Informacja

Drogi użytkowniku, aplikacja do prawidłowego działania wymaga obsługi JavaScript. Proszę włącz obsługę JavaScript w Twojej przeglądarce.

English (EN)·Polski (PL)·Yкраїнський (UK)
Przejdź do strony domowej biblioteki Centralna Biblioteka Wojskowa Link otwiera się w nowym oknie Logo biblioteki Prolib Integro - strona głównaCentralna Biblioteka Wojskowa

Wyszukujesz frazę "Lim, K.-S." wg kryterium: Autor

  Lista filtrów
Wyrównaj
    Wyświetlanie 1-15 z 15
    Tytuł:
    Warm Tensile Deformation Behavior and Constitutive Equation of Supersaturated Solid-Solutionized Al-9Mg Extruded Alloy
    Autorzy:
    Yang, Seung Y.
    Kim, Bong H.
    Lee, Da B.
    Choi, Kweon H.
    Kim, Nam S.
    Ha, Seong H.
    Yoon, Young O.
    Lim, Hyun K.
    Kim, Shae
    Kim, Young J.
    Powiązania:
    https://bibliotekanauki.pl/articles/2048882.pdf
    Data publikacji:
    2021
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    aluminum alloy
    Al-9Mg alloy
    tensile test
    constitutive equation
    Opis:
    In this paper, as a purpose to apply the supersaturated solid-solutionized Al-9Mg alloy to the structural sheet parts of automotive, tensile tests were conducted under the various conditions and a constitutive equation was derived from the tensile test results. Al-9Mg alloy was produced using a special Mg master alloy containing Al2Ca during the casting process and extruded into the sheet. In order to study the deformation behavior of Al-9Mg alloy in warm temperature forming environments, tensile tests were conducted under the temperature of 373 K-573 K and the strain rate of 0.001/s~0.1/s. in addition, by using the raw data obtained from tensile tests, a constitutive equation of the Al-9Mg alloy was derived for predicting the optimized condition of the hot stamping process. Al-9Mg alloy showed uncommon deformation behavior at the 373 K and 473 K temperature conditions. The calculated curves from the constitutive equation well-matched with the measured curves from the experiments particularly under the low temperature and high strain rate conditions.
    Źródło:
    Archives of Metallurgy and Materials; 2021, 66, 4; 1013-1018
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Improved Light Conversion Efficiency Of Dye-Sensitized Solar Cell By Dispersing Submicron-Sized Granules Into The Nano-Sized TiO2 Layer
    Poprawa efektywności konwersji światła ogniw słonecznych uczulonych barwnikiem poprzez rozproszenie submikronowych granulek w warstwie nanocząstek TiO2
    Autorzy:
    Song, S. A.
    Lim, M. J.
    Jung, K. Y.
    So, W.-W.
    Moon, S.-J.
    Powiązania:
    https://bibliotekanauki.pl/articles/353347.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    titania nanoparticles
    granules
    dye-sensitized solar cell
    light scattering
    spray pyrolysis
    nanocząsteczki tytanu
    granulat
    uczulone barwnikiem ogniwa słoneczne
    rozpraszanie światła
    Opis:
    In this work, TiO2 nanoparticles and submicron-sized granules were synthesized by a hydrothermal method and spray pyrolysis, respectively. Submicron-sized granules were dispersed into the nano-sized TiO2 layer to improve the light conversion efficiency. Granules showed better light scattering, but lower in terms of the dye-loading quantity and recombination resistance compared with nanoparticles. Consequently, the nano-sized TiO2 layer had higher cell efficiency than the granulized TiO2 layer. When dispersed granules into the nanoparticle layer, the light scattering was enhanced without the loss of dye-loading quantities. The dispersion of granulized TiO2 led to increase the cell efficiency up to 6.51%, which was about 5.2 % higher than that of the electrode consisting of only TiO2 nanoparticles. Finally, the optimal hydrothermal temperature and dispersing quantity of granules were found to be 200°C and 20 wt%, respectively.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1467-1471
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Fabrication of High-Strength Gray Cast Iron Using Permanent Magnet Scrap
    Autorzy:
    Park, S.-Y.
    Kim, J. H.
    Seo, S. J.
    On, J. S.
    Lim, K. M.
    Powiązania:
    https://bibliotekanauki.pl/articles/352204.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    gray cast iron
    rare earth element
    Nd-Fe-B magnet scrap
    graphite formation
    microstructure
    Opis:
    In this study, we have developed the manufacturing technology for high strength gray cast irons by using the spent permanent magnet scraps. The cast specimen inoculated by using a spent magnet scraps showed the excellent tensile strength up to 306MPa. This tensile strength value is 50MPa higher than that of the specimen cast without inoculation, and is similar to that of the specimen inoculated by using the expensive misch-metal. These superior mechanical properties are attributed to complex sulfides created during solidification that promote the formation and growth of Type-A graphite. It is therefore concluded that spent magnets scrap can provide an efficient and cost-effective inoculation agent for the fabrication of high-performance gray cast iron.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1113-1117
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Biodegradable Poly(Lactic Acid)/Multiwalled Carbon Nanotube Nanocomposite Fabrication Using Casting And Hot Press Techniques
    Wytwarzanie biodegradowalnych nanokompozytów typu poli(kwas mlekowy)/wielościenne nanorurki węglowe technikami odlewania i prasowania na gorąco
    Autorzy:
    Park, S. G.
    Abdal-Hay, A.
    Lim, J. K.
    Powiązania:
    https://bibliotekanauki.pl/articles/356593.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    CNTs
    biodegradable polymer
    advanced polymer matrix composites
    hot press
    mechanical properties
    polimer biodegradowalny
    zaawansowane kompozyty polimerowe
    prasowanie na gorąco
    właściwości mechaniczne
    Opis:
    Biodegradable advanced polymer composites have recently received a large amount of attention. The present study aimed to design poly(lactic acid) multiwalled carbon nanotube nanocomposites (PLA/MWCNTs) using a simple fabrication technique. A PLA sheet was first dissolved in dichloromethane, and MWCNTs were subsequently added at various concentrations (0.5, 1.5 and 5%) while applying shear strain stirring to achieve dispersion of carbon nanotubes (CNTs). These solutions were then molded and a hot press was used to generate sheets free of voids with entrapped solvent. The prepared samples were characterized using field emission scanning electron microscopy (FE-SEM), x-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), and thermogravimetric analysis (TGA). Our data showed composite samples free of defects and voids, indicating that the hot press is capable of generating sufficiently compact polymer matrices. Additionally, TGA and FTIR showed significant bonding interactions between the PLA matrix and the nano-fillers. Collectively, our results suggest that incorporation of CNTs as nano-fillers into biodegradable polymers may have multiple applications in many different sectors.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1557-1559
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Demarcation energy properties of regenerated fiber Bragg grating sensors in few-mode fibers
    Autorzy:
    Mohd Nazal, N. A.
    Lai, M.-H.
    Lim, K.-S.
    Gunawardena, D. S.
    Chong, W.-Y.
    Yang, H.-Z.
    Ahmad, H.
    Powiązania:
    https://bibliotekanauki.pl/articles/174756.pdf
    Data publikacji:
    2018
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    regenerated fiber Bragg grating
    thermal regeneration
    thermal decay
    few-mode fibers
    Opis:
    In this work, thermal regeneration of fiber Bragg gratings inscribed in single-mode fibers, two-mode step index fibers and four-mode step index fibers is performed, where the single-mode fibers are used as the reference in the analysis. Specifically, we investigate the behavior of the thermal decay, recovery and eventually the permanent erasure of the gratings in the temperature range from 25 to 1300°C. In the domain of demarcation energy, the thermal responses of the gratings can be normalized and they share similar characteristic curves despite the different temperature ramping rates used in the annealing treatment. It is found that the demarcation energy at the regeneration point and the attempt-to-escape frequency for each grating can be associated with the confinement factors of the fibers. The finding in this work has provided a new insight in the manufacture of regenerated fiber Bragg grating sensors by using few-mode fibers for multiparameter sensing in high temperature environments.
    Źródło:
    Optica Applicata; 2018, 48, 2; 263-271
    0078-5466
    1899-7015
    Pojawia się w:
    Optica Applicata
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Inter-annual and seasonal patterns of precipitable water vapour over Malaysia from 1990-2019 based on MERRA-2 reanalysis
    Autorzy:
    Makama, Ezekiel K.
    Lim, Hwee S.
    Powiązania:
    https://bibliotekanauki.pl/articles/35524412.pdf
    Data publikacji:
    2021
    Wydawca:
    Szkoła Główna Gospodarstwa Wiejskiego w Warszawie. Wydawnictwo Szkoły Głównej Gospodarstwa Wiejskiego w Warszawie
    Tematy:
    total precipitable water vapour
    MERRA-2
    monsoon
    reanalysis
    Opis:
    In this study seasonal and inter-annual patterns as well as trend in the total precipitable water vapour (TPW) over Malaysia, based on a 30-year data from MERRA-2, have been evaluated using least square regression method. Indicator TPW revealed a pair of minima in February/August and maxima in May/November with highest and lowest long-term means found in East Malaysia. Long-term seasonal variability of TPW exhibited latitudinal dependency in both the NEM and SWM seasons. Indicator TPW showed respective southeast-northwest and southwest-northeast spatial distribution in West and East Malaysia, with the highest statistically significant positive trend found in the former.
    Źródło:
    Scientific Review Engineering and Environmental Sciences; 2021, 30, 1; 208-218
    1732-9353
    Pojawia się w:
    Scientific Review Engineering and Environmental Sciences
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Microstructure and Mechanical Properties of Hot-deformed AlMg4 Alloys with the Variations of Mn, Fe, and Si Contents
    Autorzy:
    Lee, Da B.
    Kim, Bong H.
    Choi, Kweon H.
    Yang, Seung Y.
    Kim, Nam S.
    Ha, Seong H.
    Yoon, Young O.
    Lim, Hyun K.
    Kim, Shae
    Hyun, Soong K..
    Powiązania:
    https://bibliotekanauki.pl/articles/351603.pdf
    Data publikacji:
    2020
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Al-Mg alloy
    intermetallic compounds
    homogenization
    hot-rolling
    microstructure
    Opis:
    This paper aims to investigate the microstructural evolution and mechanical properties of hot-deformed AlMg4 alloys with Mn, Fe, and Si as the main impurities. For this purpose, solidification behavior and microstructural evolution during hot-rolling and heat-treatment processes are investigated by using theoretical calculations and experimental characterization. The crystallization and morphological transformation of intermetallic Al3 Fe, Al6 Mn, and Mg2 Si phases are revealed and discussed in terms of the variation in chemical composition. Following a homogenization heat-treatment, the effect of heat treatment on the intermetallic compounds is also investigated after hot-rolling. It was revealed that the Mg2 Si phase can be broken into small particles and spherodized more easily than the Al3 Fe intermetallic phase during the hot-rolling process. For the Mn containing alloys, both yield and ultimate tensile strength of the hot-rolled alloys increased from 270 to 296 MPa while elongation decreased from 17 to 13%, which can be attributed to Mn-containing intermetallic as well as dispersoid.
    Źródło:
    Archives of Metallurgy and Materials; 2020, 65, 4; 1255-1259
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effects of potential level, rotation speed and electrode gap on food waste recovery using an electrostatic separator
    Autorzy:
    Lai, K.
    Lim, S.
    Teh, P.
    Yeap, K.
    Powiązania:
    https://bibliotekanauki.pl/articles/207335.pdf
    Data publikacji:
    2017
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    electrostatic separator
    bioethanol
    waste segregation
    separator elektrostatyczny
    segregowanie odpadów
    bioetanol
    Opis:
    An environmentally friendly method to segregate FW from waste mixture has been presented. The potential level of the separator, the rotation speed and electrode gap are chosen as the independent experimental factors. Second-order quadratic equations have been elaborated to correlate the interactive relationship between the experimental factors and the separation efficiency. The results of the statistical analysis indicate that the electrode gap has immense influence on FW separation. The optimal conditions of segregation have been determined as follows: potential level of 30 kV, rotation speed of 60 rpm, electrode gap of 54 mm and a maximal separation efficiency of 84.0%.
    Źródło:
    Environment Protection Engineering; 2017, 43, 2; 81-92
    0324-8828
    Pojawia się w:
    Environment Protection Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Biological Evaluation of Anodized Biodegradable Magnesium-Calcium Alloys
    Autorzy:
    Kim, J.
    Lee, J.
    Lee, K.
    Park, S.
    Lim, H.
    Park, C.
    Bae, J.
    Yun, K.
    Powiązania:
    https://bibliotekanauki.pl/articles/1398763.pdf
    Data publikacji:
    2016-04
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    87.85.jj
    87.85.J-
    Opis:
    The objective of this study was to evaluate the biocompatibility of studied binary magnesium-calcium (Mg-Ca) alloys for biodegradable intraosseous implants. Mg is necessary for health and is a non-toxic biodegradable material that decomposes naturally in the body. Nevertheless, Mg has been implicated in problems including diminished physical properties and corrosion resistance when degradation is too rapid prior to bone healing. This study has explored the effect of Ca on the corrosion resistance and biological evaluation after anodizing treatment with different contents of Ca alloy. Binary Mg-0.5Ca, Mg-1Ca and Mg-5Ca alloys were prepared by the casting method under an argon atmosphere and cut into disc-shaped pieces. Pure Mg alloy was used as the control. Anodic oxidation was performed for 15 minutes at a voltage of 120 V using an electrolyte solution containing Ca gluconate, sodium hexametaphosphate, and sodium hydroxide at room temperature. Corrosion resistance was analyzed using a corrosion tester. After a hydrogen evolution test, the surface pattern and phase changes were observed on a scanning electron microscop (SEM) and energy dispersive spectroscop (EDS). Microscopic evaluation of the adhesion and cell biological functions of Mg was conducted by observing the response of human fetal osteoblastic 1.19 cells with regard to changes in surface film properties, depending on the amount of Ca. Our results support the view that in Mg-xCa alloys (x=0.5, 1, 5 wt.%) treated using anodic oxidation, the increasing Ca content controls the rate of decomposition and improves corrosion resistance.
    Źródło:
    Acta Physica Polonica A; 2016, 129, 4; 728-735
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Evaluation of Surface Characteristics and Physical Properties on Biodegradable Magnesium-Calcium Alloys by Anodic Oxidation
    Autorzy:
    Kim, J.
    Lee, J.
    Yang, H.
    Park, S.
    Lim, H.
    Oh, G.
    Yun, K.
    Powiązania:
    https://bibliotekanauki.pl/articles/1191716.pdf
    Data publikacji:
    2016-04
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    87.85.jj
    87.85.jc
    Opis:
    The purpose of this study was to determine the effect of calcium (Ca) on the surface characteristics and physical properties of magnesium-calcium alloys after anodization. A novel binary alloy Mg-xCa (in which x=0.5, 1, or 5 wt.%) was cast by combining magnesium (99.9%) and calcium (99.9%) in an argon gas (99.99%) atmosphere. A magnesium alloy rod having a diameter of 15 mm was cut into discs, each 2 mm thick. The specimens were subjected to anodic oxidation at 120 V for 15 minutes at room temperature in an electrolyte solution consisting of calcium gluconate, sodium hexametaphosphate, and sodium hydroxide. Surface and cross-sectional morphological changes were observed using scanning electron microscopy, and the microstructures and phases were detected by means of X-ray diffraction. Hardness and surface roughness were assessed by means of a Vickers hardness tester and a surface roughness meter, respectively. The results show that the physical properties of these magnesium-calcium alloys have been improved, because it was possible to control the dissolution rate according to the amount of calcium added.
    Źródło:
    Acta Physica Polonica A; 2016, 129, 4; 736-741
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Oxidation Behavior of Steel with Cr Content and Water Flow Rate
    Autorzy:
    Kim, D.-J.
    Kim, K. M.
    Shin, J. H.
    Cheong, Y. M.
    Lee, E. H.
    Lee, G. G.
    Kim, S. W.
    Kim, H. P.
    Choi, M. J.
    Lim, Y. S.
    Hwang, S. S.
    Powiązania:
    https://bibliotekanauki.pl/articles/351548.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    steel
    flow accelerated corrosion
    Cr content
    flow rate
    surface oxides
    Opis:
    Fast water flow facilitates ferrous ion transport leading to flow accelerated corrosion (FAC) of carbon steel and the possibility of a large accident through a failure of a secondary pipe in a nuclear power plant. Ion transport is directly linked to oxide properties such as the thickness, chemical composition and porosity. This work deals with a precise observation of the cross section of the corroded specimen focusing on an oxide passivity and its thickness using SEM (scanning electron microscope) and TEM (transmission electron microscope) as well as an apparent weight loss and a surface observation for the specimens corroded using a rotating cylindrical electrode autoclave system in pure water of pH 7 at 150°C having dissolved oxygen below 1 ppb within a flow rate range of 0 to 10 m/s. The Cr content in steel was changed from 0.02 to 2.4 wt%. Increasing the Cr content in the alloy, the FAC rate and oxide thickness decreased. The oxide porosity tends to decrease with the Cr content and immersion time owing to the development of Cr containing oxide. The oxidation behavior is not changed with the immersion time.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1383-1387
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Combined Effect of Zr and Si on Isothermal Oxidation of Ti
    Autorzy:
    Ha, S.-H.
    Kim, B.-H.
    Yoon, Y.-O.
    Lim, H.-K.
    Kim, S. K.
    Powiązania:
    https://bibliotekanauki.pl/articles/353260.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Ti
    Zr
    Si
    silicide
    oxidation
    Opis:
    In this study, the combined effect of Zr and Si on isothermal oxidation of Ti for 25 and 50h at 820°C, which is the temperature related to exhaust valves operation, was investigated. Si addition into Ti-5mass%Zr alloy led to a distribution of silicide Ti5Si3 phase formed by a eutectic reaction. The Ti sample containing only Zr showed more retarded oxidation rate than Ti-6Al-4V, the most prevalent Ti alloy, at the same condition. However, while a simultaneous addition of Zr and Si resulted in greater increase of oxidation resistance. The oxide layer formed after the addition of Zr and Si comprised TiO2, ZrO2, and SiO2.
    Źródło:
    Archives of Metallurgy and Materials; 2018, 63, 3; 1493-1495
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Synthesis and Characterization of a Water-Soluble Ionic Polyacetylene Derivative
    Autorzy:
    Gal, Y.
    Jin, S.
    Park, J.
    Lim, K.
    Powiązania:
    https://bibliotekanauki.pl/articles/1398739.pdf
    Data publikacji:
    2016-04
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    72.80.L
    73.61.P
    78.20.C
    78.30.J
    Opis:
    A new water-soluble ionic polyacetylene was synthesized by the acid-catalyzed polymerization of 2-ethynylpyridine using acrylic acid. The polymerization proceeded well to give a high yield of polymer. The acetylenic C ≡ C bond stretching (2110 cm¯¹) and acetylenic ≡ C-H bond stretching (3293 cm¯¹) peaks of 2-ethynylpyridine monomer were not seen in the FT-IR spectrum of polymer. The electro-optical and electrical properties of the ionic polyacetylene were measured and discussed. The resulting polymer showed strong maximum at 513 nm in the UV-Visible absorption, which is corresponding to photon energy of 2.42 eV. The energy gap width of polymer was estimated to be of 2.08 eV. It was observed that the electrochemical process of polymer is reproducible in the potential range of -1.80 to 1.60 V vs Ag/AgNO₃. HOMO and LUMO levels of polymer were 4.85 eV and 2.77 eV, respectively.
    Źródło:
    Acta Physica Polonica A; 2016, 129, 4; 642-646
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Fabrication of a Spherical Titanium Powder by Combined Combustion Synthesis and DC Plasma Treatment
    Autorzy:
    Choi, S. H.
    Ali, B.
    Hyun, S. K.
    Sim, J. J.
    Choi, W. J.
    Joo, W.
    Lim, J. H.
    Lee, Y. J.
    Kim, T. S.
    Park, K. T.
    Powiązania:
    https://bibliotekanauki.pl/articles/356067.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    combustion synthesis
    DC plasma treatment
    titanium powder
    3D printing process
    combustion parameters
    Opis:
    Combustion synthesis is capable of producing many types of refractory and ceramic materials, as well as metals, with a relatively lower cost and shorter time frame than other solid state synthetic techniques. TiO2 with Mg as reductant were dry mixed and hand compacted into a 60 mm diameter mold and then combusted under an Ar atmosphere. Depending on the reaction parameters (Mg concentration 2 ≤ α ≤ 4), the thermocouples registered temperatures between 1160°C and 1710°C . 3 mol of Mg gave the optimum results with combustion temperature (Tc) and combustion velocity (Uc) values of 1372°C and 0.26 cm/s respectively. Furthermore, this ratio also had the lowest oxygen concentration in this study (0.8 wt%). After combustion, DC plasma treatment was carried out to spheroidize the Ti powder for use in 3D printing. The characterization of the final product was performed using X-ray diffraction, scanning electron microscopy, energy dispersive spectroscopy, and N/O analysis.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1057-1062
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Reaction Kinetics and Morphological Study of TiNb2O7 Synthesized by Solid-State Reaction
    Autorzy:
    Choi, S. H.
    Ali, B.
    Choi, K. S.
    Hyun, S. K.
    Sim, J. J.
    Choi, W. J.
    Joo, W.
    Lim, J. H.
    Lee, T. H.
    Kim, T. S.
    Park, K. T.
    Powiązania:
    https://bibliotekanauki.pl/articles/355326.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    solid state reaction
    kinetic analysis
    quantitative phase analysis
    TiNb2O7 synthesis
    Opis:
    Although TiNb2O7 is regarded as a material with high application potential in lithium-ion batteries (LIBs) and solid-oxide fuel cells (SOFCs), it has been difficult to find suitable cost-effective conditions for synthesizing it on a commercial scale. In this study, TiNb2O7 compounds were synthesized by a solid state synthesis process. For stoichiometrically precise synthesis of the TiNb2O7 phase, the starting materials, TiO2 and Nb2O5 were taken in a 1:1 molar ratio. Activation energy and reaction kinetics of the system were investigated at various synthesis temperatures (800,1000,1200, and 1400°C) and for various holding durations (1,5,10, and 20 h). Furthermore, change in the product morphology and particle size distribution were also evaluated as a function of synthesis temperature and duration. Additionally, quantitative phase analysis was conducted using the Rietveld refinement method. It was found that increases in the synthesis temperature and holding time lead to increase in the mean particle size from 1 to 4.5 μm. The reaction rate constant for the synthesis reaction was also calculated.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1051-1056
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-15 z 15

      Ta witryna wykorzystuje pliki cookies do przechowywania informacji na Twoim komputerze. Pliki cookies stosujemy w celu świadczenia usług na najwyższym poziomie, w tym w sposób dostosowany do indywidualnych potrzeb. Korzystanie z witryny bez zmiany ustawień dotyczących cookies oznacza, że będą one zamieszczane w Twoim komputerze. W każdym momencie możesz dokonać zmiany ustawień dotyczących cookies