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    Wyświetlanie 1-6 z 6
    Tytuł:
    Synthesis and Thermal and Textural Characterization of Aniline Formaldehyde-Organoclay Composites
    Autorzy:
    Gürses, A.
    Eroğlu, Z.
    Güneş, K.
    Doğar, Ç.
    Powiązania:
    https://bibliotekanauki.pl/articles/1187414.pdf
    Data publikacji:
    2016-04
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.70.Pg
    Opis:
    In this study, the synthesis of aniline-formaldehyde resin, and its thermal and structural characterization, as well as the preparation and characterization of the resin-organoclay composites were carried out. For this, first, at 70°C and acidic conditions the aniline formaldehyde prepolymer was prepared and then cured at 120°C under vacuum. The structural and thermal characterization of the resin was made using FTIR and DSC techniques. By using the Cetyltrimethylammonium Bromide modified Montmorillonite (OMMT) and the synthesized resin, the resin-organoclay composites were prepared by melt intercalation method. Characterization of the resin-organoclay composites prepared with the different ratios of organoclay is made with the same techniques. The FTIR and thermal analysis results of the composites indicate that a cross-linked polymeric matrix was formed. The thermal behavior of the composites has also significantly changed compared to pure resin.
    Źródło:
    Acta Physica Polonica A; 2016, 129, 4; 853-856
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Investigation of Thermal Properties of PUF/colored Organoclay Nanocomposites
    Autorzy:
    Gürses, A.
    Doğar, Ç.
    Köktepe, S.
    Mindivan, F.
    Güneş, K.
    Aktürk, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/1193114.pdf
    Data publikacji:
    2015-04
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    82.35.Np
    81.70.Pg
    62.23.Pq
    Opis:
    Recently PF resins can be also prepared by the addition of urea because urea accelerates cure process of PF resin, reduces the cost and improves its strength performance. Clays have long been used as inorganic fillers in polymer systems because of low cost, availability and improved thermal properties of resulting polymer composites. Clay nanocomposites of different types yield a marked increase in a number of properties of thermoplastic and other resins and composites. This study investigates the variation of thermal properties of PUF/colored organoclay nanocomposites with increased colored clay ratio. For this the DSC, XRD, FT-IR and HRTEM analyses were made. The XRD patterns and HRTEM images showed that clay platelets were exfoliated at the lower contents of organoclay, whereas at the higher content of organo clay tactoids were observed. The XRD analysis results implied that the amorphous behaviour increased with increased content of colored organoclay. The DSC thermograms indicated that glassy transition temperature (T_{g}) was increased, appearing prominent crystallization peaks at the lower ratios of organoclay. The T_{g} value was partially decreased and the peak intensities gradually decreased with increased content of clay. The thermogram for composite with clay content of 20% was similar to the thermogram of virgin resin. This can be attributed to the shifting of the textural structure for this composite from prominent crystalline structure to amorphous one.
    Źródło:
    Acta Physica Polonica A; 2015, 127, 4; 979-983
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Preparation and Characterization of Urea/Formaldehyde/Rosa Canina sp. Seeds Composites
    Autorzy:
    Gürses, A.
    Karagöz, S.
    Mindivan, F.
    Güneş, K.
    Doğar, Ç.
    Aktürk, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/1194519.pdf
    Data publikacji:
    2014-02
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.05.Qk
    Opis:
    Urea-formaldehyde (UF) resin which is one of the most important wood adhesives is a polymeric condensation product of the chemical reaction of formaldehyde with urea, and considered as the most important type of adhesive resins for the production of particleboards. The present study is aimed to preparation and characterization of urea/formaldehyde/Rosa Canina sp. seeds - and urea/formaldehyde/ Rosa Canina sp. seeds/organo clay composites and also to determine the utility as an alternative and low cost material to manufacture particleboard. The synthesis of various composites was carried out using fresh Rosa Canina sp. seeds, typical agricultural waste, in its changing ratios from 7.7 to 83.3 wt%. Also, some of the composite mixtures were prepared by adding organo clay (0.17-3.3 wt%) in a constant ratio of 1/1 wt of urea and formaldehyde. The structural and mechanical characterization of samples was performed by X-ray diffraction, Fourier transform infrared spectra, high resolution transmission electron microscopy images and measurements of Shore D and scratch hardness. The analysis results conclude that organo clay platelets dispersed as simultaneously intercalated and exfoliated in resin matrix and also the increased organo clay ratio led to increase in the hardness values of samples.
    Źródło:
    Acta Physica Polonica A; 2014, 125, 2; 368-373
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Synthesis and Characterization of Phenol/Urea/Formaldehyde and Clay Composites
    Autorzy:
    Doğar, Ç.
    Gürses, A.
    Köktepe, S.
    Mindivan, F.
    Güneş, K.
    Aktürk, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/1194842.pdf
    Data publikacji:
    2014-02
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.05.Qk
    82.35.Gh
    82.35.Lr
    Opis:
    Recently, so-called "phenol-formaldehyde-urea resins", which are generally made only by mechanical blending of UF resin and alkaline type PF resins, have been used as adhesives for the manufacturing of wood products. Faster curing PF resins can be also prepared by the addition of urea during or after the resin synthesis to yield co-condensed phenol-urea-formaldehyde (PUF) resins. In this study, resin/clay composites were prepared by in situ polymerization of phenol(18.2%)-urea(36.3%)-formaldehyde(45.5%) (PUF) with the various ratios of organoclay (7.69-45.45%) and colored organoclay (3.22-20.0%). The objective of our work is the investigation of the effect of addition of both organoclay and colored organoclay at different ratios on the textural characteristics. The composites are characterized by X-ray diffraction, Fourier transform infrared spectroscopy techniques and using high resolution transmission electron microscopy images of the samples. It was found that clay layers exfoliated in the resin matrix.
    Źródło:
    Acta Physica Polonica A; 2014, 125, 2; 374-378
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The diagnostic importance of coagulation parameters in cattle having natural theileriosis
    Autorzy:
    Gunes, V.
    Onmaz, A.C.
    Keles, I.
    Varol, K.
    Ekinci, G.
    Powiązania:
    https://bibliotekanauki.pl/articles/31055.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Opis:
    The purpose of this study was to determine the diagnostic importance of coagulation parameters in cattle with natural theileriosis. Nine Holstein cross-breed cattle with theileriosis as infected group and 6 healthy Holstein cattle as control group were used in the present study. Mean fibrinogen level, thrombin time (TT), activated partial thromboplastin time (aPTT) and prothrombin time (PT) were not statistically different when control and infected groups compared, except for the D-dimer concentration. Quantitative D-dimer concentrations were determined by immune-turbidimetric assay. D-dimer values increased significantly (p<0.05) in infected group (631.55 ± 74.41 μg/L) compared to control group (370.00 ± 59.94 μg/L). D-dimer sensitivity and specificity were also determined at cut-off concentrations (372 μg/L). Sensitivity and specificity of D-dimer values were determined to be 88.89% and 83.33%, respectively. D-dimer is thought to be important indicator in the evaluation of the prognosis in theileriosis cases. Analysis of D-dimer values before and after treatment in controlled case studies were suggested in future studies to enlighten the issue.
    Źródło:
    Polish Journal of Veterinary Sciences; 2017, 20, 2
    1505-1773
    Pojawia się w:
    Polish Journal of Veterinary Sciences
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Antimicrobial property and antiproliferative activity of Centaurea babylonica (L.) L. on human carcinomas and cervical cancer cell lines
    Autorzy:
    Guvensen, N.C.
    Keskin, D.
    Gunes, H.
    Oktay, M.K.
    Yildirim, H.
    Powiązania:
    https://bibliotekanauki.pl/articles/2083066.pdf
    Data publikacji:
    2019
    Wydawca:
    Instytut Medycyny Wsi
    Tematy:
    Centaura babylonica
    antimicrobial activity
    antiproliferative activity
    A-549
    PC-3
    MCF-7 and HeLa cell lines
    chemical
    composition
    GC-MS
    Opis:
    Introduction and objective. Since antiquity, C. babylonica (L.) L. extracts has been used as a remedy for primary health care in traditional medicine. In this study, a total of seven different crude extracts (acetone, chloroform, hexane, ethylacetate, methanol, ethanol and water) from branches and leaves of C. babylonica (L.) L. were prepared to determine antimicrobial and antiproliferative activity against cancer cell lines. Materials and method. MIC assay was used for antimicrobial activity against gram positive and gram negative bacteria, and one yeast. MTT assay was applied to screen the antiproliferative activity of seven extracts, and to determine dose- and time-dependent effects of the aceton extract on A549, PC-3, MCF-7, and HeLa cell lines. Results. The aceton extract of C.babylonica (L.) L. showed the best antibacterial activity against Bacillus cereus, P. aeruginosa and C. albicans (MIC: 1.6 mg/mL). GC-MS analyses allowed six compounds to be determined; the main constituents of acetone extract from C. babylonica (L.) L. were diacetone alcohol (53.47 %), 1-dexadecene (10.19 %) and 1-tetradecene (8.67 %). In addition, seven different solvent extracts at 500 μg/mL caused antiproliferative activity between 84% – 88%, compared to control. Dose-dependent effects of the extracts on A549 cells indicated that chloroform, ethyl acetate, and aceton extract were the most effective extracts with the IC50 values of 9, 33, and 36 μg/mL, respectively. Conclusions. The results clearly demonstrate that C. babylonica (L.) L. exhibited a strong antimicrobial effect and antiproliferative activity against cancer cells in vitro. Further studies are required to isolate and characterize the active pure compounds responsible for the antimicrobial and antiproliferative activities.
    Źródło:
    Annals of Agricultural and Environmental Medicine; 2019, 26, 2; 290-297
    1232-1966
    Pojawia się w:
    Annals of Agricultural and Environmental Medicine
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-6 z 6

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