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    Wyświetlanie 1-7 z 7
    Tytuł:
    One-dimensional isothermal multicomponent diffusion-reaction model and its application to methanol synthesis over commercial Cu-based catalyst
    Autorzy:
    Lei, K.
    Ma, H.
    Zhang, H.
    Ying, W.
    Fang, D.
    Powiązania:
    https://bibliotekanauki.pl/articles/778972.pdf
    Data publikacji:
    2015
    Wydawca:
    Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
    Tematy:
    global kinetics
    internal effectiveness factor
    diffusion-reaction model
    methanol synthesis
    Opis:
    The present work was a study on global reaction rate of methanol synthesis. We measured experimentally the global reaction rate in the internal recycle gradientless reactor over catalyst SC309. The diffusion-reaction model of methanol synthesis was suggested. For model we chose the hydrogenation of CO and CO2 &enspas key reaction. CO and CO2 &enspwere key components in our model. The internal diffusion effectiveness factors of CO and CO2&enspin the catalyst were calculated by the numerical integration. A comparison with the experiment showed that all the absolute values of the relative error were less than 10%. The simulation results showed that decreasing reaction temperature and catalyst diameter were conducive to reduce the influence of the internal diffusion on the methanol synthesis.
    Źródło:
    Polish Journal of Chemical Technology; 2015, 17, 1; 103-109
    1509-8117
    1899-4741
    Pojawia się w:
    Polish Journal of Chemical Technology
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Process simulation of dimethyl ether synthesis via methanol vapor phase dehydration
    Autorzy:
    Bai, Z.
    Ma, H.
    Zhang, H.
    Ying, W.
    Fang, D.
    Powiązania:
    https://bibliotekanauki.pl/articles/779378.pdf
    Data publikacji:
    2013
    Wydawca:
    Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
    Tematy:
    dimethyl ether
    methanol dehydration to DME
    process simulation
    Opis:
    The production processes included catalytic dehydration of methanol in an adiabatic fixed-bed reactor and two columns product separations. In this study, the technological process for dimethyl ether (DME) synthesis is built on PRO/II platform based on the combined parameters of the reaction dynamic model for methanol dehydration reaction, the improved NRTL model of the liquid phase, the PR model of vapor phase. In order to validate the proposed model, the simulation results have been compared with the available data from a set of industrial production equipment with a production capacity of 200 000 tonnes per annum. A comparison between the calculated and measured results has proved that these results are satisfactory. The bed height and the volume of the catalytic bed are calculated aim at one million t/a DME yields and while taking account of high-purity DME production. After discussing the influence of feed stage location and reflux ratio for DME product purity, the suitable unit operation conditions are chosen. Accordingly, accurate process simulation results provide the basis and guidance for an improvement and development of the similar industrial device.
    Źródło:
    Polish Journal of Chemical Technology; 2013, 15, 2; 122-127
    1509-8117
    1899-4741
    Pojawia się w:
    Polish Journal of Chemical Technology
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The effect of preparation method on the performance of PtSn/Al2O3 &enspcatalysts for acetic acid hydrogenation
    Autorzy:
    Zhang, K.
    Zhang, H.
    Ma, H.
    Ying, W.
    Fang, D.
    Powiązania:
    https://bibliotekanauki.pl/articles/779525.pdf
    Data publikacji:
    2015
    Wydawca:
    Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
    Tematy:
    Pt-Sn catalysts
    preparation method
    acetic acid hydrogenation
    XPS
    CO-FTIR
    Opis:
    PtSn/Al2O3 &enspcatalysts with a given loading of 1 wt% Pt and 1 wt% Sn were prepared by co-impregnation or successive impregnation with aqueous solutions of Pt, Sn precursors and a commercial alumina. The catalysts were characterized by N2 &enspadsorption, H2-TPR (H2&ensp temperature-programmed reduction), H2-pulse chemisorption, XPS (X-ray photoelectron spectroscopy) and CO-FTIR (Fourier transform infrared spectroscopy), and tested in the hydrogenation of acetic acid. The results showed that the preparation method affected both the chemical properties and their performance in the hydrogenation of acetic acid. Sn enrichment on the catalysts surface was observed on the co-impregnated catalyst and catalyst in which the Pt precursor had been loaded first. It was found that the modification of Pt was a function of the sequence of Sn addition as revealed by CO-FTIR. Co-impregnated catalyst showed the highest activity and ethanol selectivity.
    Źródło:
    Polish Journal of Chemical Technology; 2015, 17, 1; 11-17
    1509-8117
    1899-4741
    Pojawia się w:
    Polish Journal of Chemical Technology
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect of boron on ZSM-5 catalyst for methanol to propylene conversion
    Autorzy:
    Xu, A.
    Ma, H.
    Zhang, H.
    Ying, W.
    Fang, D.
    Powiązania:
    https://bibliotekanauki.pl/articles/777971.pdf
    Data publikacji:
    2013
    Wydawca:
    Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
    Tematy:
    methanol to propylene
    ZSM-5
    boron modifi cation
    propylene
    Opis:
    B-ZSM-5 catalysts were prepared by various modification methods with boric acid, including ion-exchange, impregnation and direct synthesis. The catalysts were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), NH3-Temperature Programmed Desorption (NH3-TPD), N2 adsorption-desorption, Fourier Transform Infrared spectrometry (FT-IR), 27Al and 11B MAS NMR spectra. The results revealed that the weak acidity of catalysts was significantly increased by modification. The catalytic activity was measured in a fixed bed at 460°C for methanol to propylene (MTP) reaction. The results of MTP reaction showed a great increment of the propylene selectivity for the boron modified samples, especially for the directly synthesized B-ZSM-5 which also displayed high activity and selectivity towards C2 =-C4 = olefins. It was found that the remarkable selectivity strongly depended on the intensity of weak acidity.
    Źródło:
    Polish Journal of Chemical Technology; 2013, 15, 4; 95-101
    1509-8117
    1899-4741
    Pojawia się w:
    Polish Journal of Chemical Technology
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Investigations of the Optical Band Positions and Spin-Hamiltonian Parameters for the Rhombic $VO^{2+}$ Complex in CsCl Crystal
    Autorzy:
    Fang, W.
    Zheng, W.
    Yang, D.
    Tang, H.
    Powiązania:
    https://bibliotekanauki.pl/articles/1365269.pdf
    Data publikacji:
    2014-05
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    71.70.Ch
    75.10.Dg
    61.72.Bb
    76.30.Fc
    Opis:
    The optical band positions and spin-Hamiltonian parameters (g factors $g_{i}$ and hyperfine structure constants $A_{i}$, where i=x, y, z) of the rhombic $VO^{2+}$ complex in CsCl crystal are calculated together from two theoretical methods. One is the complete diagonalization (of energy matrix) method and another is the perturbation theory method. The calculated results from the two methods coincide and are in reasonable agreement with the experimental values. So, both methods are effective in the explanations of optical and electron paramagnetic resonance (EPR) data for $d^1$ ions in crystals. The calculations also suggest that in $d^1$ rhombic octahedra the ground state is almost a pure | $d_{xy}$ ⟩ state. This point is different from that of conjugate $d^9$ (e.g., $Cu^{2+}$) ions in rhombic octahedra where the ground state should be an admixture of ground and first excited states.
    Źródło:
    Acta Physica Polonica A; 2014, 125, 5; 1206-1209
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Generation of chirped microwave signal with any central frequency based on a nonuniformly spaced finite impulse response filter
    Autorzy:
    Chen, D.
    Wang, R.
    Pu, T.
    Xiang, P.
    Fang, T.
    Zheng, J.
    Xiong, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/174334.pdf
    Data publikacji:
    2016
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    microwave photonics
    microwave photonic filter
    chirped microwave signal
    dual drive Mach–Zehnder modulator
    Opis:
    A novel optical approach to generating a chirped microwave signal by using a nonuniformly spaced finite impulse response filter is proposed and demonstrated. In this scheme, a narrowband Gaussian pulse is used as the original chirped-free signal, which is easy to be acquired. To eliminate the need of a wideband chirped-free signal, a mixer and a radio frequency signal are used to up-convert the spectrum of the original Gaussian signal. Therefore, the required frequency response can be calculated and reconstructed by a finite impulse response filter with nonuniformly spaced taps. Besides, a dual drive Mach–Zehnder modulator is used to realize single sideband modulation of the chirpedfree signal. Thus, the transfer function induced by the fiber dispersion is eliminated and the chirped microwave signal with any central frequency can be generated. In this paper, a design example of a filter with a central frequency of 10GHz is provided, and generation of the target chirped microwave signal is also demonstrated by numerical simulations.
    Źródło:
    Optica Applicata; 2016, 46, 3; 399-408
    0078-5466
    1899-7015
    Pojawia się w:
    Optica Applicata
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Heavy Metal Contamination of Surface Water and Groundwater in and Around Gejiu Tin Mine, Southwest China
    Zanieczyszczenie wód powierzchniowych i podziemnych metalami ciężkimi w kopalni Gejiu Tin, południowo-zachodnie Chiny i jej okolicach
    Autorzy:
    Cheng, X.
    Qi, W.
    Danek, T.
    Matysek, D.
    Huang, Q.
    Zhao, X.
    Zhou, Z.
    Fang, R.
    Zou, L.
    Xu, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/317873.pdf
    Data publikacji:
    2016
    Wydawca:
    Polskie Towarzystwo Przeróbki Kopalin
    Tematy:
    metale ciężkie
    zanieczyszczenie
    kopalnia cyny Gejiu
    wody powierzchniowe
    wody kopalniane
    heavy metals
    contamination
    Gejiu tin mine
    surface water
    mine water
    Opis:
    Heavy metal contamination due to mining activity is a global major concern because of its potential health risks to local inhabitants. The heavy metal contamination of surface water and ground water by mining activities in Gejiu tin-polymetallic mining area, Southwest China, was studied. Surface water and ground water were sampled and analyzed using AAS for Cr6+, Cd, As, Hg, Cu, Pb, Zn, Se, Fe and Mn. Analysis of HCO3–, Cl–, SO42–, F– and NO3– in water samples was also undertaken by ion chromatography. It was shown that none of water samples exceeded the guideline of Cr6+, Se and Hg, while the contamination degree of heavy metals was Mn > Fe > Cd > Zn > Pb > As > Cu, all of which were serious contamination except mild contamination for Cu. The ground waters were polluted much worse than surface water.
    Zanieczyszczenie metalami ciężkimi spowodowane działalnością kopalń jest światowym problemem z powodu ryzyka utraty zdrowia przez okolicznych mieszkańców. Zbadano zanieczyszczenie wód powierzchniowych oraz wód podziemnych wywołane działalnością kopalni cyny w rejonie górniczym Gejiu, południowo-zachodnie Chiny. Pobrano próbki wody powierzchniowej oraz podziemnej i zanalizowano je ze względu na obecność Cd, As, Hg, Cu, Pb, Zn, Se, Fe oraz Mn. Analizy HCO3–, Cl–, SO42–, F– oraz NO3– w próbkach wody również zostały przeprowadzone za pomocą chromatografii jonowej. Ukazano, że żadna z badanych wód nie przekroczyła dopuszczalnych poziomów dla Cr6+, Se oraz Hg. Jednakże poziom zanieczyszczenia metali ciężkimi tj. Mn > Fe > Cd > Zn > Pb > As > Cu był wysoki, za wyjątkiem niewielkiego przekroczenia norm dla Cu. Wody podziemne były znacznie bardziej zanieczyszczone niż wody powierzchniowe.
    Źródło:
    Inżynieria Mineralna; 2016, R. 17, nr 1, 1; 93-98
    1640-4920
    Pojawia się w:
    Inżynieria Mineralna
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-7 z 7

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