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    Wyświetlanie 1-13 z 13
    Tytuł:
    Badania właściwości fizykochemiecznych i nawozowych wybranych grup odpadów komunalnych oraz kompostu w celu ich wykorzystywania jako podłoże dla terenów pustynnych
    Analysis of physicochemical and fertilizing properties of selected group of municipal solid waste and compost for utilization as a base for desert land
    Autorzy:
    Klasik, M.
    Alwaeli, M.
    Hryb, W.
    Powiązania:
    https://bibliotekanauki.pl/articles/357135.pdf
    Data publikacji:
    2015
    Wydawca:
    Politechnika Śląska
    Tematy:
    gospodarka odpadami
    papier
    tektura
    tekstylia naturalne
    wykorzystanie
    municipal waste
    paper
    cardboard
    natural textiles
    utilization
    Opis:
    Cywilizacja stale się rozwija, a wraz z nią wzrasta ilość wytwarzanych odpadów komunalnych. Wzrost gospodarczy i bogacenie się społeczeństwa jest wprost proporcjonalne do ilości powstających odpadów komunalnych. Odpady te nie powinny być traktowane jako bezużyteczne frakcje ale źródło surowców do recyklingu czy też wykorzystane do innych metod odzysku odpadów. W pracy przedstawiono wyniki badań wybranych właściwości fizykochemicznych i nawozowych biodegradowalnych frakcji odpadów komunalnych a mianowicie: tekstyliów pochodzenia naturalnego, papieru i tektury pod kątem możliwości ich wykorzystania jako podłoża do adaptacji roślin na terenach zdegradowanych czy pustynnych.
    With continuous economic development, rapid urbanization and industrialization, the amount of generated municipal solid waste, is growing year by year. Due the fact that paper and cardboard are one of the main compositional categories of municipal solid waste, the work was aimed to assess physicochemical and fertilizing properties of paper and cardboard for utilization as a base for desert land. Additionally, in this work we assess physicochemical and fertilizing properties of natural textile to determine their possible use natural textile.
    Źródło:
    Archiwum Gospodarki Odpadami i Ochrony Środowiska; 2015, 17, 1; 149-158
    1733-4381
    Pojawia się w:
    Archiwum Gospodarki Odpadami i Ochrony Środowiska
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Bycie w grafice - własna postawa twórcza i nauczanie
    Being in graphics - a personal creative attitude and teaching
    Autorzy:
    Jackowski, T.
    Wawrzyczek-Klasik, M.
    Masternak, A.
    Powiązania:
    https://bibliotekanauki.pl/articles/115254.pdf
    Data publikacji:
    2016
    Wydawca:
    Wyższa Szkoła Techniczna w Katowicach
    Tematy:
    grafika
    grafika warsztatowa
    proces dydaktyczny
    proces twórczy
    ewolucja własnej postawy twórczej
    technologia graficzna
    materiały graficzne
    sposób nauczania
    postawa artystyczna
    konfrontacja pokoleń
    graphics
    workshop graphics
    didactic process
    creative process
    evolution of personal creative attitude
    graphic materials and technology
    teaching method
    artistic attitude
    generation confrontation
    Opis:
    Artykuł zawiera subiektywne wypowiedzi trojga pracowników WST w Katowicach prof. Tadeusza Jackowskiego, mgr Michaliny Wawrzyczek-Klasik, mgr Artura Masternaka. Dotyczą one szeroko rozumianej grafiki, jej rozwoju i ekspery-mentowania z nią, a także prywatnych inspiracji i autorytetów w dziedzinie. Każdy z interlokutorów porusza te same zagadnienia, wspominając okres swoich studiów, uchylając rąbka tajemnicy własnego warsztatu artystycznego i peda-gogicznego, spojrzenia na sztukę i pracę zawodową. Taki zabieg pozwala na szerokie, wielopłaszczyznowe ukazanie relacji między profesorem a studentem, między mistrzem i uczniem. Projekt powstał po śmierci nieodżałowanego prof. Romana Staraka, który był mentorem i przyjacielem autorów artykułu.
    The article contains subjective statements of three academic staff members of the Katowice School of Technology, professor Tadeusz Jackowski, Michalina Wawrzyczek- Klask MSc, and Artur Masternak MSc. These statements concern a broadly-understood subject of graphics, its development, experimenting with it, as well as private inspirations and authorities in the field. Each of the interlocutors talks about the same topic, remembering the time of his studies, and revealing a small part of their own artistic and teaching workshop, their view on art and professional work. Such an approach allows for a broad, multi-layered show of the relationship between professor and the student, the master and the apprentice. The project was completed after the death of the late great professor Roman Starak, who was a mentor and a friend of the authors of the article.
    Źródło:
    Zeszyty Naukowe Wyższej Szkoły Technicznej w Katowicach; 2016, 8; 211-220
    2082-7016
    2450-5552
    Pojawia się w:
    Zeszyty Naukowe Wyższej Szkoły Technicznej w Katowicach
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Mechanical Characteristics of Ductile Iron Determined in an Original Modified Low Cycle test
    Autorzy:
    Maj, M.
    Pietrzak, K.
    Klasik, A.
    Powiązania:
    https://bibliotekanauki.pl/articles/379780.pdf
    Data publikacji:
    2019
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    iron
    mechanical properties
    microstructure
    żelazo
    właściwości mechaniczne
    mikrostruktura
    Opis:
    The results presented in this article are part of the research on fatigue life of various foundry alloys carried out in recent years in the Lukasiewicz Research Network – Institute of Precision Mechanics and AGH University of Science and Technology, Faculty of Foundry Engineering. The article discusses the test results obtained for the EN-GJS-600-3 cast iron in an original modified low-cycle fatigue test (MLCF), which seems to be a beneficial research tool allowing its users to evaluate the mechanical properties of materials with microstructural heterogeneities under both static and dynamic loads. For a comprehensive analysis of the mechanical behaviour with a focus on fatigue life of alloys, an original modified low cycle fatigue method (MLCF) adapted to the actually available test machine was used. The results of metallographic examinations carried out by light microscopy were also presented. From the analysis of the results of the conducted mechanical tests and structural examinations it follows that the MLCF method is fully applicable in a quick and economically justified assessment of the quality of ductile iron after normalizing treatment.
    Źródło:
    Archives of Foundry Engineering; 2019, 4; 27-32
    1897-3310
    2299-2944
    Pojawia się w:
    Archives of Foundry Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Microstructure and Mechanical Characteristics of the Ternary SnZnAl Lead-Free Alloy
    Autorzy:
    Pietrzak, K.
    Klasik, A.
    Maj, M.
    Sobczak, N.
    Powiązania:
    https://bibliotekanauki.pl/articles/380398.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    lead free alloy
    microstructure
    mechanical properties
    scanning electron microscopy
    stop bezołowiowy
    mikrostruktura
    właściwości mechaniczne
    mikroskop skaningowy
    Opis:
    The paper describes the studies of ternary SnZn9Al1.5 lead-free alloy from the viewpoint of its mechanical behavior as well as microstructure examined by the light and scanning electron microscopy. The authors focused their attention specifically on the fatigue parameters determined by the original modified low-cycle fatigue method (MLCF), which in a quick and economically justified way allows determination of a number of mechanical parameters based on the measurement data coming from one test sample only. The effect of the addition of 1.5% Al to the binary eutectic SnZn9 alloy on its microstructure and the obtained level of mechanical parameters was analyzed. The phases and intermetallic compounds occurring in the alloy were identified based on the chemical analysis carried out in micro-areas by the SEM/EDS technique. It was shown that the addition of 1.5% Al to the binary eutectic SnZn9 alloy resulted in a more favorable microstructure and consequently had a positive effect on the mechanical parameters of the alloy. Based on the conducted research, it was recommended to use a combinatorial method based on the phase quanta theory to quickly evaluate the microstructure and the original MLCF method to determine a number of mechanical parameters.
    Źródło:
    Archives of Foundry Engineering; 2018, 18, 3; 31-36
    1897-3310
    2299-2944
    Pojawia się w:
    Archives of Foundry Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Microstructure and Fatigue Life of the Binary Lead-free Alloys with High Zn Content
    Autorzy:
    Pietrzak, K.
    Klasik, A.
    Maj, M.
    Sobczak, N.
    Powiązania:
    https://bibliotekanauki.pl/articles/382479.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    lead free alloy
    alloy microstructure
    mechanical properties
    stop bezołowiowy
    mikrostruktura stopu
    właściwości mechaniczne
    Opis:
    The results of studies presented in this article are an example of the research activity of the authors related to lead-free alloys. The studies covered binary SnZn90 and SnZn95 lead-free alloys, including their microstructure and complex mechanical characteristics. The microstructure was examined by both light microscopy (LM) and scanning electron microscopy (SEM). The identification of alloy chemical composition in micro-areas was performed by SEM/EDS method. As regards light microscopy, the assessment was of both qualitative and quantitative character. The determination of the geometrical parameters of microstructure was based on an original combinatorial method using phase quantum theory. Comprehensive characterization of mechanical behavior with a focus on fatigue life of alloys was performed by means of the original modified low cycle fatigue method (MLCF) adapted to the actually available test machine. The article discusses the fatigue life of binary SnZn90 and SnZn95 alloys in terms of their microstructure. Additionally, the benefits resulting from the use of the combinatorial method in microstructure examinations and MLCF test in the quick estimation of several mechanical parameters have been underlined.
    Źródło:
    Archives of Foundry Engineering; 2018, 18, 4; 65-70
    1897-3310
    2299-2944
    Pojawia się w:
    Archives of Foundry Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Tribological Examination of Different Steel Materials after Special Heat Treatment and Salt Bath Nitriding
    Autorzy:
    Opaliński, M.
    Mazuro, P.
    Klasik, A.
    Rostek, E.
    Powiązania:
    https://bibliotekanauki.pl/articles/351726.pdf
    Data publikacji:
    2016
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    tribology
    mechanical properties
    steel alloys
    friction coefficient
    Opis:
    The main aim of the presented research was examination of new tribological pairs made of different types of steel. Materials of disc probes were submitted to unusual heat treatment processes and salt bath nitriding. The research is focused on the friction coefficients and mass losses of the material probes. Based on the results it was noticed that the best wear resistant pair was bearing steel 100Cr6 coupled with high speed steel S705. The lowest friction coefficient appeared for the pair bearing steel 100Cr6 and maraging steel C350.
    Źródło:
    Archives of Metallurgy and Materials; 2016, 61, 4; 1881-1888
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Fatigue Life and Microstructure after Multiple Remelting of A359 Matrix Composites Reinforced with SiC Particles
    Autorzy:
    Klasik, A.
    Maj, M.
    Pietrzak, K.
    Wojciechowski, A.
    Sobczak, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/352210.pdf
    Data publikacji:
    2016
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    alloy
    composite
    microstructure
    properties
    recycling
    Opis:
    The article presents the results of fatigue life tests and microstructure examinations of A359 alloy matrix composites (F3S.10S and F3S.30S) containing 10 and 30wt% of SiC particles, subjected to multiple remelting by conventional gravity casting. Mechanical characteristics were determined in a modified low cycle fatigue (MLCF) test, enabling rapid estimation of fatigue life and other mechanical parameters in practice of any material. Qualitative and quantitative metallographic examinations were also carried out. The quantitative evaluation of microstructure was performed by computer image analysis. A set of geometrical parameters of the reinforcing particles, pores and eutectic precipitates present in the metal matrix was determined. The relationships between the mechanical parameters, structural characteristics and the number of remelting operations were presented. It was found that up to the fourth remelting, the mechanical characteristics, including fatigue life, are slightly deteriorated but decrease gradually in the subsequent operations of remelting. The observed effect is mainly due to the shrinkage porosity occurring as a result of gravity casting. To eliminate this defect, the use of squeeze casting process was recommended. It has also been shown that multiple remelting can be an easy and economically well-founded alternative to other more expensive recycling methods.
    Źródło:
    Archives of Metallurgy and Materials; 2016, 61, 4; 2123-2128
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Comparative Studies of Microstructure and Fatigue Life of Selected Lead-free Alloys
    Autorzy:
    Pietrzak, K.
    Klasik, A.
    Maj, M.
    Sobczak, N.
    Wojciechowski, A.
    Powiązania:
    https://bibliotekanauki.pl/articles/379514.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    lead free alloys
    microstructure
    mechanical properties
    stopy bezołowiowe
    mikrostruktura
    właściwości mechaniczne
    Opis:
    Lead-free alloys containing various amounts of zinc (4.5%, 9%, 13%) and constant copper addition (1%) were discussed. The results of microstructure examinations carried out by light microscopy (qualitative and quantitative) and by SEM were presented. In the light microscopy, a combinatorial method was used for the quantitative evaluation of microstructure. In general, this method is based on the phase quanta theory according to which every microstructure can be treated as an arrangement of phases/structural components in the matrix material. Based on this method, selected geometrical parameters of the alloy microstructure were determined. SEM examinations were based on chemical analyses carried out in microregions by EDS technique. The aim of the analyses was to identify the intermetallic phases/compounds occurring in the examined alloys. In fatigue testing, a modified low cycle fatigue test method (MLCF) was used. Its undeniable advantage is the fact that each time, using one sample only, several mechanical parameters can be estimated. As a result of structure examinations, the effect of alloying elements on the formation of intermetallic phases and compounds identified in the examined lead-free alloys was determined. In turn, the results of mechanical tests showed the effect of intermetallic phases identified in the examined alloys on their fatigue life. Some concepts and advantages of the use of the combinatorial and MLCF methods in materials research were also presented.
    Źródło:
    Archives of Foundry Engineering; 2017, 17, 3; 111-116
    1897-3310
    2299-2944
    Pojawia się w:
    Archives of Foundry Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Microstructural Aspects of Fatigue Parameters of Lead-Free Sn-Zn Solders with Various Zn Content
    Autorzy:
    Pietrzak, K.
    Klasik, A.
    Maj, M.
    Wojciechowski, A.
    Sobczak, N.
    Powiązania:
    https://bibliotekanauki.pl/articles/379846.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    lutowanie bezołowiowe
    mikrostruktura
    właściwości mechaniczne
    lead-free solders
    microstructure
    mechanical properties
    Opis:
    The study includes the results of research conducted on selected lead-free binary solder alloys designed for operation at high temperatures. The results of qualitative and quantitative metallographic examinations of SnZn alloys with various Zn content are presented. The quantitative microstructure analysis was carried out using a combinatorial method based on phase quanta theory, according to which any microstructure can be treated as an array of elements disposed in the matrix material. Fatigue tests were also performed using the capabilities of a modified version of the LCF method hereinafter referred to in short as MLCF, which is particularly useful in the estimation of mechanical parameters when there are difficulties in obtaining a large number of samples normally required for the LCF test. The fatigue life of alloys was analyzed in the context of their microstructure. It has been shown that the mechanical properties are improved with the Zn content increasing in the alloy. However, the best properties were obtained in the alloy with a chemical composition close to the eutectic system, when the Zn-rich precipitates showed the most preferred morphological characteristics. At higher content of Zn, a strong structural notch was formed in the alloy as a consequence of the formation in the microstructure of a large amount of the needle-like Zn-rich precipitates deteriorating the mechanical characteristics. Thus, the results obtained during previous own studies, which in the field of mechanical testing were based on static tensile test only, have been confirmed. It is interesting to note that during fatigue testing, both significant strengthening and weakening of the examined material can be expected. The results of fatigue tests performed on SnZn alloys have proved that in this particular case the material was softened.
    Źródło:
    Archives of Foundry Engineering; 2017, 17, 1; 131-136
    1897-3310
    2299-2944
    Pojawia się w:
    Archives of Foundry Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Microstructure and Fatigue Life of the A359 Alloy Reinforced with Al2O3 after Multiple Remelting
    Autorzy:
    Pietrzak, K.
    Klasik, A.
    Maj, M.
    Sobczak, J.
    Wojciechowski, A.
    Powiązania:
    https://bibliotekanauki.pl/articles/380378.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    A359 alloy
    composite microstructure
    mechanical properties
    multiple remelting
    stop A359
    mikrostruktura kompozytu
    właściwości mechaniczne
    przetapianie wielokrotne
    Opis:
    The multiple direct remelting of composites based on the A359 alloy reinforced with 20% of Al2O3 particles was performed. The results of both gravity casting and squeeze casting were examined in terms of the obtained microstructure and mechanical characteristics. In microstructure examinations, the combinatorial method based on phase quanta theory was used. In mechanical tests, the modified low cycle fatigue method (MLCF) was applied. The effects obtained after both gravity casting and squeeze casting were compared. It was noted that both characteristics were gradually deteriorating up to the tenth remelting. The main cause was the occurrence of shrinkage porosity after the gravity casting. Much better results were obtained applying the squeeze casting process. The results of microstructure examinations and fatigue tests enabled drawing the conclusion that the A359 alloy reinforced with Al2O3 particles can confer a much better fatigue life behavior to the resulting composite than the A359 alloy without the reinforcement. At the same time, comparing these results with the results of the previous own research carried out on the composites based also on the A359 alloy but reinforced in the whole volume with SiC particles, it has been concluded that both types of the composites can be subjected to multiple remelting without any significant deterioration of the structural and mechanical characteristics. The concepts and advantages of using the combinatorial and MLCF methods in materials research were also presented.
    Źródło:
    Archives of Foundry Engineering; 2018, 18, 2; 39-44
    1897-3310
    2299-2944
    Pojawia się w:
    Archives of Foundry Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Microstructural Aspects of Fatigue Life of Sn-Zn Lead-free Solders with 1% of Ag Addition
    Autorzy:
    Pietrzak, K.
    Klasik, A.
    Maj, M.
    Sobczak, N.
    Wojciechowski, A.
    Powiązania:
    https://bibliotekanauki.pl/articles/382245.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    lead-free solders
    microstructure
    mechanical properties
    lutowanie bezołowiowe
    mikrostruktura
    właściwości mechaniczne
    Opis:
    The article presents the study results of Sn-Zn lead-free solders with the various Zn content. The results concern the hypoeutectic, eutectic and hypereutectic alloys containing respectively 4.5% Zn, 9% Zn and 13.5% Zn. Moreover, these alloys contain the constant Ag (1%) addition. The aim of the study was to determine the microstructural conditionings of their fatigue life. In particular it was focused on answer the question what meaning can be assigned to the Ag addition in the chemical composition of binary Sn-Zn alloys. The research includes a qualitative and quantitative assessments of the alloy microstructures, that have been carried out in the field of light microscopy (LM). In order to determine some geometrical parameters of the microstructure of alloys the combinatorial method based on the phase quanta theory was applied. Moreover, for the identification necessities the chemical analyses in the micro-areas by SEM/EDS technics were also performed. Based on the SEM/EDS results the phases and intermetallic compounds existing in the examined lead-free solders were identified. The mechanical characteristics were determined by means of the modified low cycle test (MLCF). Based on this method and on the results obtained every time from only one sample the dozen of essential mechanical parameters were evaluated. The research results were the basis of analyzes concerning the effects of microstructural geometrical parameters of lead-free alloys studied on their fatigue life at ambient temperature.
    Źródło:
    Archives of Foundry Engineering; 2018, 18, 1; 87-92
    1897-3310
    2299-2944
    Pojawia się w:
    Archives of Foundry Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Wpływ wielkości kropli na kinetykę zwilżania w układzie SAC305/Ni
    The influence of the drop-size effect on the wetting kinetics in SAC305/Ni system
    Autorzy:
    Turalska, P.
    Sobczak, N.
    Kudyba, A
    Nowak, R.
    Homa, M.
    Siewiorek, A.
    Boroń, Ł.
    Klasik, A.
    Powiązania:
    https://bibliotekanauki.pl/articles/391805.pdf
    Data publikacji:
    2015
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Odlewnictwa
    Tematy:
    kinetyka zwilżania
    kąt zwilżania
    lutowanie bezołowiowe
    SAC305
    nikiel
    efekt wymiarowy kropli
    wetting kinetics
    contact angle
    lead-free soldering
    nickel
    drop-size effect
    Opis:
    Badania wpływu efektu wymiarowego kropli na kinetykę zwilżania niklu bezołowiowym stopem na bazie cyny przeprowadzono metodą kropli leżącej w próżni w temperaturze 260°C. Do badań użyto komercyjny stop lutowniczy na bazie cyny SAC305 (Ag – 3,0% wag., Cu – 0,5% wag.) oraz wypolerowane podłoże niklowe o czystości 99,8%. Podczas testu zwilżalności stosowano osobne nagrzewanie badanej pary materiałów do temperatury badań, umieszczając próbkę stopu w kroplówce grafitowej nad powierzchnią podłoża niklowego. Po osiągnięciu wymaganej temperatury z kapilary wyciskano kroplę stopu i osadzano ją na podłożu. Po 30 sekundach wyciskano kolejną kroplę i osadzano ją na pierwszą, zwiększając tym samym objętość kropli dwukrotnie. Proces dokraplania powtarzano 9 razy co 30 sekund, osiągając 10-krotną objętość kropli w porównaniu do stanu pierwotnego. Po badaniach zwilżalności schłodzoną parę materiałów kropla/podłoże przecinano prostopadle do badanej powierzchni podłoża i poddano badaniom na ścinanie oraz analizie strukturalnej poprzecznego przekroju próbki metodami mikroskopii optycznej i skaningowej mikroskopii elektronowej w połączeniu z lokalną analizą składu chemicznego. Badania zwilżalności nie wykazały istotnych różnic wartości kąta zwilżania ciekłego stopu SAC305 na podłożu niklowym po wielokrotnym dokraplaniu, albowiem wartości kąta zwilżania każdorazowo mierzone w 30. sekundzie kontaktu z podłożem Ni były dla wszystkich 10 kropel zbliżone i wynosiły θ = 35 ±2°. Stwierdzona wysoka powtarzalność pomiarów θ świadczy zarówno o braku występowania efektu wymiarowego w badanym zakresie objętości kropli SAC305, jak i o chemicznej i fizycznej jednorodności powierzchni podłoża. Uzyskane wyniki wskazują na przydatność metody kropli leżącej do oceny jakości powierzchni, szczególnie przydatnej do badań jakości cienkich warstw i pokryć technologicznych stosowanych w procesach łączenia różnorodnych materiałów.
    The studies of the drop-size effect on the wetting kinetics of the nickel substrate by lead-free solder were performed by the sessile drop method in a vacuum at a temperature of 260°C. In this work, Sn-based alloy SAC305 (Ag – 3.0 wt. %, Cu – 0.5 wt. %) and polished nickel substrate (99.8%) were used. During the wettability tests, a separate heating of the couple of materials to a test temperature was performed by placing a sample of SAC305 alloy in a graphite capillary above the nickel substrate. After reaching the test temperature, the SAC305 drop was squeezed from the capillary and deposited on the Ni substrate. After 30 seconds, the second drop was squeezed and deposited on the first one, thereby increasing the volume of the drop twice. The process was repeated 9 times every 30 seconds reaching a 10 times larger drop volume, compared to the first drop. After wettability tests, the solidified drop/substrate couple was cooled, cut and subjected to a shear test and structural analysis by optical microscopy, scanning electron microscopy and energy dispersive X-ray spectroscopy analysis. Wettability studies have not shown a significant difference between the values of the contact angle obtained for each drop produced by subsequent adding of nine drops despite their different size of ten drops produced on the substrate, their contact angle values formed after 30 second contact time were similar showing θ = 35 ±2°. High repeatability of the measured contact angle value θ demonstrates not only physical homogeneity of the substrate surface but it presents a lack of size effect over a range of SAC305 drop volume used in this study. The obtained results demonstrate the suitability of the sessile drop method for surface quality evaluation, particularly for quality tests of thin technological layers or coatings used in joining dissimilar materials.
    Źródło:
    Prace Instytutu Odlewnictwa; 2015, T. 55, nr 2, 2; 3-17
    1899-2439
    Pojawia się w:
    Prace Instytutu Odlewnictwa
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
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