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    Wyświetlanie 1-7 z 7
    Tytuł:
    Influence on Static Grain Growth and Sinterability of BaO Addition into 8YSZ
    Autorzy:
    Aktas, B.
    Tekeli, S.
    Salman, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/1311666.pdf
    Data publikacji:
    2014-02
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.05.Je
    81.07.Bc
    81.20.Ev
    Opis:
    In this study, 8 mol.% yttria stabilized cubic zirconia (8YSZ) powders as a matrix material and 0-15 wt% BaO powders as an additive were used in order to determine the effect of BaO addition and amount on the microstructure, sintering and static grain growth properties of the 8YSZ. For these purposes, undoped and BaO-doped 8YSZ specimens were annealed for grain growth at 1400, 1500, and 1600C for 10, 50, and 100 h, respectively. An increase of annealing temperature and holding time resulted in grain growth in all specimens. The grain size of the 8YSZ decreased with the higher level of BaO added. A limited amount of BaO dissolved in 8YSZ, and insoluble BaO reacted with $ZrO_2$ at high sintering temperature and generated the $BaZrO_3$ second sphase compound. Energy dispersive X-ray spectroscopy results showed that the $BaZrO_3$ second phase segregated at the surrounding grains and grain boundaries of the 8YSZ. These $BaZrO_3$ second phases had a pinning effect at the grain boundaries and prevented the migration of the grain boundaries of the 8YSZ. In conclusion, the grain growth results showed that the grain growth in the BaO-doped 8YSZ specimens was controlled by a solid solution drag mechanism.
    Źródło:
    Acta Physica Polonica A; 2014, 125, 2; 652-655
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The Effect of Yttrium Oxide Reinforcement on the Microstructural and Mechanical Properties of Biologically Derived Hydroxyapatite
    Autorzy:
    Bozkurt, Y.
    Gokce, H.
    Pazarlioglu, S.
    Salman, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/1401436.pdf
    Data publikacji:
    2015-04
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    87.85.jf
    Opis:
    In the present study, hydroxyapatite used as a matrix material was derived from the femur bones of Meleagris gallapova (MGHA) and then reinforced with yttriyum oxide (Y₂O₃, 5 and 10 wt.%). Then samples pelleted at 350 MPa were sintered between 900 and 1300°C. Finally, the effect of Y₂O₃ reinforcement on the microstructural and mechanical properties of MGHA was investigated. Scanning electron microscope (SEM) and X-ray diffraction (XRD) patterns were used for microstructural examinations. Density, microhardness and compressive strengths of composites were used to analyze their mechanical properties. Experimental results show that mechanical properties of composites were enhanced by increasing the temperature. The optimum results were obtained for MGHA-10% Y₂O₃ composites sintered at 1200°C.
    Źródło:
    Acta Physica Polonica A; 2015, 127, 4; 1403-1406
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Preparation and Study of Some Electrical Properties of PVA-Ni(NO3)2 Composites
    Autorzy:
    Salman, S.A.
    Bakr, N. A.
    Mahmood, M.H.
    Powiązania:
    https://bibliotekanauki.pl/articles/411873.pdf
    Data publikacji:
    2015
    Wydawca:
    Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
    Tematy:
    polyvinyl alcohol
    Casting method
    Electrical properties
    Composites
    Opis:
    The aim of this paper is to prepare and study the (D.C.) electrical conductivity of (PVA-Ni(NO₃)₂) composites at different temperatures. For that purpose, PVA films with Ni(NO₃)₂ salt additive were prepared with different concentrations 2, 4, 6, 8 and 10 wt. % and with thickness of 45μm by using casting technique. The experimental results for PVA-Ni(NO₃)₂) films show that the (D.C.) electrical conductivity increased with increasing the filler content and the temperature, and the activation energy was decreased with increasing the filler content.
    Źródło:
    International Letters of Chemistry, Physics and Astronomy; 2015, 40; 36-42
    2299-3843
    Pojawia się w:
    International Letters of Chemistry, Physics and Astronomy
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect of Co Doping on Structural and Optical Properties of NiO Thin Films Prepared By Chemical Spray Pyrolysis Method
    Autorzy:
    Bakr, N. A.
    Salman, S. A.
    Shano, A. M.
    Powiązania:
    https://bibliotekanauki.pl/articles/412102.pdf
    Data publikacji:
    2015
    Wydawca:
    Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
    Tematy:
    NiO thin films
    Co Doping
    Chemical Spray Pyrolysis
    Optical Properties
    Structural Properties
    Opis:
    In this work, nickel-cobalt oxide (Ni(1-x)CoxO) thin films, where x = 0, 4, 6 and 8 % have been successfully deposited on glass substrates by chemical spray pyrolysis (CSP) technique at substrate temperature of (400 °C) and thickness of about 300 nm. The structural and optical properties of these films have been studied using XRD, AFM, and UV-Visible spectroscopy. The XRD results showed that all films are polycrystalline in nature with cubic structure and preferred orientation along (111) plane. The crystallite size was calculated using Scherrer formula and it is found that the undoped NiO sample has maximum crystallite size (51.16 nm). AFM results showed homogenous and smooth thin films. The absorbance and transmittance spectra have been recorded in the wavelength range of (300-900) nm in order to study the optical properties. The optical energy gap for allowed direct electronic transition was calculated using Tauc equation. It is found that the band gap decreases as the Co-concentration increases and the band gap values were in the range of 3.58-3.66 eV and 3.58 eV for the prepared Nickel-Cobalt Oxide thin films. The Urbach energy increases as the Co-concentration increases and the Urbach. The optical constants including (absorption coefficient, real and imaginary parts of dielectric constant) were also calculated as a function of photon energy. Refractive index and extinction coefficient for Nickel- Cobalt Oxide thin films were estimated as a function of wavelength.
    Źródło:
    International Letters of Chemistry, Physics and Astronomy; 2015, 41; 15-30
    2299-3843
    Pojawia się w:
    International Letters of Chemistry, Physics and Astronomy
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Hydroxyapatite Lanthanum Oxide Composites
    Autorzy:
    Bozkurt, Y.
    Pazarlioglu, S.
    Gokce, H.
    Gurler, I.
    Salman, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/1401437.pdf
    Data publikacji:
    2015-04
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    87.85.jf
    Opis:
    In the present study a commercially synthetic hydroxyapatite powders (CSHAp) were doped with lanthanum oxide (5 and 10 wt.% La₂O₃). The composite powders were well homogenized and pelleted in an uniaxial mould at 350 MPa. Pelleted green bodies were sintered at five different temperatures. Finally, the effect of La₂O₃ amount on the microstructural and mechanical properties of CSHA was investigated. Microstructural properties were detected by X-ray diffraction patterns (XRD) and scanning electron microscope (SEM). Mechanical properties of the sintered samples were determined by the density, hardness and compression strength measurements. Experimental results show that the mechanical properties of HA can be improved by the doping of La₂O₃
    Źródło:
    Acta Physica Polonica A; 2015, 127, 4; 1407-1409
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Physical Characterization of Turbot (Psetta Maxima) Originated Natural Hydroxyapatite
    Autorzy:
    Inan, A.
    Komur, B.
    Ekren, N.
    Aydogdu, M.
    Gokce, H.
    Ficai, A.
    Salman, S.
    Oktar, F.
    Gunduz, O.
    Powiązania:
    https://bibliotekanauki.pl/articles/1031973.pdf
    Data publikacji:
    2017-03
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.05.-t
    81.05.Mh
    87.85.J
    Opis:
    Nowadays hydroxyapatite is one of the most popular biomaterials, which is used in various medical and dental applications areas as graft material. Bovine bone is the biggest source for natural hydroxyapatite production, but its production can lead to very dangerous disease, like mad cow disease, without high degree calcination. Hydroxyapatite produced from marine sources is much safer and easier to produce than bovine hydroxyapatite. Here in this study natural hydroxyapatite and related phases were produced from a local source turbot (Psetta maxima). Beside the main bony internal structure, there are koshers (cycloid scale) on its skin. Koshers are bulky bumps, looking like flat, small and rounded structures. Internal bones and those bulky bumps were cleaned from flesh with chemicals and calcined at 850°C for 4 hours. After calcinations, especially those bulky bumps, were formed into mesoporous structures with very light bluish color. Those mesoporous structures can be used as natural mesoporous hydroxyapatite structures for bone grafting purposes. The internal bones have also formed hydroxyapatite. Scanning electron microscope and X-ray diffraction studies were performed. I this study it is found that the bones of turbot consist of hydroxyapatite and TCP related phases. The aim of this study is to produce natural hydroxyapatite structures from turbot scale with low carbon footprint, without harming the environment and without using complex chemicals.
    Źródło:
    Acta Physica Polonica A; 2017, 131, 3; 397-399
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Hydroxyapatite Synthesis from Fish Bones: Atlantic Salmon (Salmon Salar)
    Autorzy:
    Komur, B.
    Altun, E.
    Aydogdu, M.
    Bilgiç, D.
    Gokce, H.
    Ekren, N.
    Salman, S.
    Inan, A.
    Oktar, F.
    Gunduz, O.
    Powiązania:
    https://bibliotekanauki.pl/articles/1032056.pdf
    Data publikacji:
    2017-03
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    87.85.jj
    81.05.-t
    Opis:
    Production of the bioceramics on the market is presently conducted from typical precipitation method by using reagent grade raw chemicals or through calcination of natural sources like animal bones (especially bovine bone) and fish bones. Usually fish bones were damped near or in the water sources, which can lead to serious environmental pollution. Those were regarded as a trash, even though they still bear economic value, including conjugates. In this study bones of Atlantic Salmon (Salmo salar) were used as a bioceramic material source. Bones of Atlantic Salmon were collected from Besiktas Fish Market. Those were cleaned from possible flesh with reagent grade NaOH. Cleaned parts were washed with demineralized water very neatly. Dry fish bones were calcinated at 850°C for 4 hours. The obtained hydroxyapatite material was characterized with scanning electron microscopy and X-ray diffraction methods. It was found that the bioceramic material consisted of hydroxyapatite and various related phases. Scanning electron microscopy studies have revealed nano-structured bioceramic particles. The aim of this study is to obtain nano-structured bioceramics from bones of Atlantic Salmon in an environmentally friendly and economic way.
    Źródło:
    Acta Physica Polonica A; 2017, 131, 3; 400-402
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-7 z 7

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