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Wyświetlanie 1-6 z 6
Tytuł:
High temperature wettability and reactivity between molten Mg in contact with Ni substrate
Wysokotemperaturowe badania zwilżalności i reaktywności ciekłego Mg w kontakcie z podłożem Ni
Autorzy:
Kudyba, A.
Sobczak, N.
Turalska, P.
Bruzda, G.
Makaya, A.
Pambaguian, L.
Powiązania:
https://bibliotekanauki.pl/articles/391589.pdf
Data publikacji:
2018
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Odlewnictwa
Tematy:
sessile drop
wettability
reactivity
metal matrix composites (MMC)
kropla leżąca
zwilżalność
reaktywność
kompozyty o osnowie metalicznej (MMC)
Opis:
The paper focuses on the experimental investigation of high temperature wetting behaviour of liquid pure Mg during a contact heating on Ni substrate by the sessile drop method. High temperature wettability test was performed by the classical sessile drop method at T = 700°C for t = 300 s, under flowing Ar 99.999% atmosphere, by using the equipment and testing procedures that have been developed by the Foundry Research Institute. In order to suppress effects of heating and cooling histories on wetting and spreading behaviours, Mg/Ni couple was introduced inside a metallic heater already preheated up to the test temperature, while after the wettability test, it was immediately removed to the cold part of the chamber. During the wettability test, images of the couple were recorded by high-resolution high-speed CCD camera. It was observed, that the wetting phenomenon (θ ≤ 90°) takes place immediately after melting of Mg sample. The Mg/Ni system shows a good wetting at T = 700°C after t = 300 s forming the final contact angle of 18°.
Praca prezentuje wyniki badań wysokotemperaturowego oddziaływania ciekłego Mg w kontakcie z podłożem Ni podczas wspólnego nagrzewania badanej pary materiałów. Wysokotemperaturowe badania zwilżalności przeprowadzono klasyczna metodą kropli leżącej w temperaturze T = 700°C i czasie t = 300 s w gazie przepływowym Ar 99,999%. Do badań zastosowano aparaturę i procedury badawcze opracowane w Instytucie Odlewnictwa. W celu eliminacji wpływu historii nagrzewania i chłodzenia na zwilżalność i rozpływność, badany układ Mg/Ni wprowadzono do gorącej części komory badawczej nagrzanej do temperatury badań. Po badaniach zwilżalności badaną parę materiałów natychmiast wprowadzono do zimnej części komory badawczej. Podczas badań zwilżalności stosowano ciągłą rejestrację obrazu badanej pary materiałów za pomocą wysokorozdzielczej kamery cyfrowej CCD. Zaobserwowano, że zjawisko zwilżania (θ ≤ 90°) zachodzi natychmiast po stopieniu próbki czystego Mg. Układ Mg /Ni wykazuje bardzo dobrą zwilżalność w temperaturze T = 700° C po t = 300 s, a końcowa wartość kąta zwilżania wynosi 18°.
Źródło:
Prace Instytutu Odlewnictwa; 2018, 58, 1; 47-53
1899-2439
Pojawia się w:
Prace Instytutu Odlewnictwa
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Influence of Alloying Additions on High Temperature Interaction Between Molten Compacted Graphite Iron and Alumina
Autorzy:
Sobczak, N.
Bacior, M.
Turalska, P.
Bruzda, G.
Homa, M.
Sobczak, J. J.
Powiązania:
https://bibliotekanauki.pl/articles/354903.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
compacted graphite iron
Al2O3
sessile drop method
wettability
interface
Opis:
High temperature behavior of three compacted graphite iron (CGi) alloys on polycrystalline aluminasubstrates (99.7%, porosity <3%) were examined by the sessile drop method combined with classical contact heating procedure in flowing Ar. High-speed high-resolution CCd camera was used for continuous recording of the CGi/Al2 O3 couples during melting alloy, heating to and holding the couples at the test temperature of 1450°C for 15 min and their subsequent cooling. The comparative studies were made with conventional CGi (in wt.%: 3.70 C, 2.30 Si, 0.44 Mn, 0.054 P, 0.017 Mg, 0.015 S) and two alloys additionally containing the same amounts of 0.25 Mo, 0.1 V, 0.045 Sn and 0.032 Sb with different concentrations of Mg + Cu additions, i.e. 0.01Mg + 0.33Cu and 0.02Mg + 0.83Cu. All three CGi alloys demonstrated non-wetting behavior on the Al2 O3 substrates while the contact angle values slightly decreased with increase of the Mg + Cu content in the alloy, i.e. 131° (unalloyed CGi), 130° (0.01Mg + 0.33Cu) and 125° (0.02Mg + 0.83Cu). Structural characterization of solidified couples by light microscopy and scanning electron microscopy coupled with energy dispersive X-ray spectroscopy revealed: 1) heterogeneous nucleation of discontinuous graphite layer at the drop-side interfaces and on the surface of the drops; 2) reactively formed Mg-rich oxide layer at the substrate-side interface; 3) the formation of satellite droplets on the surface of the drops during their solidification; 4) degeneration of initially compacted graphite to lamellar graphite after remelting and subsequent solidification of the drops, particularly in their surface layer.
Źródło:
Archives of Metallurgy and Materials; 2020, 65, 3; 1227-1238
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Thermophysical properties of selected vermicular graphite cast iron alloy
Autorzy:
Homa, M.
Sobczak, N.
Turalska, P.
Bruzda, G.
Bacior, M.
Warmuzek, M.
Polkowska, A.
Powiązania:
https://bibliotekanauki.pl/articles/391848.pdf
Data publikacji:
2017
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Odlewnictwa
Tematy:
vermicular cast iron
thermophysical properties
transformation temperatures
melting heat
thermal expansion
thermal expansion coefficient
thermal diffusivity
thermal conductivity
Opis:
The paper presents the results of thermophysical properties of selected vermicular graphite cast iron with nominal chemical composition of 3.70 C; 2.30 Si; 0.44 Mn; 0.054 P; 0.015 S; 0.017 Mg (wt. %). The comparative studies of the alloy were performed using differential scanning calorimetry, dilatometry and laser flash analysis. The calorimetric investigations proved that upon the heating to melting temperature (~1200°C), four endothermic transformations take place: 1) ferromagnetic → paramagnetic at 742°C, 2) pearlite → austenite at 824.2°C, 3) allotropic transformation of bcc ferrite to fcc austenite at 802°C, 4) melting at 1173.1°C. The character of the dilatometric curve shows small deviation at the temperature above 810°C corresponding to the pearlite → austenite transformation. The values of thermal diffusivity and thermal conductivity change throughout the entire examined temperature range. Both curves showed a changeover from negative to positive trends between 700 and 800°C. This effect might be associated with the pearlite → austenite transformation.
Źródło:
Prace Instytutu Odlewnictwa; 2017, 57, 4; 345-350
1899-2439
Pojawia się w:
Prace Instytutu Odlewnictwa
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Wettability, reactivity and interfaces in the Gd/TiO2 system
Autorzy:
Turalska, P.
Homa, M.
Nowak, R.
Bruzda, G.
Sobczak, N.
Kaban, I.
Mattern, N.
Eckert, J.
Powiązania:
https://bibliotekanauki.pl/articles/391614.pdf
Data publikacji:
2017
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Odlewnictwa
Tematy:
Gd
TiO2
sessile drop
wettability
reactivity
interfaces
Opis:
High-temperature interaction of liquid Gd in contact with dense, polycrystalline TiO2 substrate, was investigated. Wettability and reactivity tests were carried out at two different temperatures (1362°C and 1412°C) in flowing gas (Ar, 850−900 hPa) using the sessile drop method and classical contact heating of the examined couple of materials. The procedure was combined with a drop pushing procedure. During high temperature studies, images of the Gd/TiO2 couple were continuously recorded by a high-resolution CCD camera. The results of wettability tests of liquid gadolinium on titanium dioxide substrate show that the Gd/TiO2 system is non-wettable at both test temperatures (in either case the final contact angle was 100°). The results of structure examinations on the cross-sectioned samples show the dissolution of the TiO2 substrate in liquid Gd and the presence of two sublayers at the drop/substrate interface: Gd2TiO5 (from the drop side) and Gd2Ti2O7 (from the substrate side).
Źródło:
Prace Instytutu Odlewnictwa; 2017, 57, 4; 303-308
1899-2439
Pojawia się w:
Prace Instytutu Odlewnictwa
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Wetting behavior of Si-13.5B alloy on polycrystalline h-BN-based substrates
Autorzy:
Polkowski, W.
Sobczak, N.
Nowak, R.
Kudyba, A.
Bruzda, G.
Polkowska, A.
Homa, M.
Turalska, P.
Shuleshova, O.
Kaban, I.
Powiązania:
https://bibliotekanauki.pl/articles/391820.pdf
Data publikacji:
2017
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Odlewnictwa
Tematy:
silicon-boron alloys
hexagonal boron nitride
wettability
interfaces
AMADEUS Project
Opis:
In this work, for the first time the results of an experimental evaluation of the high temperature behavior of molten Si-B alloy in contact with refractory materials at temperatures up to 1750°C, under static argon atmosphere (p = 850– 900 mbar), is shown. The material investigated, having a nominal chemical composition of Si-13.5B (at. %), was fabricated by using the crucible-less electric arc-melting process assisted by the levitation drop method. The wettability of the molten alloy in contact with commercial hexagonal boron nitride (h-BN) substrates was evaluated by means of especially developed sessile drop technique combined with a contact heating procedure. It was found that both couples show a lack of wettability in the whole tested temperature range (the measured contact angle was θ > 130°). The more stable behavior in contact with molten Si-13.B alloy, evidenced by higher θ values and a lack of drop vibration during the high temperature exposition, was observed for the h-BN based composite substrate.
Źródło:
Prace Instytutu Odlewnictwa; 2017, 57, 4; 321-326
1899-2439
Pojawia się w:
Prace Instytutu Odlewnictwa
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Wetting transparency of graphene deposited on copper in contact with liquid tin
Autorzy:
Sobczak, N.
Sobczak, J. J.
Kudyba, A.
Homa, M.
Bruzda, G.
Grobelny, M.
Kalisz, M.
Strobl, K.
Singhal, R.
Monville, M.
Powiązania:
https://bibliotekanauki.pl/articles/391530.pdf
Data publikacji:
2014
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Odlewnictwa
Tematy:
graphene
liquid tin
sessile drop
wetting transparency
liquophilic
liquophobic
Opis:
Wetting behavior of liquid Sn (99.99%) on graphenecoated Cu substrate was investigated by the sessile drop method using two testing procedures: 1) classical contact heating (CH) of a couple of materials; 2) capillary purification (CP) allowing non-contact heating accompanied with squeezing the Sn droplet through a hole in an alumina capillary. The tests were performed in vacuum (p < 1.80 × 10-6 mbar) at 360 °C for 300 s. The images of Sn/substrate couples were recorded by high-resolution high-speed CCD camera. The results of this study evidenced that graphene layer is transparent for liquid Sn and after 300 s interaction, it forms the contact angles (θ) similar to those on pure Cu substrates, both in CH (θ = 59°) and CP (θ = 32°) tests. However, with liquid Sn, apparently the same effect of graphene wetting transparency is more complicated than that with water and it is caused by different mechanism, most probably, accompanied with reconstruction of the graphene layer.
Źródło:
Prace Instytutu Odlewnictwa; 2014, T. 54, nr 3, 3; 3-11
1899-2439
Pojawia się w:
Prace Instytutu Odlewnictwa
Dostawca treści:
Biblioteka Nauki
Artykuł
    Wyświetlanie 1-6 z 6

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