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    Wyświetlanie 1-4 z 4
    Tytuł:
    Significance of the receding contact angle in the determination of surface free energy
    Autorzy:
    Chodkowski, Michał Paweł
    Powiązania:
    https://bibliotekanauki.pl/articles/2079958.pdf
    Data publikacji:
    2018
    Wydawca:
    Uniwersytet Marii Curie-Skłodowskiej. Wydawnictwo Uniwersytetu Marii Curie-Skłodowskiej
    Tematy:
    receding contact angle
    equilibrium contact angle
    Tadmor’s contact angle
    CAH
    surface free energy
    Opis:
    Surface free energy measurements of solids are a very important issue in various fields of science. Many functional, chemical and physical properties of a given material depend on its surface free energy. The basic method of the surface free energy determination are the contact angle measurements. There are several empirical methods useful to calculate the surface free energy of solids. They are based on the measurements of the contact angle of liquids with the defined surface tension. The aim of this paper is to examine the significance of the receding contact angle measurements in the determination of surface free energy of solids.
    Źródło:
    Annales Universitatis Mariae Curie-Skłodowska, sectio AA – Chemia; 2018, 73, 1; 61-80
    2083-358X
    Pojawia się w:
    Annales Universitatis Mariae Curie-Skłodowska, sectio AA – Chemia
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Surface properties of the doped silica hydrophobic coatings deposited on plasma activated glass supports
    Autorzy:
    Chodkowski, Michał
    Terpiłowski, Konrad
    Goncharuk, Olena
    Powiązania:
    https://bibliotekanauki.pl/articles/110289.pdf
    Data publikacji:
    2019
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    hydrophobicity
    surface chemistry
    glass
    silica
    sol-gel method
    immersion
    plasma
    Opis:
    The paper discusses preparation and characteristics of silica hydrophobic layers deposited on the plasma-modified glass supports. The surfaces were investigated using wettability measurements, profilometry, photoacoustic and infrared spectroscopy, X-ray photoelectron spectroscopy as well as scanning electron microscopy. The wettability measurements showed that the obtained surfaces are hydrophobic – the water contact angle was in the range of 140-150 degrees. The photoacoustic and infrared spectroscopy as well as X-ray photoelectron spectroscopy disclosed the surface compositions, particularly that of the hydrophobic alkyl groups deposited on them. They were methyl groups introduced during hydrophobization by hexamethyldisilazane. In addition, it was found that the number of groups on the surface depends on the kind of plasma by which the supports were activated. The optical profilometer showed differences in the surface roughness which affects their hydrophobicity. Moreover, the surface free energies were determined using the contact angle hysteresis method. They disclosed differences in each surface, depending on the way of supports activation. The largest hydrophobicity was obtained on the layer deposited on the support activated by the argon plasma. However, support activation by the air plasma resulted in a decrease of hydrophobicity compared to that of the non-activated surface.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2019, 55, 6; 1450-1459
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Fabrication of transparent polysiloxane coatings on a glass support via the sol-gel dip coating technique and the effect of their hydrophobization with hexamethyldisilazane
    Autorzy:
    Chodkowski, Michał
    Terpiłowski, Konrad
    Pasieczna-Patkowska, Sylwia
    Powiązania:
    https://bibliotekanauki.pl/articles/1450109.pdf
    Data publikacji:
    2020
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    silica
    coating
    hydrophobization
    wettability
    HMDS
    bubbler
    Opis:
    This study aimed at synthesis, preparation, and physicochemical properties investigation of undoped polysiloxane-based coatings deposited on the glass supports. The other goal was to test the effectiveness of their hydrophobization with hexamethyldisilazane at an elevated temperature using a bubbler. The coatings were obtained in a sol-gel process by acid-assisted hydrolysis of tetraethoxysilane and they were applied to the glass supports using the dip coating technique with various withdrawal speeds. The synthesized composition was scanned using TurbiscanLAB and its particle size was determined by means of the dynamic light scattering technique. The obtained surfaces were examined based on the water wettability measurements, photoacoustic spectroscopy, and transmittance measurements. It was found that the stability of the sol did not change during the dip-coating. Smooth, homogeneous, uniform, hydrophobic, and transparent coatings on the glass supports were obtained. Their wettability was determined by the contact angle in the range from 83.5 to 95.2 degrees and very low contact angle hysteresis. The hydrophobic effect obtained by modification with hexamethyldisilazane appears to be permanent – the contact angles do not change significantly after 7 days. The synthesized sol composition appears to be a good starting point for its chemical and physical modification for hydrophobicity increase and surface properties modification. Moreover, the hydrophobization of the coatings with hexamethyldisilazane at an elevated temperature using the bubbler did not have the desired effect.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2020, 56, 6; 76-88
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-4 z 4

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