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    Wyświetlanie 1-7 z 7
    Tytuł:
    Recovery Of Nickel From Spent Nickel-Cadmium Batteries Using A Direct Reduction Process
    Odzysk niklu z zużytych baterii niklowo-kadmowych za pomocą bezpośredniej redukcji
    Autorzy:
    Shin, D. J.
    Joo, S.-H.
    Wang, J.-P.
    Shin, S. M.
    Powiązania:
    https://bibliotekanauki.pl/articles/355948.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    spent nickel-cadmium batteries
    direct reduction
    recycling
    heat treatment
    zużyte baterie niklowo-kadmowe
    redukcja bezpośrednia
    recykling
    obróbka cieplna
    Opis:
    Most nickel is produced as Ferro-Nickel through a smelting process from Ni-bearing ore. However, these days, there have been some problems in nickel production due to exhaustion and the low-grade of Ni-bearing ore. Moreover, the smelting process results in a large amount of wastewater, slag and environmental risk. Therefore, in this research, spent Ni-Cd batteries were used as a base material instead of Ni-bearing ore for the recovery of Fe-Ni alloy through a direct reduction process. Spent Ni-Cd batteries contain 24wt% Ni, 18.5wt% Cd, 12.1% C and 27.5wt% polymers such as KOH. For pre-treatment, Cd was vaporized at 1024K. In order to evaluate the reduction conditions of nickel oxide and iron oxide, pre-treated spent Ni-Cd batteries were experimented on under various temperatures, gas-atmospheres and crucible materials. By a series of process, alloys containing 75 wt% Ni and 20 wt% Fe were produced. From the results, the reduction mechanism of nickel oxide and iron oxide were investigated.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1365-1370
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Synthesis of Hexabenzylhexaazaisowurtzitane (HBIW) under Ultrasound Irradiation with Fe3O4@PCA Nanoparticles as an Efficient and Reusable Nanomagnetic Catalyst
    Autorzy:
    Malekzadeh, A. M.
    Shokrollahi, S.
    Ramazani, A.
    Rezaei, S. J. T.
    Asiabi, P. A.
    Joo, S. W.
    Powiązania:
    https://bibliotekanauki.pl/articles/358107.pdf
    Data publikacji:
    2017
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    hexabenzylhexaazaisowurtzitane (HBIW)
    nanomagnetic catalyst
    solid acid
    Fe3O4@PCA
    ultrasound irradiation
    Opis:
    Magnetic Fe3O4@polycitric acid (Fe3O4@PCA) nanoparticles were prepared by the reaction of Fe3O4 nanoparticles with an excess amount of citric acid at 100-160 °C. The magnetic Fe3O4@PCA nanoparticles were characterized by infrared spectroscopy (FTIR), scanning electron microscope (SEM), Transmission Electron Microscopy (TEM), Thermogravimetric Analysis (TGA) and powder X-ray diffraction (XRD). Finally, the synthesized magnetic Fe3O4@PCA nanoparticles were used as a heterogeneous solid acid catalyst for the synthesis of HBIW from benzylamine and glyoxal in acetonitrile-water solvent under ultrasonic irradiation conditions. The catalyst could be reused up to 6 times without significant loss of activity.
    Źródło:
    Central European Journal of Energetic Materials; 2017, 14, 2; 336-350
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Microstructure and Compression Properties of Fe-Cr-B Alloy Manufactured using Laser Metal Deposition
    Autorzy:
    Joo, Y.-A.
    Yoon, T.-S.
    Park, S.-H.
    Lee, K.-A.
    Powiązania:
    https://bibliotekanauki.pl/articles/352075.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Fe-Cr-B composite
    laser Metal Deposition
    bulk type
    microstructure
    compressive properties
    Opis:
    Fe-Cr-B alloy is a material with precipitation of boride inside Fe matrix, and it features outstanding hardness and wear resistance properties. However, Fe-Cr-B alloy is a difficult material to process, making it difficult to use as a bulk type structure material which requires delicate shapes. This study attempted to manufacture Fe-Cr-B alloy using a 3D printing process, laser metal deposition. This study also investigated the microstructure, hardness and compression properties of the manufactured alloy. Phase analysis results is confirmed that α-Fe phase as matrix and (Cr, Fe)2B phase as reinforcement phase. In the case of (Cr, Fe)2B phase, differences were observed according to the sample location. While long, coarse, unidirectional needle-type boride phases (~11 μm thickness) were observed in the center area of the sample, relatively finer boride phases (~6 μm thickness) in random directions were observed in other areas. At room temperature compression test results confirmed that the sample had a compression strength is approximately 2.1 GPa, proving that the sample is a material with extremely high strength. Observation of the compression fracture surface identified intergranular fractures in areas with needle-type boride, and transgranular fractures in areas with random borides. Based on this results, this study also reviewed the deformation behavior of LMD Fe-Cr-B alloy in relation to its microstructures.
    Źródło:
    Archives of Metallurgy and Materials; 2018, 63, 3; 1459-1462
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Extraction Of Cobalt From Spent CMB Catalyst Using Supercritical CO2
    Ekstrakcja kobaltu z zużytych katalizatorów CMB przy użyciu nadkrytycznego
    Autorzy:
    Joo, S.-H.
    Shin, S. M.
    Powiązania:
    https://bibliotekanauki.pl/articles/356283.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    supercritical CO2
    CMB
    cobalt
    manganese
    nadkrytyczny CO2
    kobalt
    mangan
    Opis:
    The metal extraction from spent CMB catalyst using supercritical CO2(scCO2) was investigated with single organic system, binary organic system and ternary organic system to extract metal ions. Leaching solution of spent CMB catalyst containing 389 mg L-1 Co2+, 187 mg L-1 Mn2+, 133 mg L-1 Na+, 14.97 mg L-1 Ca2+ and 13.2 mg L-1 Mg2+. The method consists of scCO2/ligands complexation process and metal extraction process at 60°C and 200bar. The result showed the Co and Mn was selectively extracted from Mg, Ca and Na in the ternary system of mixture of Cyanex272, DEA and Alamine304-I.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1535-1537
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Fabrication of a Spherical Titanium Powder by Combined Combustion Synthesis and DC Plasma Treatment
    Autorzy:
    Choi, S. H.
    Ali, B.
    Hyun, S. K.
    Sim, J. J.
    Choi, W. J.
    Joo, W.
    Lim, J. H.
    Lee, Y. J.
    Kim, T. S.
    Park, K. T.
    Powiązania:
    https://bibliotekanauki.pl/articles/356067.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    combustion synthesis
    DC plasma treatment
    titanium powder
    3D printing process
    combustion parameters
    Opis:
    Combustion synthesis is capable of producing many types of refractory and ceramic materials, as well as metals, with a relatively lower cost and shorter time frame than other solid state synthetic techniques. TiO2 with Mg as reductant were dry mixed and hand compacted into a 60 mm diameter mold and then combusted under an Ar atmosphere. Depending on the reaction parameters (Mg concentration 2 ≤ α ≤ 4), the thermocouples registered temperatures between 1160°C and 1710°C . 3 mol of Mg gave the optimum results with combustion temperature (Tc) and combustion velocity (Uc) values of 1372°C and 0.26 cm/s respectively. Furthermore, this ratio also had the lowest oxygen concentration in this study (0.8 wt%). After combustion, DC plasma treatment was carried out to spheroidize the Ti powder for use in 3D printing. The characterization of the final product was performed using X-ray diffraction, scanning electron microscopy, energy dispersive spectroscopy, and N/O analysis.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1057-1062
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Reaction Kinetics and Morphological Study of TiNb2O7 Synthesized by Solid-State Reaction
    Autorzy:
    Choi, S. H.
    Ali, B.
    Choi, K. S.
    Hyun, S. K.
    Sim, J. J.
    Choi, W. J.
    Joo, W.
    Lim, J. H.
    Lee, T. H.
    Kim, T. S.
    Park, K. T.
    Powiązania:
    https://bibliotekanauki.pl/articles/355326.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    solid state reaction
    kinetic analysis
    quantitative phase analysis
    TiNb2O7 synthesis
    Opis:
    Although TiNb2O7 is regarded as a material with high application potential in lithium-ion batteries (LIBs) and solid-oxide fuel cells (SOFCs), it has been difficult to find suitable cost-effective conditions for synthesizing it on a commercial scale. In this study, TiNb2O7 compounds were synthesized by a solid state synthesis process. For stoichiometrically precise synthesis of the TiNb2O7 phase, the starting materials, TiO2 and Nb2O5 were taken in a 1:1 molar ratio. Activation energy and reaction kinetics of the system were investigated at various synthesis temperatures (800,1000,1200, and 1400°C) and for various holding durations (1,5,10, and 20 h). Furthermore, change in the product morphology and particle size distribution were also evaluated as a function of synthesis temperature and duration. Additionally, quantitative phase analysis was conducted using the Rietveld refinement method. It was found that increases in the synthesis temperature and holding time lead to increase in the mean particle size from 1 to 4.5 μm. The reaction rate constant for the synthesis reaction was also calculated.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1051-1056
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-7 z 7

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