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Wyszukujesz frazę "Liu, Y. J." wg kryterium: Autor


Tytuł:
Wavelength-adjustable all-optical wavelength conversion using a tunable fiber laser and an electroabsorption modulator
Autorzy:
Tseng, C.-L.
Lin, Y.-W.
Ching, P.-J.
Cheng, Y.-T.
Jou, J.-J.
Liu, C.-K.
Powiązania:
https://bibliotekanauki.pl/articles/174311.pdf
Data publikacji:
2016
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
wavelength conversion
fiber ring laser
erbium-doped fiber
electroabsorption modulator
wavelength division multiplexing (WDM) network
Opis:
A wavelength conversion scheme is presented experimentally using a wavelength tunable erbium-doped fiber laser as a probe light source and an electroabsorption modulator with a DC bias only.For the input wavelength of 1557nm with a 10-Gb/s non-return to zero signal, the Q value is 10.6and the power penalty is less than 1.5dB at a bit error rate of 10–9 at the probe wavelength of1560nm. Given a fixed Q value of 6, probe wavelengths cover a range of 25nm. Furthermore,the relationship between the range of probe wavelength and the amount of power penalty is alsoinvestigated.
Źródło:
Optica Applicata; 2016, 46, 3; 347-352
0078-5466
1899-7015
Pojawia się w:
Optica Applicata
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Water-exit process modeling and added-mass calculation of the submarine-launched missile
Autorzy:
Yang, J.
Feng, J.
Li, Y.
Liu, A.
Hu, J.
Ma, Z.
Powiązania:
https://bibliotekanauki.pl/articles/260251.pdf
Data publikacji:
2017
Wydawca:
Politechnika Gdańska. Wydział Inżynierii Mechanicznej i Okrętownictwa
Tematy:
submarine-launched missile
fluid-structure interaction
water-exit dynamic model
time-varying added-mass
numerical simulation
Opis:
In the process that the submarine-launched missile exits the water, there is the complex fluid solid coupling phenomenon. Therefore, it is difficult to establish the accurate water-exit dynamic model. In the paper, according to the characteristics of the water-exit motion, based on the traditional method of added mass, considering the added mass changing rate, the water-exit dynamic model is established. And with help of the CFX fluid simulation software, a new calculation method of the added mass that is suit for submarine-launched missile is proposed, which can effectively solve the problem of fluid solid coupling in modeling process. Then by the new calculation method, the change law of the added mass in water-exit process of the missile is obtained. In simulated analysis, for the water-exit process of the missile, by comparing the results of the numerical simulation and the calculation of theoretical model, the effectiveness of the new added mass calculation method and the accuracy of the water-exit dynamic model that considers the added mass changing rate are verified.
Źródło:
Polish Maritime Research; 2017, S 3; 152-164
1233-2585
Pojawia się w:
Polish Maritime Research
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Validating performance based critical actions in a high tech start-up
Autorzy:
Vuoti, V. P.
Takala, J.
Mäntylä, A.
Liu, Y.
Yang, W.
binti Abdul Malek, N. A.
Kronman, P.
Kreuzer, A.
Zafar, A.
Powiązania:
https://bibliotekanauki.pl/articles/406824.pdf
Data publikacji:
2014
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
sustainable competitive advantage
sense and respond
manufacturing strategy index
operations strategy
balanced critical factor index
operations start up
case study
Opis:
The objective of this study is to analyze a Finnish manufacturing case company’s operational competitiveness. A proposed analytical model based on analyses the corresponding angles of the strategic triangles (Prospector, Analyzer, and Defender). The model compares the angle differences between the strategy and resource triangles with opinions from different management groups of informants. It was found out that Normalized Scaled Critical Factor Index (NSCFI) model is more scientific comparing to formal ones through validation. Calculations based on the MSI questionnaire resulted in medium high values for the Prospector strategy both for past- and future orientation. S&R calculations regarding the past orientation resulted in low values for all strategy types, except P-NSCFI for Analyzer. Moreover this study covers a case, in where Balanced Critical Factor Index (BCFI) was used defining company annual strategy plan.
Źródło:
Management and Production Engineering Review; 2014, 5, 1; 74-86
2080-8208
2082-1344
Pojawia się w:
Management and Production Engineering Review
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Validating knowledge and technology effects to operative sustainable competitive advantage
Autorzy:
Takala, J.
Koskinen, J.
Liu, Y.
Tas, M. S.
Muhos, M.
Powiązania:
https://bibliotekanauki.pl/articles/407066.pdf
Data publikacji:
2013
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
sustainable competitive advantage
SCA
knowledge
technology rankings
manufacturing strategy
sense and respond
S&R
operational excellence
operations management
dynamic capabilities
Opis:
Purpose: This paper aims to present a fresh idea on how to model and examine the level of sustainable competitive advantage (SCA) with and without knowledge and /technology (K/T) effects in a case company’s operation by taking the manufacturing strategy’s development directions and the efficiency of resource allocation among its attributes into consideration. Design/Methodology/approach: In this paper, questionnaires are filled by two different managerial groups, company’s management team (G1) and company’s global directors (G2). The analyses based on G1, G2 and G1-G2 (mixed results) are performed and examined as well as the effect of knowledge and /technology rankings to observe the differences on how they effect on company’s operations strategy and what kind of strategy type that decision makers might follow. Besides, the effects of knowledge/technology rankings on SCA risk levels are examined on different case companies to perceive the similarities and differences with our case company. In this case study, the objectives are achieved based on several methodologies: manufacturing strategy index (MSI) [1] and sense and respond (S&R) methodology [2]. Findings: The achieved results through the model are found to be promising corresponding to the feedback from the respondents. Research limitations/implications: The model is applied only in a big sized B2B global company that produces power electronics products. Therefore, further tests need to be applied to the model in case of multiple companies from different sizes and areas to figure out the best formula in case of validation of strategic direction (MAPE, RSME or MAD). Practical implications: As a result of its wide applicability and its ease in arrangement the model has an enormous potential for strategic decision-making process and strategic analysis. Originality/Value:The model can provide a more dependable possibility of sustainable improvement to the corporate operational excellence and strategy.
Źródło:
Management and Production Engineering Review; 2013, 4, 3; 45-54
2080-8208
2082-1344
Pojawia się w:
Management and Production Engineering Review
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
UV-Vis spectroscopic detection coupled with chemometrics for the measurement of mixed organic acids in water samples enriched by radial electric focusing solid phase extraction
Autorzy:
Guo, Y.
Liu, X.
Liu, J.
Bian, X.
Zhang, Q.
Pan, J.
Wan, D.
Powiązania:
https://bibliotekanauki.pl/articles/221808.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
chemometrics
UV-Vis spectrophotometer
radial electric focusing solid phase extraction
mixed organic acids
Opis:
Due to the difficulty of detecting traces of organic acid mixture in an aqueous sample and the complexity of resolving UV-Vis spectra effectively, a combinatory method based on a self-made radical electric focusing solid phase extraction (REFSPE) device, UV-Vis detection and partial least squares (PLS) calculation is proposed here. In this study, REFSPE was used to enhance the extraction process of analytes between the aqueous phase and the membrane phase to enrich the trace of mixed organic acid efficiently. Then, the analytes, which were eluted from the adsorption film by ethanol with the assistance of an ultrasonic cleaning machine, were detected with UV-Vis spectrophotometry. After that, the PLS method was introduced to solve the problem of overlapping peaks in UV-Vis spectra of mixed substances and to quantify each compound. The linearly dependent coefficients between the predicted value of the model and the actual concentration of the sample were all higher than 0.99. The limit values of detection for benzoic acid, phthalic acid and p-toluene sulfonic acid were found at 9.9 μg/L, 12.2 μg/L and 13.8 μg/L with the relative recovery values between 84.8% and 117.9%. The RSD (n = 20) values of each component are 1.17%, 1.11% and 0.86%, respectively. Therefore, the proposed combined method can determine traces of complex materials in an aqueous sample efficiently and has wonderful potential applications.
Źródło:
Metrology and Measurement Systems; 2018, 25, 2; 317-329
0860-8229
Pojawia się w:
Metrology and Measurement Systems
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Ustalanie harmonogramu obsługi dla systemu wieloelementowego: podejście oparte na stochastycznych sieciach Petriego oraz algorytmie genetycznym
Maintenance scheduling for multi-unit system: a stochastic Petri-net and genetic algorithm based approach
Autorzy:
Zhang, T.
Cheng, Z.
Liu, Y. J.
Guo, B.
Powiązania:
https://bibliotekanauki.pl/articles/301668.pdf
Data publikacji:
2012
Wydawca:
Polska Akademia Nauk. Polskie Naukowo-Techniczne Towarzystwo Eksploatacyjne PAN
Tematy:
ustalanie harmonogramu obsługi
system wieloelementowy
sieć Petriego
algorytm genetyczny
minimalny przekrój niezdatności
maintenance scheduling
multi-unit system
Petri net
genetic algorithm
deterioration
minimal cut set
Opis:
Częste czynności obsługowe prowadzą do niskiej gotowości systemu oraz wymagają dużych nakładów pieniężnych. W systemie wieloelementowym całkowity czas i koszt obsługi można obniżać łącząc ze sobą czynności obsługowe niektórych elementów. Dlatego też konieczne jest planowanie zoptymalizowanego harmonogramu czynności obsługowych. W artykule zaproponowano model symulacyjny optymalizacji harmonogramu obsługi oparty na stochastycznych sieciach Petriego uwzględniający niepewność zarówno procesu deterioracji jak i procesu obsługi elementów systemu. Algorytm genetyczny wykorzystano do opracowania terminarza czynności obsługowych, który pozwalałby na minimalizację kosztów całkowitych w przyjętym horyzoncie planowania przy uwzględnieniu całkowitego czasu obsługi, stanu elementów, strat wynikających z cyklu życia oraz wykonalności rozwiązania. Ponadto opisano techniki zastosowane w celu zmniejszenia wysiłku obliczeniowego potrzebnego do wykonania analizy. W końcowej części pracy przedstawiono studium przypadku.
Frequent maintenance activities would cause low system availability and require large sums of money. For a multi-unit system, maintenance activities of some units can be combined together to reduce the total maintenance possession time and cost. Therefore, an optimized timetable of the maintenance activities is needed to be planned. Considering the uncertainties in both the deterioration and maintenance process of the units in a system, this paper advances a stochastic Petri-net based simulation optimization model for maintenance scheduling. The genetic algorithm is used to get the solution of the timetable of the maintenance activity schedule such that the overall cost is minimized in a planning horizon taking into account total maintenance possession time, unit condition, life cycle loss and solution feasibility. Some techniques used to reduce the computational effort required to perform the analysis are also described. A case study is given in the end.
Źródło:
Eksploatacja i Niezawodność; 2012, 14, 3; 256-264
1507-2711
Pojawia się w:
Eksploatacja i Niezawodność
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Using a vision cognitive algorithm to schedule virtual machines
Autorzy:
Zhao, J.
Mhedheb, Y.
Tao, J.
Jrad, F.
Liu, Q.
Streit, A.
Powiązania:
https://bibliotekanauki.pl/articles/330838.pdf
Data publikacji:
2014
Wydawca:
Uniwersytet Zielonogórski. Oficyna Wydawnicza
Tematy:
cloud computing
vision cognitive algorithm
VM scheduling
simulation
chmura obliczeniowa
algorytm poznawczy
szeregowanie
symulacja
Opis:
Scheduling virtual machines is a major research topic for cloud computing, because it directly influences the performance, the operation cost and the quality of services. A large cloud center is normally equipped with several hundred thousand physical machines. The mission of the scheduler is to select the best one to host a virtual machine. This is an NP-hard global optimization problem with grand challenges for researchers. This work studies the Virtual Machine (VM) scheduling problem on the cloud. Our primary concern with VM scheduling is the energy consumption, because the largest part of a cloud center operation cost goes to the kilowatts used. We designed a scheduling algorithm that allocates an incoming virtual machine instance on the host machine, which results in the lowest energy consumption of the entire system. More specifically, we developed a new algorithm, called vision cognition, to solve the global optimization problem. This algorithm is inspired by the observation of how human eyes see directly the smallest/largest item without comparing them pairwisely. We theoretically proved that the algorithm works correctly and converges fast. Practically, we validated the novel algorithm, together with the scheduling concept, using a simulation approach. The adopted cloud simulator models different cloud infrastructures with various properties and detailed runtime information that can usually not be acquired from real clouds. The experimental results demonstrate the benefit of our approach in terms of reducing the cloud center energy consumption.
Źródło:
International Journal of Applied Mathematics and Computer Science; 2014, 24, 3; 535-550
1641-876X
2083-8492
Pojawia się w:
International Journal of Applied Mathematics and Computer Science
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Understanding the impact of ‘hard’ and ‘soft’ elements of TQM in south-east European firms
Autorzy:
Imeri, S.
Kekäle, T.
Takala, J.
Liu, Y.
Powiązania:
https://bibliotekanauki.pl/articles/406866.pdf
Data publikacji:
2014
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
TQM
hard element
‘soft’ element
south-eastern Europe
Opis:
The study emphasizes on the understanding of the impact of ‘hard’ and ‘soft’ elements of TQM in South-Eastern European (SEE) firms in Albania, Bulgaria, Bosnia-Herzegovina, Greece, Macedonia, Montenegr, Serbia and Romania. Thus, 350 questionnaires were collected out of 1000. From different industry sectors in order to have reliable statistical measurements of the ‘hard’ and ‘soft’ side of TQM. Hence, this study adopts an exploratory rather than a confirmatory research approach. This approach seeks not only to investigate firms’ awareness and perception to TQM but also explores to what extent are firms’ familiar with TQM tools techniques, and systems as well as TQM philosophies and principles. Therefore, it can be noted TQM is this SEE firms is neither resisted nor directly accepted, rather they tend to see it from a technical aspect, being familiar and understanding only the essential of its ‘hard’ elements and less the ‘soft’ elements.
Źródło:
Management and Production Engineering Review; 2014, 5, 3; 9-13
2080-8208
2082-1344
Pojawia się w:
Management and Production Engineering Review
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Two-terminal reliability analysis for multi-phase communication networks
Analiza niezawodności par terminali w wielofazowych sieciach komunikacyjnych
Autorzy:
Lu, J.-M.
Innal, F.
Wu, X.-Y.
Liu, Y.
Lundteigen, M. A.
Powiązania:
https://bibliotekanauki.pl/articles/301295.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Polskie Naukowo-Techniczne Towarzystwo Eksploatacyjne PAN
Tematy:
binary decision diagram
component-behavior model
multi-phase network systems
system reliability
binarny schemat decyzji
model zachowania komponentów
systemów sieciowych wielofazowe
niezawodność systemu
Opis:
Most researches of network reliability generally assume that the system structures do not change with time. This paper presents the concept of multi-phase network systems (MPNS) to consider dynamic characteristics of networks, and analyze the reliability of MPNS. MPNS reliability is evaluated through a cross-phase binary decision diagram (BDD). The BDD-based algorithm can act as a platform to consider various components behaviors such as repair and growing pressure. Case study shows that the proposed MPNS concept is an effective description of some practical communication networks, and the cross-phase BDD model is efficient in analyzing MPNS reliability.
Większość badań niezawodności sieci ogólnie przyjąć, że struktury systemu nie zmieniają się w czasie. W artykule przedstawiono koncepcję systemów sieciowych wielofazowych (MPNS) rozpatrywanie dynamicznych właściwości sieci i analizy niezawodności MPNS. MPNS niezawodność jest oceniany przez cross-fazowego schematu decyzyjnego binarny (BDD). Algorytm z siedzibą w BDD może działać jako platforma do rozważenia różnych komponentów zachowań, takich jak naprawy i rosnącej presji. Studium przypadku pokazuje, że proponowana koncepcja MPNS jest skutecznym opis niektórych praktycznych sieci komunikacyjnych, a cross-fazowego modelu BDD jest skuteczny w analizie MPNS niezawodność.
Źródło:
Eksploatacja i Niezawodność; 2016, 18, 3; 418-427
1507-2711
Pojawia się w:
Eksploatacja i Niezawodność
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Transformational leadership in operational competitiveness improvement: a case study in Malaysian automotive industry
Autorzy:
Wu, Q.
Shamsuddin, A.
Tasmin, R.
Takala, J.
Liu, Y.
Powiązania:
https://bibliotekanauki.pl/articles/407307.pdf
Data publikacji:
2012
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
przemysł motoryzacyjny
konkurencyjność
transformacja
operational competitiveness
transformational leadership
strategic adjustment
Malaysia
automobile company
Opis:
The purpose of this paper is to analyze operational competitiveness by two core factors, i.e. manufacturing strategy and transformational leadership with technology level. In additional, CFI models in sense and respond (S&R) method are introduced to optimize strategic adjustments, which give supports in fast strategic decision-making process. The analysis results of case study show that leaders in automobile companies in Malaysia should deeply develop their leadership by inspirational motivation, intellectual stimulation and building trust and confidence etc. to improve operational competitiveness. Agile operations strategy should be utilized towards automobile enterprises in Malaysia in order to be competitive under dynamic and tightrope business situations.
Źródło:
Management and Production Engineering Review; 2012, 3, 1; 62-70
2080-8208
2082-1344
Pojawia się w:
Management and Production Engineering Review
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Trace muscovite dissolution separation from vein quartz by elevated temperature and pressure acid leaching using sulphuric acid and ammonia chloride solutions
Autorzy:
Lin, M.
Pei, Z.-Y.
Lei, S.-M.
Liu, Y.-Y.
Xia, Z.-J.
Xie, F.-X.
Powiązania:
https://bibliotekanauki.pl/articles/110755.pdf
Data publikacji:
2018
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
vein quartz
muscovite
sulphuric acid
ammonium chloride
acid leaching
Opis:
Effects of sulphuric acid and ammonia chloride on muscovite dissolution were studied in acid leaching of vein quartz under elevated temperature and pressure. The leaching processes have been studied in detail by analyzing sources of impurity minerals, optimizing leaching process, analyzing leaching kinetics of Al in muscovite and charactering leaching mechanism of muscovite. The results showed that elements of Al and K mainly occurred in muscovite, and 98.10% or more of muscovite could be removed by acid leaching, while the process had limited influence on the particle size of quartz sand. Leaching of Al in the quartz ore was mainly controlled by chemical reaction. A calcination process and ammonia chloride were used for reducing chemical reaction resistance by damaging crystal structure of muscovite and providing stable acid leaching environment. Combined with the calcination process, muscovite, as a main gangue mineral, was effectively extracted during acid leaching of vein quartz at elevated temperature and pressure.
Źródło:
Physicochemical Problems of Mineral Processing; 2018, 54, 2; 448-458
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Toluene Mono-nitration in a Semi-batch Reactor
Autorzy:
Chen, L. P.
Chen, W. P.
Liu, Y.
Peng, J. H.
Liu, R. H.
Powiązania:
https://bibliotekanauki.pl/articles/358853.pdf
Data publikacji:
2008
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
toluene mono-nitration
apparent activation energy
semi-batch reaction
thermal hazard
Opis:
Toluene mono-nitration in a semi-batch reactor was investigated with reaction calorimeter (RC1). The mixed acid HNO3/H2SO4/H2O (wt%) was used in proportion 13/66/21, which is similar to industrial parameters. The exothermic rates at different reaction temperatures were compared, and then the curves of heat generation rate after dosing were analyzed. The Maximal Temperature attainable by runaway of the desired Synthetic Reaction (MTSR) under different conditions were calculated for the course hazard evaluation. The results showed that the average reaction heat of mono-nitration was between 169.07~177.11 kJ mol-1, and the special heat of reactant was about 2 kJ kg-1 K-1. Average Ea of second order kinetic was about 30 kJ mol-1, and reaction rate was 10-4 mol s-1 l-1 order of magnitude when the strength of sulphuric acid was about 73.5%. It was also found that when temperature or stirring speed increases, the potential heat accumulation decreases.
Źródło:
Central European Journal of Energetic Materials; 2008, 5, 2; 37-47
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Thermally Induced Polymorphic Transformation of Hexanitrohexaazaisowurtzitane (HNIW) Investigated by in-situ X-ray Powder Diffraction
Autorzy:
Liu, Y.
Li, S.
Wang, Z.
Xu, J.
Sun, J.
Huang, H.
Powiązania:
https://bibliotekanauki.pl/articles/358065.pdf
Data publikacji:
2016
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
HNIW
polymorphism
in situ X-ray diffraction
phase transition
heat stimulation
Opis:
The ε→γ phase transition of HNIW induced by heat was investigated with in situ X-ray powder diffraction (PXRD). The effects of purity, particle size, insensitive additives and the time of isothermal heat treatment on the phase transition were evaluated. It was found that the phase transition is irreversible with changes in temperature, and the two phases can coexist in a certain temperature range. Moreover, the initial phase transition temperature increases with increasing purity and decreasing particle size of HNIW, and thus with the approximate crystal density. The addition of graphite and paraffin wax to HNIW as insensitive additives leads to a decrease in the initial phase transition temperature, but the addition of TATB does not affect the initial phase transition temperature. Thus, TATB is a suitable insensitive additive. Moreover, at the critical temperature, the isothermal time determined the efficiency of the ε- to γ-phase transition. This work lays the foundations for the choice of molding technologies, performance test methods, ammunition storage options, as well as the manufacture of HNIW-based explosive formulations.
Źródło:
Central European Journal of Energetic Materials; 2016, 13, 4; 1023-1037
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Thermal stability and mechanical properties of hybrid materials based on nitrocellulose grafted by aminopropylisobutyl polyhedral oligomeric silsesquioxane
Stabilność termiczna i właściwości mechaniczne materiałów hybrydowych na bazie nitrocelulozy szczepionej oligomerycznym wielofunkcyjnym aminopropyloizobutylosilseskwioksanem
Autorzy:
Yang, X.
Wang, Y.
Li, Y.
Li, Z.
Song, T.
Liu, X.
Hao, J.
Powiązania:
https://bibliotekanauki.pl/articles/945783.pdf
Data publikacji:
2017
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Chemii Przemysłowej
Tematy:
nitrocellulose
hybrid material
aminopropylisobutyl polyhedral oligomeric silsesquioxane
thermal stability
mechanical properties
nitroceluloza
materiał hybrydowy
oligomeryczny wielofunkcyjny aminopropyloizobutylosilseskwioksan
stabilność termiczna
właściwości mechaniczne
Opis:
The need for improvement in nitrocellulose (NC) storage safety and convenience of application requires an increase in NC thermal stability and enhancement of its mechanical properties. To this aim, hybrid materials were synthesized by grafting NC with aminopropylisobutyl polyhedral oligomeric silsesquioxane (amino-POSS) using isophorone diisocyanate (IPDI) as a crosslinking agent. The structure and elemental composition of the resulting products were confirmed by Fourier transform infrared spectroscopy (FT-IR), nuclear magnetic resonance (1H NMR and 29Si NMR), X-ray diffraction (XRD), and X-ray photoelectron spectroscopy (XPS). It was found, based on the silicon mapping using energy dispersive X-ray spectroscopy (EDS), that amino-POSS was well dispersed in NC matrix. Differential scanning calorimetry (DSC) and thermogravimetric analysis (TGA) studies showed that hybrid amino-POSS-NC materials have higher thermal decomposition activation energy (Ea) compared to NC control sample. According to TGA results, the temperatures of 5 % weight loss (T5 %) and 50 % weight loss (T50 %) as well as the residual masses at 240 °C (CR240 °C), were increased as a result of NC modification with amino-POSS. As can be seen from the digital and scanning electron microscopy (SEM) images, the char layers of amino-POSS-NC hybrid materials after burning in air became more compact with increasing amino-POSS content. XPS studies have shown an increased content of the graphitized carbon in the char residues of the modified samples. The results of DSC, TGA, SEM and XPS studies have directly proved the enhancement of the thermal stability of amino-POSS-NC hybrid materials. In addition, tensile strengths and Young's moduli of amino-POSS-NC hybrid materials were increased gradually with the amino-POSS content in the uniaxial tensile tests. All these results show that the proposed modification of nitrocellulose improves the safety of manufacture and use of this material.
Poprawa bezpieczeństwa przechowywania nitrocelulozy (NC) wymaga zwiększenia jej stabilności termicznej, a wygoda używania poprawy właściwości mechanicznych. W tym celu zsyntetyzowano materiały hybrydowe, w których NC szczepiono oligomerycznym wielofunkcyjnym aminopropyloizobutylosilseskwioksanem (amino-POSS) stosując jako środek sieciujący izoforonodiizocyjanian (IPDI). Strukturę i skład otrzymanych materiałów potwierdzono za pomocą spektroskopii w podczerwieni z transformatą Fouriera (FT-IR), jądrowego rezonansu magnetycznego (1H NMR i 29SiNMR), dyfraktometrii rentgenowskiej (XRD) oraz spektroskopii fotoelektronów rentgenowskich (XPS). Na podstawie wyników badań mapowania Si, otrzymanych metodą spektroskopii dyspersji energii promieniowania rentgenowskiego (EDS), stwierdzono, że amino-POSS został dobrze zdyspergowany w matrycy NC. Badania stabilności termicznej przeprowadzone za pomocą różnicowej kalorymetrii skaningowej (DSC) wykazały, że materiały hybrydowe typu amino-POSS-NC charakteryzują się większymi wartościami energii aktywacji rozkładu termicznego (Ea) niż próbka kontrolna NC. Zgodnie z wynikami analizy termograwimetrycznej (TGA) wartości temperatury ubytku 5 % (T5 %) i 50% (T50 %) masy próbki oraz pozostałości masy w temperaturze 240 °C (CR240 °C) zwiększały się na skutek modyfikacji NC za pomocą amino-POSS. Według fotografii cyfrowych i fotografii wykonanych metodą skaningowej mikroskopii elektronowej (SEM) warstwy węglowe powstałe po spaleniu materiałów hybrydowych w powietrzu wraz ze zwiększeniem zawartości amino-POSS stawały się coraz bardziej zwarte, a wyniki badań XPS wykazały, że tworzyło się coraz więcej węgla w postaci grafitu. Wszystkie wyniki DSC, TGA, SEM i XPS dowodzą poprawy stabilności termicznej materiałów hybrydowych amino-POSS-NC. Stwierdzono także, że wytrzymałość na rozciąganie i moduł Young'a podczas prób jednoosiowego rozciągania materiałów hybrydowych rosną ze zwiększaniem się zawartości amino-POSS. Wyniki wszystkich przeprowadzonych badań dowodzą, że zaproponowana modyfikacja NC poprawia bezpieczeństwo wytwarzania i użytkowania tych materiałów w porównaniu z niemodyfikowanym NC.
Źródło:
Polimery; 2017, 62, 7-8; 576-587
0032-2725
Pojawia się w:
Polimery
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Thermal Mechanical Stress Analysis of Ladle Lining with Integral Brick Joint
Autorzy:
Chang, W.
Li, G.
Kong, J.
Sun, Y.
Jiang, G.
Liu, H.
Powiązania:
https://bibliotekanauki.pl/articles/354915.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
ladle
heat transfer model
lining
expansion joint
thermal mechanical stress
Opis:
Based on the theory of heat transfer, the influence of expansion joints on the temperature and stress distribution of ladle lining is discussed. In view of the current expansion joint, the mathematical model of heat transfer and the three dimensional finite element model of ladle lining brick are established. By analyzing the temperature and stress distribution of ladle lining brick when the expansion joints are in different sizes, the thermal mechanical stress caused by the severe temperature difference can be reduced by the suitable expansion joint of the lining brick during the ladle baking and working process. The analysis results showed that the thermal mechanical stress which is caused by thermal expansion can be released through the 2 mm expansion joint, which is set in the building process. So we can effectively reduce the thermal mechanical stress of the ladle lining, and there is no risk of steel leakage, thus the service life of ladle can be effectively prolonged.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 2; 659-666
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł

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