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Tytuł:
Development and validation of reversed phase gradient HPLC method for the simultaneous estimation of olmesartan medoxomil and chlorthalidone in dosage forms
Autorzy:
Manikandan, S.
Thirunarayanan, G.
Powiązania:
https://bibliotekanauki.pl/articles/1194011.pdf
Data publikacji:
2015
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Accuracy
Acetonitrile
Buffer pH 3.0
Chlorthalidone
Forced degradation
Linearity
Olmesartan medoxomil
Precision
RP-gradient HPLC
Robustness
Simultaneous estimation
Opis:
The main objective of the proposed study is to develop and validate a new stability indicating reverse phase HPLC gradient method for the simultaneous estimation of olmesartan medoxomil and chlorthalidone in combined dosage form. The method is optimized by using zorbax phenyl column (250 x 4.6 mm, 5 μ). For pump-A, ammonium dihydrogen orthophosphate and pump-B, acetonitrile: are used. Phosphate buffer pH was adjusted with orthophosphoric acid to 3.0. Water and acetonitrile (45:50) are used as diluent. The flow rate is 1.5 ml/min and the elutant is monitored at 220 nm with uv detector. The retention time of olmesatran medoxomil and chlorthalidone are 10.70 ±0.1 mins and 4.8 ± 0.1 mins respectively. Precision shows that % Relative standard deviation of olmesartan medoxomil and chlorthalidone is about 0.23 and 0.56 respectively. The percentage recoveries of both the drugs olmesartan medoxomil and chlorthalidone from the dosage formulation are 100.3% and 99.20% respectively. Linearity of olmesartan medoxomil and chlorthalidone is in the range of 10.0 to 60.0 μg/ml and 6.25 μg/ml respectively. Calibration curve shows good linearity and range. The correlation coefficient of olmesartan medoxomil and chlorthalidone is 0.999. And the results obtained for Robustness and Ruggedness are well within the acceptance criteria. The proposed method is found to be simple, rapid, accurate and precise. It is found to be economical and suitable for simultaneous determination of olmesartan medoxomil and chlorthalidone in pharmaceutical dosage form.
Źródło:
World Scientific News; 2015, 9; 101-123
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Development and validation of dissolution method for levocetirizine dihydrochloride by isocratic reverse phase HPLC
Autorzy:
Thirunarayanan, G.
Manikandan, S.
Powiązania:
https://bibliotekanauki.pl/articles/1194036.pdf
Data publikacji:
2015
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Accuracy
Buffer
Levocetirizine hydrochloride
Precision
Reverse Phase HPLC
Ruggedness
pH
Opis:
Levocetirizine hydrochloride is an orally active, non-sedative antihistamine used in the symptomatic relief of seasonal and perennial allergic rhinitis. The main objective of the proposed study is to develop and validate a dissolution method of Levocetirizine hydrochloride dosage form by reverse phase HPLC isocratic method. The method is optimized by various filteration methods such as centrifuge and whatman 42. The filteration methods are evaluated by reverse phase isocratic HPLC method using column- Phenomenex Luna - C 18 (250 mm x 4.6 mm; 5 µ), mobile phase – mixture of buffer and acetonitrile (580:420), adjusted pH to 6.0 with 10 % sodium hydroxide. buffer - 4.08 g Potassium dihydrogen orthophosphate in 600 mL of water. The flow rate is 1.0 mL/min and the elutant is monitored at 230 nm with UV detector. The retention time of levocetirizine hydrochloride is 5.5. Precision shows that % relative standard deviation is about 1.1%. The percentage recovery of the levocetirizine from the dosage formulation is 99.6%. The results obtained for robustness and ruggedness of levocetirizine hydrochloride are well within the acceptance criteria. The proposed method is found to be simple, rapid, accurate and precise. The proposed methods are validated as per ICH guidelines and successfully applied for the determination of Levocetirizine tablet.
Źródło:
World Scientific News; 2015, 11; 1-17
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis, spectral (FT-IR, 1H and 13C NMR) and antimicrobial studies some of (E)-2-(2-((aryl)(phenyl)methylene)hydrazinyl)benzo[d] thiazole
Autorzy:
Manikandan, S.
Thirunarayanan, G.
Powiązania:
https://bibliotekanauki.pl/articles/1177421.pdf
Data publikacji:
2018
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Aryl hydrazone
IR and NMR spectra
antibacterial and antifungal activities
Opis:
A series of (E)-2-(2-((aryl)(phenyl)methylene)hydrazinyl)benzo[d] thiazole compounds by condensation of substituted benzophenone with 2-hydrazinobenzothizol in the presence acetic acid. The synthesized compounds 1-6 were characterized by elemental, FT-IR, 1H and 13C NMR spectral data. From the IR and NMR spectra, the characteristic frequencies were assigned and the data used for confirmation of the formation hydrazones 1-6. All compounds were screened for their preliminary antibacterial and antifungal activities. The methoxy substituted compound 6 shows good antibacterial activity against their bacterial strains within the agreed mm of zone of inhibition. The methyl (5) and methoxy (6) substituted hydrazones show good antifungal activities against their fungal strains.
Źródło:
World Scientific News; 2018, 103; 1-18
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
FT-IR, 1H and 13C NMR QSAR and molecular docking study on some (E)-2-(2-((aryl)(phenyl)methylene) hydrazinyl)benzo[d]thiazoles
Autorzy:
Muthuvel, I.
Thirunarayanan, G.
Manikandan, S.
Powiązania:
https://bibliotekanauki.pl/articles/1066169.pdf
Data publikacji:
2019
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
(E)-2-(2-((aryl)(phenyl)methylene)hydrazinyl)benzo[d]thiazoles
Docking analysis
Hammett equation
IR spectra
NMR spectra
QSAR study
Schiff’s bases
Opis:
About six (E)-2-(2-((aryl)(phenyl)methylene)hydrazinyl)benzo[d]thiazoles have been synthesized and characterized by literature data. The infra-red stretching frequencies (ν, cm-1) of NH, CN, C=C and the NMR chemical shifts (δ, ppm) of NH, C=N and ipso carbons were assigned. These spectroscopic data were correlated for studying the QSAR employing Hammett equation with various Hammett substituent constants, Swain-Lupton’s F and R parameters using single and multi-regression analysis. From the results of regression analysis, the QSAR will be predicted by means of effects of substituents on the spectroscopic data of the functional group frequencies. The molecular docking character was evaluated by Schrodinger program, probing analogue docking in Topoisomerase enzymes. The crystallographic enzyme ligand complex (PDB entry 3TTZ) was obtained from the RCSB Protein Data Bank.
Źródło:
World Scientific News; 2019, 131; 54-74
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Ethnobotanical survey of medicinal plants in kalrayan hills, eastern Ghats, Tamil Nadu
Autorzy:
Manikandan, S.
Alagu Lakshmanan, G. M.
Powiązania:
https://bibliotekanauki.pl/articles/970636.pdf
Data publikacji:
2014
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
ethnobotany
medicinal plant
botanical name
ethnomedicine
ethnoveterinary medicine
Kalrayan hills
Tamil Nadu
India
Opis:
An ethnomedicinal survey among the kalrayan hills, Salem district, Tamil Nadu during September 2010 to February 2012. A total of 64 species of ethnomedicinal plants belonging to 34 families and 10 species of ethno veterinary plants belonging to 10 families were reported with the help of standard flora among local healers, village head man and elderly tribal persons. The medicinal plants used by village people, tribal and are arranged alphabetically followed by botanical name, family name, local and English name and their therapeutic uses.
Źródło:
International Letters of Natural Sciences; 2014, 12, 2
2300-9675
Pojawia się w:
International Letters of Natural Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Morphological variation assessment in different accessions of Plectranthus forskohlii (Willd) Briq. from South India
Autorzy:
Lakshmanan, G.M.A.
Manikandan, S.
Powiązania:
https://bibliotekanauki.pl/articles/11817.pdf
Data publikacji:
2015
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Opis:
The genus Plectranthus belongs to the family Lamiaceae is found in wild and cultivated condition. In the present work, the cultivars of Plectranthus forskohlii have been collected from Tamil Nadu, Kerala and Karnataka at different places. The accessions collected from Karnataka showed high tuber size, length and volume when compared to accessions collected from Tamil Nadu and Kerala. The most significant observation was made in Karnataka and Tamil Nadu cultivar accessions which were grown in the same soil in field condition have much branched root tuber with significant fresh weight as compared with accessions from Kerala. The Kerala accessions were observed with less diffused root tuber with low fresh weight. On the basis of the present research, it was concluded that the phenotypic variations present in leaf, stem and root characters might be due to some genetic heritable variation which may exist in the accessions collected from different locality, and this require further study with respect to their genotypic nature of Plectranthus forskohlii.
Źródło:
International Letters of Natural Sciences; 2015, 01
2300-9675
Pojawia się w:
International Letters of Natural Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Review on pharmacological effects of Plectranthus forskohlii (Willd) briq
Autorzy:
Lakshmanan, G.M.A.
Manikandan, S.
Powiązania:
https://bibliotekanauki.pl/articles/11222.pdf
Data publikacji:
2015
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Opis:
Plectranthus forskohlii (Willd). Briq. (Syn: Coleus forskohlii) is an important indigenous medicinal plant in India. It has been used in traditional Ayurveda medicine for curing various disorders and this is the only source of the diterpenoid forskolin. Forskolin is used for the treatment of eczema, asthma, psoriasis, cardiovascular disorders and hypertension, where decreased intracellular cAMP level is believed to be a major factor in the development of the disease process. A comprehensive account of the morphology, medicinal uses, phytochemistry, pharmacological activities, analytical methods and biotechnological approaches for forskolin production reported are included in view of the many recent findings of importance on this plant.
Źródło:
International Letters of Natural Sciences; 2015, 01
2300-9675
Pojawia się w:
International Letters of Natural Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
C7-Decompositions of the Tensor Product of Complete Graphs
Autorzy:
Manikandan, R.S.
Paulraja, P.
Powiązania:
https://bibliotekanauki.pl/articles/31341796.pdf
Data publikacji:
2017-08-01
Wydawca:
Uniwersytet Zielonogórski. Wydział Matematyki, Informatyki i Ekonometrii
Tematy:
cycle decomposition
tensor product
Opis:
In this paper we consider a decomposition of Km × Kn, where × denotes the tensor product of graphs, into cycles of length seven. We prove that for m, n ≥ 3, cycles of length seven decompose the graph Km × Kn if and only if (1) either m or n is odd and (2) 14 | m(m − 1)n(n − 1). The results of this paper together with the results of [Cp-Decompositions of some regular graphs, Discrete Math. 306 (2006) 429–451] and [C5-Decompositions of the tensor product of complete graphs, Australasian J. Combinatorics 37 (2007) 285–293], give necessary and sufficient conditions for the existence of a p-cycle decomposition, where p ≥ 5 is a prime number, of the graph Km × Kn.
Źródło:
Discussiones Mathematicae Graph Theory; 2017, 37, 3; 523-535
2083-5892
Pojawia się w:
Discussiones Mathematicae Graph Theory
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis and Hammett spectral QSAR analysis of some (E)-1-(4-methoxyphenyl)-3-phenylprop-2-en-1-ones
Autorzy:
Vijayakumar, S.
Manikandan, V.
Arulkumaran, R.
Christuraj, P.
Sundararajan, R.
Thirunarayanan, G.
Powiązania:
https://bibliotekanauki.pl/articles/1076503.pdf
Data publikacji:
2019
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
(E)-1-(4-methoxyphenyl)-3-phenylprop-2-en-1-ones
IR
NMR spectra
QSAR study
UV
regression analysis
Opis:
About nine substituted (E)-1-(4-methoxyphenyl)-3-phenylprop-2-en-1-ones have been synthesized by solvent-free method. These enones were analyzed by spectral techniques. The characteristic spectral frequencies were correlated through Hammett equation with Hammett substituent constants, F and R parameters using single and multi-regression analysis method. From the statistical analysis results, the quantitative structure activity relationships have been discussed by means of effects of substituents on the spectral frequencies.
Źródło:
World Scientific News; 2019, 115; 52-67
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
IR and 1H NMR spectral studies of some 2-Amino-4-isopropyl-6-methoxy-N-phenylpyrimidine-5-carboxamides: Assessment of substituent effects
Autorzy:
Arulkumaran, R.
Sundararajan, R.
Manikandan, V.
Sathiyendiran, V.
Pazhamalai, S.
Thirunarayanan, G.
Powiązania:
https://bibliotekanauki.pl/articles/412343.pdf
Data publikacji:
2014
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
2-Amino-4-isopropyl-6-methoxy-N-phenylpyrimidine-5-carboxamides
IR spectra
NMR spectra
substituent effects
Opis:
A series of 2-Amino-4-isopropyl-6-methoxy-N-phenylpyrimidine-5-carboxamide compounds have been synthesized from various substituted dithioacetal and guanidine. The purities of these compounds were checked by their physical constants, UV, IR, NMR and MASS spectral data. The IR and 1HNMR spectral data of these compounds have been correlated with Hammett sigma constants, F and R parameters using single and multi-linear regression analysis. From the results of statistical analysis, the effects of substituents on the spectral group frequencies have been discussed.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2014, 19, 1; 15-25
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis and LFER study of some substituted hydrazones
Autorzy:
Vijayakumar, R.
Rajarajan, M.
Senbagam, R.
Balaji, S.
Manikandan, V.
Vanangamudi, G.
Thirunarayanan, G.
Powiązania:
https://bibliotekanauki.pl/articles/1182767.pdf
Data publikacji:
2017
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Hydrazones and substituent effect
LFER study
Synthesis
Opis:
A series containing ten substituted hydrazones have been synthesized by condensation between semicarbazide and various substituted benzaldehydes. The hydrazones were confirmed by their physical constants and UV, IR, 1H NMR and 13C NMR spectral data. This UV, IR, 1H NMR and 13C NMR spectral data have been used for LFER studied with Hammett constants and Swain-Lupton’s parameters.
Źródło:
World Scientific News; 2017, 66; 263-280
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis, and spectral Hammett correlation analysis of some (E)-1-(5-chloro-2-hydroxyphenyl)-3-phenylprop-2-en-1-one compounds
Autorzy:
Balaji, S.
Vijayakumar, R.
Manikandan, V.
Senbagam, R.
Rajarajan, M.
Vanangamudi, G.
Thirunarayanan, G.
Powiązania:
https://bibliotekanauki.pl/articles/1182925.pdf
Data publikacji:
2016
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
(e)-5-chloro-2-hydroxyphenyl chalcones
synthesis
uv
ir and nmr spectra
hammett correlation analysis
substituent effect
Opis:
A series of substituted of (E)-1-(5-chloro-2-hydroxyphenyl)-3-phenylprop-2-en-1-one compounds by cross-aldol condensation reaction of 5-chloro-2-hydroxy acetophenone with various substituted benzaldehyde in the presence sodium hydroxide (base). The synthesized substituted (E)-1-(5-chloro-2-hydroxyphenyl)-3-phenylprop-2-en-1-one compounds was characterized by physical constants, UV, FT-IR, 1H & 13C-NMR spectral data. All the spectral data of substituted (E)-1-(5-chloro-2-hydroxyphenyl)-3-phenylprop-2-en-1-one compounds has been Hammett correlation with linear regression analyses.
Źródło:
World Scientific News; 2016, 49, 2; 144-161
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis and antimicrobial activity of substituted (E)-1-(4-fluoro-3-methylphenyl)-3-phenylprop-2-en-1-one compounds
Autorzy:
Balaji, S.
Senbagam, R.
Rajarajan, M.
Vijayakumar, R.
Manikandan, V.
Vanangamud, G.
Thirunarayanan, G.
Powiązania:
https://bibliotekanauki.pl/articles/1189942.pdf
Data publikacji:
2016
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Antibacterial activity
Antifungal activity
Bacillus subtilis
vibrio cholera
Opis:
In an effort to develop antimicrobial agents, a series of substituted (E)-1-(4-fluoro-3-methylphenyl)-3-phenylprop-2-en-1-one compounds were synthesized by crossed-aldol condensation reaction of 4-fluoro-3-methyl acetophenone with various substituted benzaldehydes in the presence of sodium hydroxide. The synthesized compounds were characterized by means of their UV, IR and NMR spectral data. The synthesized substituted (E)-1-(4-fluoro-3-methylphenyl)-3-phenylprop-2-en-1-one compounds were tested for their antibacterial and antifungal activities by the Bauer-Kirby disc diffusion method.
Źródło:
World Scientific News; 2016, 52; 14-30
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis, Assessment of substituent effect and Antimicrobial activities of some substituted (E)-N-benzylidene-4H-1,2,4-triazol-4-amines
Autorzy:
Senbagam, R.
Rajarajan, M.
Vijayakumar, R.
Manikandan, V.
Balaji, S.
Vanangamudi, G.
Thirunarayanan, G.
Powiązania:
https://bibliotekanauki.pl/articles/1194005.pdf
Data publikacji:
2015
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
IR and NMR spectra
QSAR study
UV
antimicrobial study
heterocyclic Schiff bases
synthesis
Opis:
Schiff H., Justus Liebigs Annalen der Chemie. 131(1) (1864) 118-9. [2] Lau K. Y., Mayr A., Cheung K. K., Inorgnic Chimica Acta. 285 (1999) 223-232. [3] Shawali A. S., Harb N. M. S., Badahdah K. O., Journal of Heterocyclic Chemistry. 22 (1985) 1397-1403. [4] Gupta K. C., Sutar A. K., Coordination Chemistry Review. 252 (2008) 1420-1450. [5] Yuan M., Zhao F., Zhang W., Wang Z. M., Gao S., Inorgnic Chemistry. 46 (2007) 11235-42. [6] Nakaic T., Meddu S., Kurahashi T., Japan Patent. 7389932 (1973); Chemical Abstracts. 81(1974) 65182. [7] Quraishi Harion M. A., Sharma K., Journal of Materials Chemistry and Physics. 78 (2002) 18-21. [8] Ramesh S., Rajeshwari S., Elctrochimica Acta. 49 (2004) 811-820. [9] Colter R. J., Matzner M., Ring terming poly, Part B-1, ‘Heterocyclic Ring’ Academic, New Youk, (1972). [10] Popp. F. D., Journal of Organic Chemistry. 26 (1961) 1566-1568. [11] Rao X., Huang X., He L., Song J., Song Z., Shang S., Combinatorial Chemistry & High Throughput Screening. 15 (2012) 840-844. [12] Hadjipavlou-litina D. J., Geronikaki A. A., Letters in Drug Design & Discovery. 15 (1996) 199-206. [13] Tiwary M., Naik S. N., Tiwari D. K., Mittal P. K., Yadav S., Journal of vector Brone Diseases. 44 (2007) 198-204. [14] Solak N., Rollas S., Arkivoc. (2006) 173-181. [15] Wadher S. J., Puranik M. P., Karande N. A., Yeole P. G., International Journal of Pharm Tech Research 1 (2009) 22-33. [16] Cates A. L., Rasheed S. M., Pharmaceutical Research 6 (1984) 271-273. [17] Sakthinathan S. P., Suresh R., Mala V., Sathiyamoorthi K., Kamalakkannan D., Ranganathan K., John Joseph S., Vanangamudi G., Thirunarayanan G., International Journal of Scientific Research and Knowledge, 1(11) (2013) 472. [18] Sakthinathan S. P., Suresh R., Mala V., Sathiyamoorthi K., Kamalakkannan D., Ranganathan K., Arulkumaran R., Vijayakumar S., Sundararajan R., Vanangamudi G., Thirunarayanan G., International Letters of Chemistry, Physics and Astronomy. 6 (2013) 77. [19] Suresh R., Kamalakkannan D., Ranganathan K., Arulkumaran R., Sundararajan R., Sakthinathan S. P., Vijayakumar S., Sathiyamoorthi K., Mala V., Vanangamudi G., Thirumurthy K., Mayavel P., Thirunarayanan G., Spectrochim. Acta, 101A (2013) 239. [20] Arulkumaran R., Vijayakumar S., Sakthinathan S.P., Kamalakkannan D., Ranganathan K., Suresh R., Sundararajan R., Vanangamudi G., Thirunarayanan G., Journal of Chilean Chemical Society. 2 (2013) 58. [21] Thirunarayanan G., Gopalakrishnan M., Vanangamudi G., Spectrochemica Acta 67A (2007)1106-1112 [22] Swain C. G., Lupton E. C., Journal of American Chemical Society. 90 (1968) 4328-4337. [23] Bauer A. W., Kirby W. M. M., Sherris J. C., Truck M., American Journal of Clinical Pathology. 45 (1966) 493-498.
Źródło:
World Scientific News; 2015, 8; 176-191
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis and correlation analysis of spectral data of some (E)-2-benzylidenehydrazine carbothioamides
Autorzy:
Vijayakumar, R.
Rajarajan, M.
Balaji, S.
Manikandan, V.
Senbagam, R.
Vanangamudi, G.
Thirunarayanan, G.
Powiązania:
https://bibliotekanauki.pl/articles/1194021.pdf
Data publikacji:
2015
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Benzaldehyde
Hydrazones
IR & NMR spectral data and substituent effect
Thiosemicarbazide
UV-Vis
Opis:
A series containing ten substituted (E)-2-benzylidenehydrazinecarbothioamide were synthesized by condensation between thiosemicarbazide and various substituted benzaldehydes. The synthesized (E)-2-benzylidenehydrazinecarbothioamide were characterized by their physical constants and spectral data. The UV C=N λmax (nm), infrared ν C=N (cm-1), 1H NMR δ (CH= N) and 13C δ (C=N) spectral data have been correlated with Hammett substituent constants and F and R parameters using single and multi-linear regression analysis. From the results of statistical analysis, the effect of substituents on the above Spectral data has been studied.
Źródło:
World Scientific News; 2015, 9; 70-87
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
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