- Tytuł:
- Carbonization of solid uranyl-ascorbate gel as an indirect step of uranium carbide synthesis
- Autorzy:
-
Brykala, M.
Rogowski, M.
Olczak, T. - Powiązania:
- https://bibliotekanauki.pl/articles/147109.pdf
- Data publikacji:
- 2015
- Wydawca:
- Instytut Chemii i Techniki Jądrowej
- Tematy:
-
carbonization
complex sol-gel process (CSGP)
uranium carbide
uranyl-ascorbate complex - Opis:
- The studies of the synthesis of uranium carbide from uranyl-ascorbate gels using the complex sol-gel process (CSGP) have been carried out. The synthesis of uranyl-ascorbate mixture as liquid sol from uranium trioxide and ascorbic acid and solid gel by extraction of water from sol were carefully examined. Ascorbic acid was used as a complexing agent in complex sol-gel process and as a carbon source. The crucial step to obtain final uranium carbides from the aforementioned substrates is the carbonization process. The thermal behavior of ascorbic acid and uranyl-ascorbate gels in a nitrogen atmosphere in the temperature range of 25–900°C were investigated using TG-DTG. Furthermore, the products of the carbonization of uranyl-ascorbate gels in nitrogen, argon and vacuum atmosphere were identifi ed by X-ray diffraction. TG-DTG was used also as a method for determining of carbon residues in the samples.
- Źródło:
-
Nukleonika; 2015, 60, No. 4, part 2; 921-925
0029-5922
1508-5791 - Pojawia się w:
- Nukleonika
- Dostawca treści:
- Biblioteka Nauki
Artykuł