf
Data publikacji:
2013
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
iron
MCM-41 silica mesoporous materials
N2 sorption
positron annihilation
positron lifetime spectra
Opis:
MCM-41 silica materials modified by iron incorporation in the stage of its synthesis were investigated. The aim of the studies was determination of the nature of iron species and the influence of its content on the structural changes of materials and following the changes of their properties. For this purpose, the N2 sorption/desorption method and positron annihilation lifetime spectroscopy (PALS) were used. Disappearance of the longest-lived ortho-positronium (o-Ps) component (tau5) present in the PALS spectra of the initial MCM-41 material in the spectra of Fe-modified MCM-41 measured in vacuum is a result of a strong chemical o-Ps quenching and/or the Ps inhibition mechanism. Filling of pores by air or N2 at ambient pressure causes reappearance of the (tau5) component with lifetime shortened in comparison to that observed in vacuum for pure MCM-41 to the extent which can be explained by usual paramagnetic quenching in air. In contrary to the tendency observed for (tau5) lifetime which is practically independent of Fe content, the relevant intensity I5 monotonically decreases. This fact suggests that only inhibition of Ps formation occurs for the samples in air. Observed anti-quenching effect of air seems to be a result of competition of two processes : neutralization of surface active centres acting as inhibitors and considerably weaker paramagnetic quenching by O2 molecules.
Źródło:
Nukleonika; 2013, 58, 1; 245-250
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Sc substitution for Y on structural properties and hyperfine interactions in Y1-xScxFe2 compounds
Autorzy:
Budzyński, M.
Sarzyński, J.
Wiertel, M.
Surowiec, Z.
Powiązania:
https://bibliotekanauki.pl/articles/148816.pdf
Data publikacji:
2003
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
hyperfine interactions
Mössbauer effect
quasibinary Laves phase
Y1-xScxFe2
Opis:
Measurements of X-ray diffraction and Mössbauer effect were made on a series of Y1-xScxFe2 polycrystalline samples (x = 0.0, 0.2, 0.5, 0.7, 0.8, 1.0). It was found that the system has the cubic MgCu2 structure except for x = 1.0 where hexagonal MgZn2 structure type is stable. The lattice constant decreases with increasing x. The results of Mössbauer effect study at room temperature show that the easy axes of magnetization remain in the <111> direction for the cubic samples and <100> for the hexagonal one. Curie temperatures TC were determined from temperature dependence of the hyperfine magnetic fields. The concentration dependence of the hyperfine fields and TC show similar trends, exhibiting a maximum at x = 0.8. The magnetic and structural behaviour show that, in spite of being isoelectronic, the substitution of Y by Sc induces clear changes in the structural and magnetic properties of the compounds under investigation.
Źródło:
Nukleonika; 2003, 48,suppl.1; 79-83
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 35

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