Autor: Oluropo Adeosun, Samson - Katalog OPAC zbiorów

Skocz do pozycji: 1.

Tytuł:: A Morphological Characterization of High Yield Chitin from Periwinkle Shells
Autorzy:: Odili, Cletus Chiosa
Philips Gbenebor, Oluwashina
Adekola Haffner, Henry
Oluropo Adeosun, Samson
Powiązania:: https://bibliotekanauki.pl/articles/2056029.pdf
Data publikacji:: 2021
Wydawca:: Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Wydawnictwo AGH
Tematy:: periwinkle
polysaccharide
demineralization
deproteinization
morphology
polisacharyd
demineralizacja
deproteinizacja
morfologia
Opis:: Research on obtaining chitin from periwinkle shell is scarce due to the very low yield of chitin from this kind of shell. This study reports a method of processing periwinkle shells to obtain high yield, bio-medically suitable chitin. The experiment was designed using IM and 2M concentrations of HCl for demineralization and a 1M NaOH concentration for deproteinization. FTIR, SEM, XRD and DTA analytical tools were used to characterize the extracted chitin. The FTIR spectral, XRD patterns and SEM analysis, revealed the complete removal of calcium carbonate by the acid concentrations used. The particle-like form of periwinkle shell was transformed to sheet-like fiber and globular-like fiber of α-chitin by increasing the concentration of HCl from1M to 2M respectively. The crystal size increased from 11.2Å (1M HCl) to 13.4Å (2M HCl). The yield of chitin from periwinkle shell also increased from 52% to 71% using 1M and 2M HCl respectively. Thus, acid concentrations can be used to alter the structure of chitin with different mechanical properties.
Źródło:: Journal of Casting & Materials Engineering; 2021, 5, 4; 61--65
2543-9901
Pojawia się w:: Journal of Casting & Materials Engineering
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 2.

Tytuł:: Structural and Morphological Evaluations of Natural Hydroxyapatite from Calcined Animal Bones for Biomedical Applications
Autorzy:: Ojo, Olusola Emmanuel
Sekunowo, Olatunde Israel
Ilomuanya, Margaret Okonawan
Gbenebor, Oluwashina Philips
Adeosun, Samson Oluropo
Powiązania:: https://bibliotekanauki.pl/articles/2056038.pdf
Data publikacji:: 2022
Wydawca:: Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Wydawnictwo AGH
Tematy:: hydroxyapatite
calcination
animal bones
crystallinity
porosity
Opis:: Several biomedical materials have been employed as drug delivery systems, but natural Hydroxyapatite (HAP) has been proven to be exceptionally better than other materials owing to its excellent bioactivity and biocompatibility properties. In this study, natural HAP was obtained from bovine and caprine bones and comparatively analysed for biomedical applications. The bones were hydrothermally treated, calcined in the temperature range of 700–1100°C, held for 2 hours in an electric furnace to remove the organic contents; milled, sifted with 150 μm mesh sieve and then characterized. It was revealed by Energy Dispersive X-Ray Spectroscopy (EDS) that the bovine and caprine bone samples calcined at 1000°C had calcium/phosphorus ratio (Ca/P) of 1.66 closest to the standard of 1.67. The bovine HAP showed the best crystallinity (86.23%) at 1000°C while caprine HAP had its highest (87.25%) at 1100°C. Fourier Transform Infrared Spectroscopy (FTIR) results revealed that the calcination temperature must be greater than 700°C to isolate high quality HAP. The Scanning Electron Microscopy (SEM) showed that the samples calcined at 800°C had the largest average particle size (85.34 μm) while porosity increases with calcination temperature in both samples. The HAP obtained at a calcination temperature of 1000°C proved to have the best quality for biomedical applications.
Źródło:: Journal of Casting & Materials Engineering; 2022, 6, 1; 14--21
2543-9901
Pojawia się w:: Journal of Casting & Materials Engineering
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 3.

Tytuł:: Strength, Water Absorption, Thermal and Antimicrobial Properties of a Biopolymer Composite Wound Dressing
Autorzy:: Odili, Cletus Chiosa
Sekunowo, Olatunde Israel
Ilomuanya, Margaret Okonawan
Gbenebor, Oluwashina Philips
Adeosun, Samson Oluropo
Powiązania:: https://bibliotekanauki.pl/articles/2056037.pdf
Data publikacji:: 2022
Wydawca:: Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Wydawnictwo AGH
Tematy:: chitin
chitosan
hydrophilicity
polylactide acid
skin
wound
staphylococcus-Auerus
Opis:: Conventional wound material allows bacterial invasions, trauma and discomfort associated with the changing of the dressing material, and the accumulation of body fluid for wounds with high exudate. However, there is a shift from conventional wound dressing materials to polymeric nanofibers due to their high surface area to volume ratio, high porosity, good pore size distribution, which allows for cell adhesion and proliferation. There is an urgent need to synthesis a biodegradable composite that is resistant to bacterial infection. In this study, an electrospun polylactide (PLA) composite suitable for wound dressing, with enhanced antimicrobial and mechanical properties, was produced. The neat PLA, PLA/CH (10 wt.%), PLA/CH (5 wt.%), PLA/CHS (10 wt.%), PLA/CHS (5 wt.%), PLA/CH (2.5 wt.%) /CHS (2.5 wt.%) and PLA/CH (5 wt.%)/CHS (5 wt.%), were electrospun using 0.14 g/ml solution. Results show that crystallinity (67.6%) of neat PLA declined by 3.8% on the addition of 2.5 wt.% chitin/chitosan with improved hydrophilicity of the composite. The tensile strength of neat PLA (0.3 MPa) increased (0.6 MPa) with 2.5 wt.% chitin/chitosan addition. The slight increase in the glass transition temperature from 75°C for neat PLA to 78°C of the composite fibre, showed improved ductility. The fibres showed little beads, hence suitable for wound dressing. The electrospun mats have good water absorption capacity and strong resistance against Staphylococcus aureus. Good performance was attained at 5 wt.% of chitin, chitosan and hybrid reinforcements. Therefore, a PLA/chitin/chitosan composite is recommended as a wound dressing material.
Źródło:: Journal of Casting & Materials Engineering; 2022, 6, 1; 22--32
2543-9901
Pojawia się w:: Journal of Casting & Materials Engineering
Dostawca treści:: Biblioteka Nauki

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