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Tytuł:
Valorization of Cobalt from Waste LIB Cathode through Cobalt Oxalate and Cobalt Oxide Synthesis by Leaching-Solvent Extract-Precipitation Stripping
Autorzy:
Swain, B.
Lee, J.-C.
Lee, C.-G.
Powiązania:
https://bibliotekanauki.pl/articles/352333.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
valorization of cobalt
cobalt oxide powder
rod-shaped cobalt oxalate
precipitation stripping
Opis:
An ecoefficient, economical and sustainable valorization process for the synthesis of Co3O4 from waste lithium-ion battery (LIB) by leaching-solvent extract-scrubbing-precipitation stripping route has been developed. Through an optimization, the waste LIB cathode was leached using 2000 mole/m3 of H2SO4 and 5 Vol. % of the H2O2 at a pulp density of 100 kg/m3 under leaching time 60 minutes and temperature 75°C. From the separated leach liquor, cobalt was purified by saponified Cyanex 272. From cobalt, loaded Cyanex 272 impurities were scrubbed and the CoC2O4·2H2O was recovered through precipitation stripping. Finally, the precipitate was calcined to synthesize Co3O4, which is a precursor for LIB cathode materials manufacturing. From TGA-DTA, followed by XRD analysis it was confirmed that at 200°C the CoC2O4·2H2O can be converted to anhydrous CoC2O4 and at 350°C the anhydrous can be converted to Co3O4 and at 1100°C the Co3O4 can be converted to CoO. Through reported route waste LIB can back to LIB manufacturing process through a versatile and flexible industrial approach.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 2; 1037-1042
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The effect of patterns on image-based modelling of texture-less objects
Autorzy:
Hafeez, J.
Jeon, H.-J.
Hamacher, A.
Kwon, S.-C.
Lee, S.-H.
Powiązania:
https://bibliotekanauki.pl/articles/221814.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
structure-from-motion
feature detection
patterns analysis
3D reconstruction
surface comparison
Opis:
The task of generating fast and accurate three-dimensional (3D) models of objects or scenes through a sequence of non-calibrated images is an active field of research. The recent development in algorithm optimization has resulted in many automatic solutions that can provide an accurate 3D model from texture-full objects. Structure-from-motion (SfM) is an image-based method that uses discriminative point-based feature identifier, such as SIFT, to locate feature points in the images. This method faces difficulties when presented with the objects made of homogenous or texture-less surfaces. To reconstruct such surfaces a well-known technique is to apply an artificial variety by covering the surface with a random texture pattern prior to the image capturing process. In this work, we designed three series of image patterns which are tested based on the contrast and density ratio which increases from the first to the last pattern within the same series. The performance of the patterns is evaluated by reconstructing the surface of a texture-less object and comparing it with the true data. Using the best-found patterns from the experiments, a 3D model of a Moai statue is reconstructed. The experimental results demonstrate that the density and structure of a pattern highly affects the quality of the reconstruction.
Źródło:
Metrology and Measurement Systems; 2018, 25, 4; 755-767
0860-8229
Pojawia się w:
Metrology and Measurement Systems
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
System Identification from Multiple-Trial Data Corrupted by Non-Repeating Periodic Disturbances
Autorzy:
Phan, M. Q.
Longman, R. W.
Lee, S. C.
Lee, J. W.
Powiązania:
https://bibliotekanauki.pl/articles/908209.pdf
Data publikacji:
2003
Wydawca:
Uniwersytet Zielonogórski. Oficyna Wydawnicza
Tematy:
automatyka
robotyka
system identification
disturbance identification
iterative learning control
repetitive control
interaction matrix
Opis:
Iterative learning and repetitive control aim to eliminate the effect of unwanted disturbances over repeated trials or cycles. The disturbance-free system model, if known, can be used in a model-based iterative learning or repetitive control system to eliminate the unwanted disturbances. In the case of periodic disturbances, although the unknown disturbance frequencies may be the same from trial to trial, the disturbance amplitudes, phases, and biases do not necessarily repeat. Furthermore, the system may not return to the same initial state at the end of each trial before starting the next trial. In spite of these constraints, this paper shows how to identify the system disturbance-free dynamics from disturbance-corrupted input-output data collected over multiple trials without having to measure the disturbances directly. The system disturbance-free model can then be used to identify the disturbances as well, for use in learning or repetitive control. This paper represents the first extension of the interaction matrix approach to the multiple-trial environment of iterative learning control.
Źródło:
International Journal of Applied Mathematics and Computer Science; 2003, 13, 2; 185-192
1641-876X
2083-8492
Pojawia się w:
International Journal of Applied Mathematics and Computer Science
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis, Structure, Photoluminescence, and Raman Spectrum of Indium Oxide Nanowires
Autorzy:
Kim, H.
Na, H.
Yang, J.
Lee,, C.
Powiązania:
https://bibliotekanauki.pl/articles/1505485.pdf
Data publikacji:
2011-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.07.-b
78.55.-m
Opis:
Production of indium oxide $(In_2O_3)$ whiskers at a very low temperature of 650°C was reported. The synthetic route was comprised of a thermal heating process of a mixture of In and Mg powders. We have investigated the structural properties of the as-synthesized nanowires by using X-ray diffraction and scanning electron microscopy. The product consisted of one-dimensional nanowires, with a crystalline cubic structure of $In_2O_3$. The photoluminescence measurement with the Gaussian fitting exhibited visible light emission bands centered at 2.1 eV and 2.8 eV. The peaks of the Raman spectrum were indexed to the modes being associated with cubic $In_2O_3$.
Źródło:
Acta Physica Polonica A; 2011, 119, 2; 143-145
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Surface Modification of Self-Consolidated Microporous Ti Implant Compacts Fabricated by Electro-Discharge-Sintering in Air
Autorzy:
Jo, Y. J.
Yoon, Y. H.
Kim, Y. H.
Chang, S. Y.
Kim, J. Y.
Lee, Y. K.
Van Tyne, C. J.
Lee, W. H.
Powiązania:
https://bibliotekanauki.pl/articles/356790.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
titanium
implant
porous
sintering
X-ray photoelectron spectroscopy (XPS)
Opis:
A single pulse of 0.75-2.0 kJ/0.7g of atomized spherical Ti powders from 300 mF capacitor was applied to produce a microporous Ti implant compact by electro-discharge-sintering (EDS). A solid core in the middle of the compact surrounded by a microporous layer was found. X-ray photoelectron spectroscopy was employed to study the surface characteristics of the EDS Ti compact and it revealed that Ti, C and O were the main constituents on the surface with a smaller amount of N. The surface was lightly oxidized and was primarily in the form of TiO2 resulting from the air oxidation during EDS processing. The lightly oxidized surface of the EDS compact also exhibited Ti nitrides such as TiN and TiON, which revealed that the reaction between air constituents and the Ti powders even in times as short as 128 msec.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1287-1291
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Study On The Electro-Refining Of Tin In Acid Solution From Electronic Waste
Badanie elektrorafinacji cyny w roztworze kwasu z e-odpadów
Autorzy:
Son, S. H.
Park, S. C.
Kim, J. H.
Kim, Y. H.
Lee, M. S.
Ahn, J.-W.
Powiązania:
https://bibliotekanauki.pl/articles/352665.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
electrorefining
tin
electronic waste
recycling
high purity
elektrorafinacja
cyna
odpady elektroniczne
recykling
Opis:
The tin metal could be retractable from wasted tin scrap, sludge, and wasted electroplated solution hydrometallurgical treatment, and purification process. In order to be used as resource of electronic devices, the retracted crude metal should be purified to the extent of higher than 99.9%. In this study, tin electro-refining process was performed to purify the casted tin crude metal at various experimental conditions: at the current density of 3, 5A/dm2, and in various electrolytes such as hydrochloric acid, sulfuric acid and methansulfonic acid. Additional experiment was conducted using Rotating Disk Electrode (RDE) in order to investigate the rate determining step of tin electro-refining process. The current efficiency, 65.6%, was achievable at the condition of current density, 5A/dm2, and in the electrolyte of Hydrochloric acid. During tin electro-refining process, impurity dissolved from tin crude metal into the electrolyte was analyzed using Inductively Coupled Plasma Optical Emission Spectrometer (ICP-OES), and the result showed the concentration of impurity metal gradually increased. Quantitative analysis on casted tin crude metal showed that it consists of tin with 93.9 wt.% and several impurity metals of Ag, Bi, Pb, Cu, and etc. After tin electro-refining process, the purity of tin increased up to 99.985 wt.%.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1217-1220
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structural Properties and Mechanical Behavior of the 2 Step-Reinforced Al-Si/SiCp Metal Matrix Composite by Titanium-Fiber
Autorzy:
Oak, J.-J.
Lee, Y. C.
Park, Y. H.
Powiązania:
https://bibliotekanauki.pl/articles/356010.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
metal matrix composite
sintering
Ti fiber
mechanical properties
diffusion
Opis:
In this study, the newly designed Al-9Si/SiC particles (SiCp) + Ti-fiber (2step-reinforced Al-9Si alloy matrix) metal matrix composites (MMCs) were fabricated by hot-pressing sintering at 560°C. 2step-reinforced Al-based MMCs were characterized by thermal shrinkage, phase transition, microstructure and tensile strength. The addition of Ti-fiber reduced thermal shrinkage was caused by temperature difference in sintering process as well as enhanced assistance for tensile strength and plastic deformation at room temperature. Experimental results reveal that the 2step-reinforcment sintering by ceramic and metal has a significant effect to increase interface bonding in boundary of each component material and the improved mechanical properties were due to the influence of interfacial product by diffusion. Tensile strength and elongation at room temperature by 2step-reinforcement were improved in 19.5% and 26.2% more than those of Al-9Si/SiCp, respectively. Especially, it reveals that diffusion direction may be varied by sintering methods at low temperature in this study.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1089-1097
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Self-Consolidation Mechanism Of Porous Ti-6Al-4V Implant Prototypes Produced By Electro-Discharge-Sintering Of Spherical Ti-6Al-4V Powders
Mechanizm autokonsolidacji prototypów porowatych implantów wytworzonych przez spiekanie sferycznych proszków Ti-6Al-4V
Autorzy:
Lee, W. H.
Jo, Y. J.
Kim, Y. H.
Jo, Y. H.
Seong, J. G.
Van Tyne, C. J.
Chang, S. Y.
Powiązania:
https://bibliotekanauki.pl/articles/356277.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Ti-6Al-4V
implant
porous
sintering
electrodischarge
porowatość
spiekanie
proszki spiekane
Opis:
Electro-Discharge-Sintering (EDS) was employed to fabricate Ti-6Al-4V porous implant prototypes from atomized powders (100 – 150 μm), that were subjected to discharges of 0.75 to 2.0 kJ/0.7g-powder from 150, 300, and 450 μF capacitors. Both fully porous and porous-surfaced Ti-6Al-4V compacts with various solid core sizes were self-consolidated in less than 86 – 155 μsec. It is known that EDS can simultaneously produce the pinch pressure to squeeze and deform powder particles and the heat to weld them together. The formation of a solid core in these prototypes depends on the amounts of both the pinch pressure and heat generated during a discharge. The size of the solid core and the thickness of the porous layer can be successfully controlled by manipulating the discharge conditions such as input energy and capacitance.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1185-1189
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Recovery Of Electrodic Powder From Spent Lithium Ion Batteries (LIBs)
Odzysk proszku elektrodowego z zużytych akumulatorów litowo-jonowych
Autorzy:
Shin, S. M.
Jung, G. J.
Lee, W-J.
Kang, C. Y.
Wang, J. P.
Powiązania:
https://bibliotekanauki.pl/articles/354084.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
lithium ion battery
electrodic powder
cobalt
lithium
thermal treatment
bateria litowo-jonowa
proszek elektrodowy
kobalt
lit
obróbka termiczna
Opis:
This study was focused on recycling process newly proposed to recover electrodic powder enriched in cobalt (Co) and lithium (Li) from spent lithium ion battery. In addition, this new process was designed to prevent explosion of batteries during thermal treatment under inert atmosphere. Spent lithium ion batteries (LIBs) were heated over the range of 300°C to 600°C for 2 hours and each component was completely separated inside reactor after experiment. Electrodic powder was successfully recovered from bulk components containing several pieces of metals through sieving operation. The electrodic powder obtained was examined by X-ray diffraction (XRD), energy dispersive X-ray spectroscopy (EDS), and atomic absorption spectroscopy (AA) and furthermore image of the powder was taken by scanning electron microscopy (SEM). It was finally found that cobalt and lithium were mainly recovered to about 49 wt.% and 4 wt.% in electrodic powder, respectively.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1145-1149
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Rapid Synthesis of Gold Nano-Particles Using Pulse Waved Potential in a Non-Aqueous Electrolyte
Autorzy:
Jang, J. G.
Lee, J.-O.
Lee, C. K.
Powiązania:
https://bibliotekanauki.pl/articles/352529.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
gold
nanoparticle
nonaqueous electrolyte
pulse wave
catalyst
Opis:
Rapid synthesis of gold nanoparticles (AuNPs) by pulsed electrodeposition was investigated in the non-aqueous electrolyte, 1-ethyl-3-methyl-imidazoliumbis(trifluoro- methanesulfonyl)imide ([EMIM]TFSI) with gold trichloride (AuCl3). To aid the dissolution of AuCl3, 1-ethyl-3-methyl-imidazolium chloride ([EMIM]Cl) was used as a supporting electrolyte in [EMIM]TFSI. Cyclicvoltammetry experiments revealed a cathodic reaction corresponding to the reduction of gold at −0.4 V vs. Pt-QRE. To confirmthe electrodeposition process, potentiostatic electrodeposition of gold in the non-aqueous electrolyte was conducted at −0.4 V for 1 h at room temperature. To synthesize AuNPs, pulsed electrodeposition was conducted with controlled duty factor, pulse duration, and overpotential. The composition, particle-size distribution, and morphology of the AuNPs were confirmed by field-emission scanning electron microscopy (FE-SEM), energy-dispersive spectroscopy (EDS), and transmission electron microscopy (TEM). The electrodeposited AuNPs were uniformly distributed on the platinum electrode surface without any impurities arising from the non-aqueous electrolyte. The size distribution of AuNPs could be also controlled by the electrodeposition conditions.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1389-1392
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Quantitative Analysis of Cryomilled Nanocrystalline Ti-6Al-4V Alloy Powder by X-Ray Diffraction
Autorzy:
Oh, M.
Yu, H. K.
Lee, J.-H.
Oh, M. C.
Jung, S.-H.
Ahn, B.
Powiązania:
https://bibliotekanauki.pl/articles/356265.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
nanocrystalline
cryomilling
Ti alloy
X-ray diffraction
size-strain plot method
Opis:
A nanocrystalline Ti alloy powder was fabricated using cryomilling. The grain size and lattice strain evolution during cryomilling were quantitatively analyzed using X-ray diffraction (XRD) based on the Scherrer equation, Williamson-Hall (W-H) plotting method, and size-strain (S-S) method assuming uniform deformation. Other physical parameters including stress and strain have been calculated. The average crystallite size and the lattice strain evaluated from XRD analysis are in good agreement with the result of transmission electron microscopy (TEM).
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1439-1442
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Photoluminescence Studies of Aluminum Nitride Nanowires
Autorzy:
Yang, J.
Na, H.
Kim, H.
Kebede, M.
Choi, R.
Jeong, J.
Lee, C.
Powiązania:
https://bibliotekanauki.pl/articles/1505466.pdf
Data publikacji:
2011-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.07.-b
78.55.-m
Opis:
We report the production of AlN nanowires by the thermal heating method, for exploring their photoluminescence properties. The room-temperature photoluminescence properties were investigated with different annealing environment. While broad emissions with peaks at around 2.45 and 2.95 eV were obtained from both unannealed and annealed samples, the additional 2.1 eV peak was found from the annealed samples. We have suggested the possible emission mechanisms based on the assumption that both 2.45 eV peak and 2.1 eV peak are ascribed to the nitrogen vacancies. Annealing in N_2 environment exhibited lower intensities of 2.45 eV peak and 2.1 eV peak in comparison to those in Ar environment, presumably due to the suppression of nitrogen vacancies.
Źródło:
Acta Physica Polonica A; 2011, 119, 2; 125-127
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Oxide Formation In Metal Injection Molding Of 316L Stainless Steel
Tworzenie tlenków podczas wtryskiwania proszku stali nierdzewnej 316L
Autorzy:
Jang, J. M.
Lee, W.
Ko, S.-H.
Han, C.
Choi, H.
Powiązania:
https://bibliotekanauki.pl/articles/351352.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
powder injection molding
sintering
316L stainless steel
sintering atmosphere
micro parts
wtryskiwanie proszku
spiekanie
stal nierdzewna 316L
mikro-część
Opis:
The effects of sintering condition and powder size on the microstructure of MIMed parts were investigated using water-atomized 316L stainless steel powder. The 316L stainless steel feedstock was injected into micro mold with micro features of various shapes and dimensions. The green parts were debound and pre-sintered at 800°C in hydrogen atmosphere and then sintered at 1300°C and 1350°C in argon atmosphere of 5torr and 760torr, respectively. The oxide particles were formed and distributed homogeneously inside the sample except for the outermost region regardless of sintering condition and powder size. The width of layer without oxide particles are increased with decrease of sintering atmosphere pressure and powder size. The fine oxides act as the obstacle on grain growth and the high sintering temperature causes severe grain growth in micro features due to larger amount of heat gain than that in macro ones.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1281-1285
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Morphology Change Of Si Deposit In Molten Salt Electrorefining
Zmiana morfologii osadu Si podczas elektrorafinacji w stopionych solach
Autorzy:
Ryu, H. Y.
Kwon, S. C.
Han, M. H.
An, Y. S.
Lee, J. S.
Lee, J. H.
Powiązania:
https://bibliotekanauki.pl/articles/354346.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
molten salt
silicon
morphology
electrorefining
current density
sól stopiona
krzem
morfologia
elektrorafinacja
gęstość prądu
Opis:
The effects of processing parameters on the morphology change in a Si deposit recovered by means of molten salt electrorefining are evaluated using electrochemical techniques such as cyclic voltammetry and chronopotentiometry at 800°C. It was found that concentration of K2SiF6 and current density were important parameters in determining deposit size. Higher concentrations of K2SiF6 were effective in coarsening the silicon deposit and decreasing the cell potential. Silicon nanofiber was recovered at 5 wt% of K2SiF6 whereas dense particles were prepared at 30 and 50 wt% of K2SiF6. The morphology of the Si deposit was determined by the concentration of Si in the electrolyte which is related to the formation of crystal and growth of Si. The formation mechanism of the Si deposit was interpreted by using high resolution TEM as well as electrochemical properties.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1491-1497
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure Evolution of Tungsten-Based ODS Alloys Reinforced with the γ(Ni, Fe) Phase by a Secondary Ball Milling Method
Autorzy:
Chen, C.
Zeng, Y.
Lee, J.
Powiązania:
https://bibliotekanauki.pl/articles/1375180.pdf
Data publikacji:
2014-10
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.20.Ev
81.20.Wk
81.07.Bc
81.05.Ni
Opis:
In the current study, $W-5Ni-2Fe-Y_2O_3$ model alloys were produced using a high-energy planetary ball mill. The presence of the γ(Ni, Fe) phase is favored with respect to material properties in this alloy. Therefore, a secondary ball milling method was introduced to obtain a fine and uniformly distributed γ(Ni, Fe) phase. Phase development of mechanical alloyed powders was investigated by X-ray diffraction. The results show that the formation of the γ(Ni, Fe) phase was found after 18 h of a pre-milling procedure. A further secondary milling method produced a uniform microstructure with grain refinement. TEM results also show changes in the lattice parameters of the tungsten and γ(Ni, Fe) phase associated with the solid solubility limits in the alloy produced by secondary ball milling.
Źródło:
Acta Physica Polonica A; 2014, 126, 4; 907-911
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
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