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Tytuł:
Nickel Composite Coatings Reinforced Nano SiC Particles
Autorzy:
Nowak, M.
Mizera, J.
Kłyszewski, A.
Dobkowska, A.
Boczkal, S.
Kozik, A.
Koprowski, P.
Powiązania:
https://bibliotekanauki.pl/articles/356955.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
nanoparticles
organic additives
SiC
composite coatings
nickel coatings
zeta potential
Opis:
The paper presents the results of the electrodeposition of nickel composite coatings reinforced with the nano size SiC ceramic particles. The type and size of the ceramic particles or organic additives used play a important role during electrodeposition processes. A Watts type galvanic bath with various organic additives was used. These additives were: 2-sulfobenzoic acid imide, dioctyl sulfosuccinate sodium salt (DSS), sodium dodecyl sulfate, tris (hydroxymethyl) aminomethane and hexamethyldisilizane. The nickel composite coating was electrodeposited on a 2xxx aluminum alloy series substrate (EN-AW 2017) with zinc interlayer. The work concerns the determination of the impact of the change in the zeta potential of SiC nanoceramic particles used on properties of composite coatings (wear resistance, corrosion, etc.). The paper characterized the composite nickel coatings on aluminum alloy using SEM techniques, wear resistance tests by TABER method and coating adhesion to the substrate using the “scratch test” method. The corrosion resistance of coatings was also tested using electrochemical methods. The research allowed to determine the effect of SiC nanoceramic particle size on the value of the zeta potential in the model KCl solution.
Źródło:
Archives of Metallurgy and Materials; 2020, 65, 2; 935-940
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Effect of Rare Earth Addition on Microstructure and Mechanical Properties of the Rapidly Solidified Al-Si and Al-Si-Ni Alloys
Autorzy:
Kapinos, D.
Szymanek, M.
Augustyn, B.
Boczkal, S.
Szymański, W.
Tokarski, T.
Lelito, J.
Powiązania:
https://bibliotekanauki.pl/articles/353569.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
aluminium alloy
rapid solidification
grain refinement
ultrafine structure
Opis:
The article presents research aimed at determining the effect of adding rare earth elements to near-eutectic Al-Si and Al-Si-Ni alloys on the microstructure and mechanical properties of the obtained products. Material for the research was prepared using a melt spinner - a device used for rapid crystallization, casting thin ribbons, which were then subjected in subsequent stages to fragmentation, consolidation and plastic working. The ribbons and extruded rods cast were described in terms of their structure and their strength properties were determined at different measurement temperatures. It was shown that the lightweight materials produced from aluminium alloys using the rapid solidification process have an ultra-fine structure and good strength properties. Analysis under a microscope confirmed that the addition of rare earth alloys Al-Si and Al-Si-Ni causes fragmentation of the microstructure in the tapes produced. The presence of rare earth elements in the alloys tested has an impact on the type and the morphology of the particles of the microstructure’s individual components. In addition to the change in particle morphology, the phenomenon of the separation of numerous nanometric particles of intermetallic phases containing rare earth elements was also observed. The change in microstructure caused by the addition of rare earth elements in the form of a mischmetal increases the mechanical properties.
Źródło:
Archives of Metallurgy and Materials; 2020, 65, 1; 185-192
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Application of X-Ray Diffraction to Analyse Phase Composition of Aluminium Alloys for Plastic Working
Autorzy:
Pachut, K.
Żelechowski, J.
Boczkal, S.
Powiązania:
https://bibliotekanauki.pl/articles/354144.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
aluminium alloys
X-ray diffraction
qualitative phase analysis
Opis:
An attempt was made to determine phase composition of commercial aluminium alloys using X-ray diffraction. Samples for phase composition analysis were selected from the group of aluminium alloys covered by the EN 573-3:2013 standard [1]. Representative samples were taken from eight groups of alloys with different chemical composition (at least one sample from each group). The diffraction intensity was measured with a standard X-ray diffractometer in Bragg-Brentano geometry in a way that allowed identification of the weakest diffraction peaks. As a results of the performed research it has been shown that X-ray phase analysis can be used to identify the matrix of aluminium alloys, Si and crystalline intermetallic phases such as Mg2Si, Al93.38Cu6.02Fe24Si16.27, Al4.01MnSi0.74, MgZn2, Al17 (Fe3.2Mn0.8)Si2, Al65Cu20Fe15, and Cu3Mn2Al. The detectability limit of the above-mentioned phases is better than 0.5%. The research has also shown that X-ray phase analysis is applicable in the investigation of phase transformations taking place in aluminium alloys.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 4; 1315-1319
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Various Organic Additives in Galvanic Bath on Properties of Ni-SiC Composite Coatings
Autorzy:
Nowak, M.
Mizera, J.
Kłyszewski, A.
Dobkowska, A.
Boczkal, S.
Kozik, A.
Koprowski, P.
Powiązania:
https://bibliotekanauki.pl/articles/357020.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
organic additives
SiC
composite coatings
nickel coatings
zeta potential
Opis:
The paper presents the results of the electrodeposition of nickel composite coatings reinforced with the ceramic SiC particles. A Watts type galvanic bath modified with various organic additives was used. These additives were: 2-sulfobenzoic acid imide (LSA), dioctyl sulfosuccinate sodium salt (DSS), sodium dodecyl sulfate (SDS), tris (hydroxymethyl) aminomethane (THAM) and hexamethyldisilizane (HMDS). The nickel composite coating was electrodeposited on a 2xxx aluminum alloy series substrate (EN-AW 2017) with zinc interlayer. Studies concerned the effect of the applied organic additives on properties of composite coatings such as: microstructure, microhardness, adhesion to the substrate, corrosion resistance and roughness. The structure of the coatings was assessed by scanning electron microscopy and light microscopy. Based on the studies of zeta potential it was found that the bath modification had a significant impact on the amount of the ceramic phase embedded in metal matrix. The tests conducted in a model 0.01 M KCl solution were not fully representative of the true behavior of particles in a Watts bath.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 4; 1327-1333
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Influence of Plastic Forming Processes on the Dissolution Rate of Biocompatible Mg Alloys
Autorzy:
Boczkal, S.
Karaś, M.
Korczak, P.
Kapinos, D.
Koprowski, P.
Szymański, W.
Wroński, S.
Powiązania:
https://bibliotekanauki.pl/articles/355548.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
MgLiCaZn alloys
biomaterials
structure
properties
immersion test
Opis:
The effect of plastic deformation process on the dissolution rate of biocompatible Mg alloys was investigated. Two biocompatible MgLi1Ca0,2Zn1 and MgLi1Ca1Zn1 alloys were selected for the study. The alloys were deformed on a 100T press at a temperature of 350°C by conventional extrusion and by the equal channel angular extrusion process (ECAE). The grain size analysis showed a high degree of the grain refinement from approximately 110 mm in the initial state to 2.8 mm after the 3rd pass of the ECAE process. Compared to as-cast state, the degree of strengthening has increased after plastic forming. The results of biodegradation tests have shown a significant increase in corrosion rate after both conventional extrusion and ECAE, although after subsequent ECAE passes, this rate was observed to slightly decrease in the MgLi1Ca1Zn1 alloy. Based on the results of macro- and microstructure examinations, the corrosion progress in samples after the extrusion process was described.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 3; 997-1004
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Conversion and polymer-based coatings as strategies to increase corrosion resistance of biodegradable magnesium-calcium alloys
Autorzy:
Karaś, M.
Boczkal, S.
Domalik-Pyzik, P.
Powiązania:
https://bibliotekanauki.pl/articles/285944.pdf
Data publikacji:
2017
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Polskie Towarzystwo Biominerałów
Tematy:
magnesium-calcium alloys
biodegradation
coatings
Źródło:
Engineering of Biomaterials; 2017, 20, no. 143 spec. iss.; 78
1429-7248
Pojawia się w:
Engineering of Biomaterials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Diversification of Intermetallic Zn Phases Growth on Steel During Hot-Dip Galvanizing
Autorzy:
Węgrzynkiewicz, S.
Jędrzejczyk, D.
Szłapa, I.
Hajduga, M.
Boczkal, S.
Powiązania:
https://bibliotekanauki.pl/articles/352256.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
hot-dip zinc galvanizing
heat-affected zone
softening annealing
oxy-acetylene cutting
Opis:
The steel substrate formed as the result of oxy-acetylene cutting (OAB) was treated differently - using: softening annealing, grinding and electro-polishing. Investigations were focused on the influence of additional processing on the structure and corrosion resistance of the deposited zinc coating. The hot - dip Zn galvanizing process was conducted in industrial conditions. Parameters were fixed: temperature 457 °C, dipping time 150 s. The coating thickness diversification dependent on the sub-surface steel structure was analysed and compared to the previous results. The correlation between conducted treatment and coatings morphology was determined.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 2A; 515-520
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Al2O3 Ceramic Particles on Corrosion Behaviour and Tribological Properties of Nickel Composite Coatings
Autorzy:
Nowak, M.
Najder, A.
Opyrchał, M.
Boczkal, S.
Żelechowski, J.
Bigaj, M.
Gawlik, M.
Powiązania:
https://bibliotekanauki.pl/articles/354798.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
composite coating
Al2O3
corrosion resistance
tribological properties
Opis:
The paper presents a study on corrosion behaviour and tribological properties of nickel composite coatings deposited by electrochemical method on aluminium alloy from 2xxx series (AlCu4MgSi). The nickel composite coatings were produced in a Watts bath of the following chemical composition: NiSO4·7H2O 150 g/l, NiCl2·6H2O 30 g/l, H3BO3 30 g/l with the addition of saccharin in an amount of 2 g/l. As hard ceramic dispersed particles embedded in the coating, alumina (Al2O3) was used in an amount of 12,5; 25; 50 and 75 g/l. Coatings were produced using cathodic current density of 6 A/dm2, bath temperature of 60°C, pH 4, and the time 60 minutes. The electroplating bath was stirred with a mechanical stirrer (350 rpm). The results obtained were compared with a nickel coating deposited without the ceramic particles. It was found that the presence of Al2O3 increases the wear resistance of composite coatings, but does not significantly improve the corrosion properties.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 1; 195-198
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of SiC and GR Reinforcement Particles on the Structure and Functional Properties of Composite Casting E43 MMC Reinforced with SiC Particles
Autorzy:
Boczkal, S.
Dolata, A. J.
Nowak, M.
Powiązania:
https://bibliotekanauki.pl/articles/351537.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
aluminium hybrid composite
microstructure
wear tests
Opis:
The aim of the study was to describe the structure of composites based on the AlSi7Mg2Sr0.03 alloy matrix reinforced with SiC particles added in an amount of 10% and with a mixture of SiC and GR particles added in a total amount of 20%. Studies of the composite structure, were carried out by scanning electron microscopy (SEM). Based on the results of chemical analysis in microregions, an increased content of elements such as Mg, O and Si and of the precipitates was observed at the interface. In many places in the examined sample, GR particles formed partly disintegrated conglomerates with well developed boundaries. The effect of the content of particles of the reinforcing phase on the functional properties of the composite was investigated during studies of abrasion. The lowest mass loss of 5,33mg was obtained for the AlSi7Mg2Sr0.03 alloy reinforced with 10% SiC particles.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 1; 399-404
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Heat Treated AZ61 Magnesium Alloy Obtained by Direct Extrusion and Continuous Rotary Extrusion Process
Autorzy:
Bigaj, M.
Boczkal, S.
Żelechowski, J.
Gawlik, M.
Mitka, M.
Powiązania:
https://bibliotekanauki.pl/articles/351751.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
AZ61
heat treatment
Mg17Al12
continuous rotary extrusion process
direct extrusion
Opis:
The results of studies carried out on the heat treated AZ61 magnesium alloy extruded by two methods, i.e. direct extrusion and continuous rotary extrusion, were presented. As part of the work, parameters of the T6 heat treatment were proposed and aging curves were plotted. The solution heat treatment process was accompanied by the grain growth. During artificial aging, due to the decomposition of solid solution, the β-Mg17Al12 phase was precipitated from the supersaturated α solution. It precipitated in a coagulated form at the grain boundaries and in the form of fine-dispersed plates arranged in a preferred direction relative to the grain orientation. Rods obtained by continuous rotary extrusion, unlike those made by the direct process, exhibited a low degree of texturing and lack of anisotropic properties.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 1; 405-410
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of the Sr and Mg Alloying Additions on the Bonding Between Matrix and Reinforcing Particles in the AlSi7Mg/SiC-Cg Hybrid Composite
Autorzy:
Dolata, A. J.
Dyzia, M.
Boczkal, S.
Powiązania:
https://bibliotekanauki.pl/articles/356551.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
hybrid aluminium composites
Mg and Sr modification
solidification
structure
permanent mould casting
Opis:
The aim of the work was to perform adequate selection of the phase composition of the composite designated for permanent - mould casting air compressor pistons. The hybrid composites based on AlSi7Mg matrix alloy reinforced with mixture of silicon carbide (SiC) and glassy carbon (Cg) particles were fabricated by the stir casting method. It has been shown that the proper selection of chemical composition of matrix alloy and its modification by used magnesium and strontium additions gives possibility to obtain both the advantageous casting properties of composite suspensions as well as good bonding between particles reinforcements and matrix.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 2A; 651-656
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Texture and Microtexture of Pure (6N) and Commercially Pure Aluminum after Deformation by Extrusion with Forward-Backward Rotating Die (Kobo)
Autorzy:
Bieda, M.
Boczkal, S.
Koprowski, P.
Sztwiertnia, K.
Pieła, K.
Powiązania:
https://bibliotekanauki.pl/articles/958221.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
pure aluminium
KOBO
texture
EBSD
orientation microscopy
Opis:
Pure aluminium (6N) and commercially pure aluminium (99.7) was deformed by KOBO method. Microstructure and texture of both materials after deformation was analyzed by means of scanning and transmission electron microscopy. Advanced methods of crystallographic orientations measurements like Electron Backscatter Diffraction - EBSD (SEM) and microdiffraction (TEM) was used. Grain size distribution and misorientation between grains in cross and longitudinal sections of the samples were analyzed. Differences in size and homogeneity of the grains were observed in both materials. Pure aluminium was characterized by larger grain size in both sections of extruded material. Whereas commercially pure aluminium reveals smaller grain size and more homogeneous and stable microstructure.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 1; 461-468
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Cathodic Current Density on Microstructure and Properties of Nickel Composite Coatings
Wpływ katodowej gęstości prądu na mikrostrukturę i właściwości niklowych powłok kompozytowych
Autorzy:
Nowak, M.
Opyrchał, M.
Boczkal, S.
Żelechowski, J.
Najder, A.
Karaś, M
Powiązania:
https://bibliotekanauki.pl/articles/353679.pdf
Data publikacji:
2014
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
electrodeposition
current density
composite coatings
Al2O3
elektroosadzanie
gęstość prądu
powłoki kompozytowe
Opis:
Studies were carried out to characterise the nickel composite coatings deposited on a 2xxx series aluminium alloy. The composite coatings were prepared in a Watts bath with the addition of fine-dispersed particles of Al2O3 powder introduced in an amount of 100 g/l using current densities of 2, 4, 6 and 8 A/dm2. The morphology, structure, thickness and microhardness of the obtained composite coatings were described. The volume fraction of Al2O3 particles in composite coating was determined. The corrosion resistance of thus produced coatings was examined. Based on the results of the conducted studies it was stated that all the produced coatings were characterised by good adhesion to the substrate, but coatings produced at high current densities were characterised by a lower content of the Al2O3 reinforcing phase present in the composite.
W pracy przedstawiono badania charakteryzujące kompozytowe powłoki niklowe osadzane na stopie aluminium serii 2xxx. Powłoki kompozytowe wytwarzano w kąpieli Wattsa z dodatkiem drobnodyspersyjnych cząstek proszku AI2O3 w ilości 100 g/l przy zastosowaniu gęstości prądu: 2, 4. 6 oraz 8 A/dm2. Przedstawiono morfologię, strukturę, grubość oraz mikrotwardość uzyskanych powłok kompozytowych. Określono objętościowy udział cząstek AI2O3 w powłoce kompozytowej. Zbadano odporność korozyjną wytworzonych powłok. Na podstawie przeprowadzonych badań stwierdzono, iż wszystkie uzyskane powłoki są dobrze przyczepne do podłoża, jednak powłoki uzyskane przy wyższych gęstościach prądów charakteryzują się niższą zawartością fazy zbrojącej AI2O3 w kompozycie.
Źródło:
Archives of Metallurgy and Materials; 2014, 59, 1; 323-327
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Formation of Structure and Properties in Casting Processes on the Example of AZ91 Magnesium Alloy
Autorzy:
Augustyn, B.
Szymanek, M.
Kapinos, D.
Boczkal, S.
Korczak, P.
Powiązania:
https://bibliotekanauki.pl/articles/383152.pdf
Data publikacji:
2014
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
innovative foundry technologies
innovative foundry materials
magnesium alloy
AZ91 alloy
RS process
mechanical properties
innowacyjne technologie odlewnicze
innowacyjne materiały odlewnicze
stop magnezu
stop AZ91
właściwości mechaniczne
Opis:
Contemporary materials engineering requires the use of materials characterised by high mechanical properties, as these precisely properties determine the choice of material for parts of machinery and equipment. Owing to these properties it is possible to reduce the weight and, consequently, the consumption of both material and energy. Trying to meet these expectations, the designers are increasingly looking for solutions in the application of magnesium alloys as materials offering a very beneficial strength-to-weight ratio. However, besides alloying elements, the properties are to a great extent shaped by the solidification conditions and related structure. The process of structure formation depends on the choice of casting method forced by the specific properties of casting or by the specific intended use of final product. The article presents a comparison of AZ91 magnesium alloys processed by different casting technologies. A short characteristic was offered for materials processed by the traditional semi-continuous casting process, which uses the solidification rates comprised in a range of 5 - 20⁰C/s, and for materials made in the process of Rapid Solidification, where the solidification rate can reach 106⁰C/s. As a result of the casting process, a feedstock in the form of billets and thin strips was obtained and was subjected next to the process of plastic forming. The article presents the results of structural analysis of the final product. The mechanical properties of the ø7 mm extruded rods were also evaluated and compared.
Źródło:
Archives of Foundry Engineering; 2014, 14, 2; 43-48
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of a Substrate Surface on the (Zn) : Coating Formation
Wpływ powierzchni podłoża na kształtowanie się powłoki (Zn)
Autorzy:
Węgrzynkiewicz, S.
Jędrzejczyk, D.
Szłapa, I.
Hajduga, M.
Boczkal, S.
Powiązania:
https://bibliotekanauki.pl/articles/352854.pdf
Data publikacji:
2014
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
hot-dip Zn galvanizing
heat-affected zone (HAZ)
water jet cutting
oxyacetylene cutting
laser cutting
cynkowanie ogniowe Zn
strefa wpływu ciepła (HAZ)
cięcie strumieniem wody
cięcie tlenowo-acetylenowe
cięcie laserem
Opis:
The steel substrate was cut by means of different methods, like water jet, laser or oxyacetylene blowpipe. So, some different surfaces (after cutting / without cutting) were subjected to the (Zn) - hot dip galvanizing. The galvanizing process was performed in industrial conditions by applying the constant temperature equal to 457°C, and a dipping time equal to 150 s. The (Zn) - coating morphologies and sub-layer thicknesses were analyzed to explain some expected differences in the coatings formation.
W prezentowanej pracy podłoże stalowe cięto stosując różne metody: strumień wody, laser, palnik acetylenowo-tlenowy. W wyniku tego otrzymano zróżnicowaną powierzchnię (po cięciu/bez cięcia), która poddano cynkowaniu ogniowemu. Proces cynkowania wykonywano w warunkach przemysłowych stosując stałe parametry: temperaturę 457°C, czas zanurzenia t=150 s. W trakcie badań analizowano morfologię powłoki cynkowej oraz grubości poszczególnych podwarstw w celu wyjaśnienia różnic w narastaniu powłok.
Źródło:
Archives of Metallurgy and Materials; 2014, 59, 4; 1373-1378
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
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