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    Wyświetlanie 1-5 z 5
    Tytuł:
    Mechanism and Kinetics Studies on Non-Isothermal Decomposition of Ludwigite in Inert Atmosphere
    Autorzy:
    Fu, X.
    Chu, M.
    Gao, L.
    Liu, Z.
    Powiązania:
    https://bibliotekanauki.pl/articles/352128.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    ludwigite
    non-isothermal decomposition
    kinetics
    activation energy
    model function
    Opis:
    Ludwigite is the main available boron-bearing resource in China. In order to enrich the theory system and optimize its utilization processes, this paper study the mechanism and kinetics on non-isothermal decomposition of ludwigite in inert atmosphere by means of thermal analysis. Results show that, the decomposition of serpentine and szajbelyite is the main cause of mass loss in the process. At the end of decomposition, hortonolite and ludwigite are the two main phases in the sample. The average E value of structural water decomposition is 277.97 kJ/mol based on FWO method (277.17 kJ/mol based on KAS method). The results is proved to be accurate and reliable. The mechanism model function of structural water decomposition is confirmed by Satava method and Popescu method. The form of the most probable model function is G(α) = (1 – α)–1– 1 (integral form) and f (α) = (1 – α)2 (differential form), and its mechanism is chemical reaction. This is verified by the criterion based on activation energy of model-free kinetics analysis.
    Źródło:
    Archives of Metallurgy and Materials; 2018, 63, 3; 1217-1224
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Modification Mechanism and Growth Process of Al3(Sc, Zr) Particles in As-cast Al-Si-Mg-Cu-Zr-Sc Alloy
    Autorzy:
    Li, Y.
    Du, X.
    Fu, J.
    Zhang, Y.
    Zhang, Z.
    Zhou, S.
    Wu, Y.
    Powiązania:
    https://bibliotekanauki.pl/articles/382672.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    solidification process
    Al3(Sc, Zr)
    three-dimensional morphology
    eutectic growth
    krzepnięcie stopu
    morfologia trójwymiarowa
    wzrost eutektyczny
    Opis:
    In this study, the modification mechanism and growth process of Al3(Sc, Zr) particles in as-cast Al-Si-Mg-Cu based alloy with addition of Sc and Zr were systematically investigated. It was found that 0.57 wt-%Sc addition caused a significant refinement in the average grain size of the investigated alloy, which brought about a remarkable transformation in as-cast microstructure, from thick dendritic shape to fine equiaxed structure. A large amount of primary Al3(Sc, Zr) particles with the dimension of around 5-6 μm were also observed within the equiaxed grain. Due to the identical orientation and similar crystal structure between primary Al3(Sc, Zr) particles and α-Al matrix, the primary particles always served as heterogeneous nucleus for the α-Al matrix. In addition, these cusped cubic primary Al3(Sc, Zr) particles showed triangle, star, rhomboid morphologies are generated from sectioning the particle in (111), (100) and (110) planes, respectively. Particularly, the typical eutectic structure which contained odd number-layer (Al3(Sc, Zr)+α-Al+ ... +Al3(Sc, Zr)) was observed within the investigated particles.
    Źródło:
    Archives of Foundry Engineering; 2018, 18, 2; 51-56
    1897-3310
    2299-2944
    Pojawia się w:
    Archives of Foundry Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Thermal Decomposition Characteristics of Ammonium Nitrate(V) in the Presence of Mn2O3/Graphene Oxides
    Autorzy:
    Xu, Z.
    Xu, G.
    Fu, X.
    Wang, Q.
    Powiązania:
    https://bibliotekanauki.pl/articles/358837.pdf
    Data publikacji:
    2017
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    ammonium nitrate(V)
    nano-oxides
    graphene oxide
    thermal decomposition
    RSFTIR
    Opis:
    Nano-composites (Mn2O3, Mn2O3/graphene oxides (GO)) were prepared by a new method. The nano-composites were characterized by XRD and HRTEM. The catalytic performance of the nano-composites on the thermal decomposition of ammonium nitrate(V) (AN) was investigated by TG-DSC and TG-MS. The reaction of AN with the nano-composites in the condensed phase was investigated by RSFTIR. The results of TG-DSC experiments indicated that the nano-composites significantly catalyze the thermal decomposition of AN, especial Mn2O3/GO. The exothermic reaction of AN with Mn2O3/GO commenced at about 185 °C. Based on the TG-MS results, it was ascribed to N2O formation. In the RSFTIR experiments, the dissociation reaction and ionization reaction of AN were both detected. NOx formation at low temperature was also found. NH2 was directly oxidized by HNO3/NO3− at low temperature. The interaction between Mn2O3 and NH3 was detected according to DRIFT experiments. At elevated temperature, the functional groups of GO are destroyed, which had an influence on the interaction between Mn2O3 and GO. A probable mechanism for the exothermic reaction and then its disappearance is proposed. HNO3 gas was absorbed on the surface of solid AN, which can markedly catalyze the thermal decomposition of AN. Perhaps the HNO3 plays a key role in the exothermic reaction and then the reaction of AN disappears at very low temperatures.
    Źródło:
    Central European Journal of Energetic Materials; 2017, 14, 3; 636-659
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Phase Stability of Ammonium Nitrate with Organic Potassium Salts
    Autorzy:
    Xu, Z.-X.
    Fu, X.-Q.
    Wang, Q.
    Powiązania:
    https://bibliotekanauki.pl/articles/358264.pdf
    Data publikacji:
    2016
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    ammonium nitrate(V)
    phase transition
    organic compounds
    differential scanning calorimetry
    Opis:
    A study has been undertaken on the effect of additives on the phase transition of ammonium nitrate(V) (AN). Results obtained using Differential Scanning Calorimetry (DSC) showed that organic compounds and potassium salts of organic compounds have an effect on the phase transition behavior of AN. The samples were further analyzed using infrared (IR) and powder X-ray diffraction (XRD). The mechanism of phase stabilization of AN by compounds of this kind was examined. The present study showed that the influence of additives on the phase transition of AN occurs through the polar groups that are involved in intermolecular interactions of orbital and electrostatic types that form new hydrogen bonds. AN exists in only one phase in the temperature range from 30 °C to +100 °C, when a potassium salt of organic compounds was added. However, with organic compounds, the III→II phase transition was changed. IR and XRD of composites are characterized by new intermolecular interactions. Compacted samples of AN containing potassium salts of organic compounds exhibited better stability than AN containing organic compounds to multiple cyclic changes within a temperature range. This we named ‘freezing and thawing analysis’. Additives have two functions on the AN phase transition. First, solid solutions of AN mixture were formed for K+ replacement of NH4+. Second, hydrogen bonds formed, which caused AN and salts of organic compounds to interact intimately.
    Źródło:
    Central European Journal of Energetic Materials; 2016, 13, 3; 736-754
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The distribution of different virulence grass carp reovirus strains in some neglected tissues
    Autorzy:
    Liang, H.R.
    Fu, X.Z.
    Li, N.Q.
    Liu, L.H.
    Lin, Q.
    Li, Y.G.
    Peng, Y.A.
    Huang, Z.B.
    Wu, S.Q.
    Powiązania:
    https://bibliotekanauki.pl/articles/30668.pdf
    Data publikacji:
    2016
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Źródło:
    Polish Journal of Veterinary Sciences; 2016, 19, 4
    1505-1773
    Pojawia się w:
    Polish Journal of Veterinary Sciences
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-5 z 5

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