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    Wyświetlanie 1-3 z 3
    Tytuł:
    Direct Energy Deposition of Mo Powder Prepared by Electrode Induction Melting Gas Atomization
    Autorzy:
    Roh, Goo-Won
    Park, Eun-Soo
    Moon, Jaeyun
    Lee, Hojun
    Byun, Jongmin
    Powiązania:
    https://bibliotekanauki.pl/articles/2049331.pdf
    Data publikacji:
    2021
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    molybdenum powder
    electrode induction melting gas atomization
    direct energy deposition
    porosity
    hardness
    Opis:
    Molybdenum (Mo) is used to form a barrier layer for metal wiring in displays or semiconductor devices. Recently, researches have been continuously attempted to fabricate Mo sputtering targets through additive manufacturing. In this study, spherical Mo powders with an average particle size of about 37 um were manufactured by electrode induction melting gas atomization. Subsequently, Mo layer with a thickness of 0.25 mm was formed by direct energy deposition in which the scan speed was set as a variable. According to the change of the scan speed, pores or cracks were found in the Mo deposition layer. Mo layer deposited with scan speed of 600 mm/min has the hardness value of 324 Hv with a porosity of approximately 2%. We demonstrated that Mo layers with higher relative density and hardness can be formed with less effort through direct energy deposition compared to the conventional powder metallurgy.
    Źródło:
    Archives of Metallurgy and Materials; 2021, 66, 3; 795-798
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Morphology Control of One-Dimensional Gallium Nitride Nanostructures by Modulating the Crystallinity of Sacrificial Gallium Oxide Templates
    Autorzy:
    Ko, Yun Taek
    Park, Mijeong
    Park, Jingyeong
    Moon, Jaeyun
    Choa, Yong-Ho
    Lee, Young-In
    Powiązania:
    https://bibliotekanauki.pl/articles/2049246.pdf
    Data publikacji:
    2021
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    GaN
    nanofiber
    nanotube
    electrospinning
    chemical transformation
    Opis:
    In this study, we demonstrated a method of controllably synthesizing one-dimensional nanostructures having a dense or a hollow structure using fibrous sacrificial templates with tunable crystallinity. The fibrous Ga2O3 templates were prepared by calcining the polymer/gallium precursor nanofiber synthesized by an electrospinning process, and their crystallinity was varied by controlling the calcination temperature from 500°C to 900°C. GaN nanostructures were transformed by nitriding the Ga2O3 nanofibers using NH3 gas. All of the transformed GaN nanostructures maintained a one-dimensional structure well and exhibited a diameter of about 50 nm, but their morphology was clearly distinguished according to the crystallinity of the templates. When the templates having a relatively low crystallinity were used, the transformed GaN showed a hollow nanostructure, and as the crystallinity increased, GaN was converted into a denser nanostructure. This morphological difference can be explained as being caused by the difference in the diffusion rate of Ga depending on the crystallinity of Ga2O3 during the conversion from Ga2O3 to GaN. It is expected that this technique will make possible the tubular nanostructure synthesis of nitride functional nanomaterials.
    Źródło:
    Archives of Metallurgy and Materials; 2021, 66, 3; 709-712
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Simple synthesis of Black TiO2 Nanofibers Via Calcination in Inert Atmosphere
    Autorzy:
    Ji, Myeongjun
    Kim, Eung Ryong
    Park, Mi-Jeong
    Jeon, Hee Yeon
    Moon, Jaeyun
    Byun, Jongmin
    Lee, Young-In
    Powiązania:
    https://bibliotekanauki.pl/articles/2174573.pdf
    Data publikacji:
    2022
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    black TiO2
    nanofibers
    electrospinning
    calcination
    atmosphere
    Opis:
    Black TiO2 nanofibers have recently emerged as a promising material that has both advantages of black metal oxide and one-dimensional nanostructure. However, current reduction-based synthesis approaches are not compatible with practical applications because these processes require high process costs, complicated processes, and sophisticated control. Therefore, it is still necessary to develop a simple and facile method that can easily introduce atomic defects during the synthesis process. This work suggests an electrospinning process with an antioxidant and subsequent calcination process for the facile synthesis of black TiO2 nanofibers. The synthesized black TiO2 nanofiber has an average diameter of 50.3 nm and a rutile structure. Moreover, this nanofiber represented a noticeable black color and a bandgap of 2.67 eV, clearly demonstrating the bandgap narrowing by the introduced atomic defects.
    Źródło:
    Archives of Metallurgy and Materials; 2022, 67, 4; 1481--1486
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-3 z 3

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