- Tytuł:
- Preparation and Characterization of 1-(5-Azido-1H-1,2,4-triazol-3-yl)tetrazole
- Autorzy:
-
Izsák, D.
Klapötke, T. M. - Powiązania:
- https://bibliotekanauki.pl/articles/358367.pdf
- Data publikacji:
- 2015
- Wydawca:
- Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
- Tematy:
-
energetic materials
heterocycles
triazoles
tetrazoles
azides - Opis:
- This study presents the preparation of 1-(5-azido-1H-1,2,4-triazol-3yl)tetrazole (5) from commercially available chemicals in a five step synthesis. The energetic title compound was comprehensively characterized by various means, including vibrational (IR, Raman) and multinuclear (1H, 13C, 14N, 15N) NMR spectroscopy, mass spectrometry and differential scanning calorimetry. The sensitivities towards various outer stimuli (impact, friction) were determined according to BAM standards. The enthalpy of formation was calculated at the CBS-4M level of theory.
- Źródło:
-
Central European Journal of Energetic Materials; 2015, 12, 3; 403-416
1733-7178 - Pojawia się w:
- Central European Journal of Energetic Materials
- Dostawca treści:
- Biblioteka Nauki
Artykuł