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    Wyświetlanie 1-7 z 7
    Tytuł:
    A Validated Reverse Phase HPLC Technique for the Determination of TATB Assay
    Autorzy:
    Bhattacharyya, S. C.
    Patil, R. S.
    Santosh, M. S. S. N. M.
    Bhattacharya, B.
    Malik, R. K.
    Mehra, A.
    Powiązania:
    https://bibliotekanauki.pl/articles/951496.pdf
    Data publikacji:
    2016
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    TATB
    HPLC
    HPTLC
    explosive
    LOQ
    LOD
    Opis:
    The main hurdle for the estimation of the purity of 1,3,5-triamino-2,4,6-trinitrobenzene (TATB) is its insolubility in most of the known organic solvents. In the conventional method, TATB is digested with steam in a modified Kjeldahl digester and the ammonia evolved is estimated quantitatively. To do away with this cumbersome method, a simple, rapid HPLC technique using a reverse phase C-18 column has been established for quantitative determination of the purity of TATB. A sharp and symmetrical peak with a retention time of 2.92 min at 355 nm is obtained for pure TATB when the flow rate is 2.0 mL/min. The linearity of the detector response has been studied with sample concentrations ranging from 10 to 50 mg/L. The method addresses two important issues of sample preparation and the precision of measurement. Unlike the previously reported HPLC techniques which mainly aimed at the detection of TATB, the present work is a validated account of a quantitative estimation of purity. Regular production batch samples have been assayed by this method and the results are compared with those obtained from the conventional analysis. The HPLC method is convenient and reliable for quality control of the product at the plant level.
    Źródło:
    Central European Journal of Energetic Materials; 2016, 13, 3; 641-657
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Multiplicative Zagreb indices and coindices of some derived graphs
    Autorzy:
    Basavanagoud, B.
    Patil, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/256021.pdf
    Data publikacji:
    2016
    Wydawca:
    Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Wydawnictwo AGH
    Tematy:
    multiplicative Zagreb indices and coindices
    derived graphs
    Opis:
    In this note, we obtain the expressions for multiplicative Zagreb indices and coindices of derived graphs such as a line graph, subdivision graph, vertex-semitotal graph, edge-semitotal graph, total graph and paraline graph.
    Źródło:
    Opuscula Mathematica; 2016, 36, 3; 287-299
    1232-9274
    2300-6919
    Pojawia się w:
    Opuscula Mathematica
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    A Note on Total Graphs
    Autorzy:
    Forouhandeh, S.F.
    Jafari Rad, N.
    Vaqari Motlagh, B.H.
    Patil, H.P.
    Pandiya Raj, R.
    Powiązania:
    https://bibliotekanauki.pl/articles/31339326.pdf
    Data publikacji:
    2015-08-01
    Wydawca:
    Uniwersytet Zielonogórski. Wydział Matematyki, Informatyki i Ekonometrii
    Tematy:
    total graph
    central graph
    middle graph
    Mycielski graph
    Opis:
    Erratum Identification and corrections of the existing mistakes in the paper On the total graph of Mycielski graphs, central graphs and their covering numbers, Discuss. Math. Graph Theory 33 (2013) 361-371.
    Źródło:
    Discussiones Mathematicae Graph Theory; 2015, 35, 3; 585-587
    2083-5892
    Pojawia się w:
    Discussiones Mathematicae Graph Theory
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Modern tillage and integrated nutrient management practices for improving soil fertility and productivity of groundnut (Arachis hypogaea L.) under rainfed farming system
    Autorzy:
    Patil, S.B.
    B.C., Balakrishna Reddy
    Chitgupekar, S.C.
    Patil, B.B.
    Powiązania:
    https://bibliotekanauki.pl/articles/11868.pdf
    Data publikacji:
    2015
    Wydawca:
    Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
    Opis:
    The field experiment was conducted with four tillage and three nutrient management practices at Agronomy field unit, University of Agricultural Sciences, GKVK, Bangalore, Karnataka, India. The results of the study indicated that, higher groundnut pod yield (1307 and 1282 kg ha-1) and haulm yield (2733 and 2889 kg ha-1) was recorded with mechanical tillage + two intercultivations and integrated application of 50% organics and 50% inorganics, respectively as compared to rest of the treatments. Further, the same treatments noticed higher availability of N, P2O5 and K2O in soil after harvest of groundnut, but greater improvement in soil organic carbon content was observed with conventional tillage + one intercultivation (0.62%) as compared to rest of the tillage practices. The maximum net returns and benefit-cost ratio was recorded with mechanical tillage + two intercultivations (Rs. 11,287 ha-1 and 1.75, respectively) and integrated application of 50% organics + 50% inorganics (Rs. 10,462 ha-1 and 1.69, respectively). However, interaction effect of tillage and nutrient management practices were not influenced significantly on soil fertility and productivity of groundnut under rainfed farming system.
    Źródło:
    International Letters of Natural Sciences; 2015, 02
    2300-9675
    Pojawia się w:
    International Letters of Natural Sciences
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Nanostructured CdO thin films for LPG and CO2 gas sensor prepared by spray pyrolisis technique
    Autorzy:
    Bari, R. H.
    Patil, S. B.
    Powiązania:
    https://bibliotekanauki.pl/articles/411726.pdf
    Data publikacji:
    2014
    Wydawca:
    Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
    Tematy:
    spray pyrolysis techniques
    LPG
    CO2 sensor
    nanostructured CdO
    gas response
    Opis:
    Nanostructured CdO thin films were deposited by spray pyrolysis techniques at different spray deposition time on glass substrates. Nanostructured CdO thin films was prepared using 0.05 M of cadmium acetate dehydrate (CH3COO) 2Cd•2H2O) was dissolved in the deionised water. These thin films were annealing in air at temperatures 500 °C for 60 min. The thickness of the films, crystallite and grain size were observed to increase with the increase in spray deposition time. As prepared thin films were characterized using XRD, FE-SEM and EDAX. The XRD analysis shows that CdO films were cubic structured. The electrical and gas sensing properties of these films were investigated. Prepared nanostructure CdO thin films show LPG (S = 1600) and CO2 (S = 435) gas response at different operating temperature. Gas response, selectivity, response and recovery time of the sensor were measured and presented.
    Źródło:
    International Letters of Chemistry, Physics and Astronomy; 2014, 18; 31-46
    2299-3843
    Pojawia się w:
    International Letters of Chemistry, Physics and Astronomy
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Studies on spray pyrolised nanostructured SnO2 thin films for H2 gas sensing application
    Autorzy:
    Bari, R. H.
    Patil, S. B.
    Powiązania:
    https://bibliotekanauki.pl/articles/411918.pdf
    Data publikacji:
    2014
    Wydawca:
    Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
    Tematy:
    Spray Pyrolysis
    Nanostructured SnO2
    thin films
    H2 gas sensor
    Microstrain
    Electrical conductivity
    Opis:
    The objective of this work is to study the influence of pyrolysis temperature on structural, surface morphology and gas sensing properties of the nanostructured SnO2 thin films prepared by spray pyrolysis technique. These films were characterized for the structural, morphological and elemental composition carried by means of X-ray diffraction (XRD), scanning electron microscopy (SEM) and energy dispersive spectrophotometer (EDAX). The information of crystallite size, dislocation density and microstrain is obtained from the full width-at half- maximum (FWHM) of the diffraction peaks. Effect of sprayed deposition temperature on H2 gas sensing performance and electrical properties were studied using static gas sensing system. The sensor (Tpyr. = 350 °C) showed high gas response (S = 1200 at 350 °C) on exposure of 500 ppm of H2 and high selectivity against other gases The results are discussed and interpreted.
    Źródło:
    International Letters of Chemistry, Physics and Astronomy; 2014, 17, 2; 125-141
    2299-3843
    Pojawia się w:
    International Letters of Chemistry, Physics and Astronomy
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Removal of lindane from wastewater using liquid-liquid extraction process
    Autorzy:
    Patil, I. D.
    Patil, Y. S.
    Pangarkar, B. L.
    Powiązania:
    https://bibliotekanauki.pl/articles/778239.pdf
    Data publikacji:
    2013
    Wydawca:
    Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
    Tematy:
    lindane
    extraction
    ternary diagram
    wastewater treatment
    Opis:
    Pesticide pollution is a serious problem being faced. Harmful levels of pesticides are found in the water which is used for daily purposes. In the event of such a scenario, this paper presents a working solution for bringing down the Pesticide levels in the water to safe levels by using the method of liquid-liquid extraction. The experimental liquid-liquid equilibrium data on pesticide-water-solvent ternary mixtures at a temperature of 288.15 K are presented here. The pesticide used here is a chlorinated hydrocarbon called lindane found in the water (underground, land), beverages and foods. The solvents used are Petro-ether-Chloroform (1:1), Ethylene di chloride and n-hexane. The equilibrium generation diagram, triangular diagram, tie lines and bimodal curves as well as the distribution coefficient have been determined and reported. The petro-ether-chloroform was found to be the right solvent for the separation of lindane from wastewater because of high selectivity (25.36) and distribution coefficient (4). The extraction process is simulated into ‘C’ language.
    Źródło:
    Polish Journal of Chemical Technology; 2013, 15, 3; 81-84
    1509-8117
    1899-4741
    Pojawia się w:
    Polish Journal of Chemical Technology
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-7 z 7

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