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Tytuł:
A Comparative Study on the Corrosion Behaviour of Gas Nitrided and TiAlN Coated AISI D2 Steel by Thermo-Reactive Diffusion Technique
Autorzy:
Cegil, O.
Sen, U.
Sen, S.
Powiązania:
https://bibliotekanauki.pl/articles/1399731.pdf
Data publikacji:
2013-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.05.Je
81.65.Kn
Opis:
In this study, the corrosion behaviors of nitride and titanium aluminum nitride (TiAlN) layers deposited on AISI D2 steel samples are reported. Steel was at first nitrided in a nitrogen and ammonia atmosphere at 575C for 8 h and then titanium nitride coating treatment was performed in the powder mixture consisting of ferro-titanium, aluminum, ammonium chloride and alumina at 1000C for 2 h by thermo-reactive diffusion technique. Phase analysis and corrosion tests were realized on the titanium aluminum nitride coated steel. The corrosion properties of uncoated and coated samples were characterized by potentiostatic polarization test. The tests were conducted using a three-electrode system test unit with a platinum counter electrode of $2.269 cm^2$ and an Ag/AgCl, 3 M KCl electrode as the reference electrode. Nitrided and TiAlN coated steel specimens exhibited higher corrosion resistance than uncoated steel in 0.5 M $H_2SO_4$ solution. Conclusively, the application of nitride and TiAlN films on AISI D2 steel increased surface hardness and corrosion resistance. TiAlN coating exhibits the highest corrosion resistance.
Źródło:
Acta Physica Polonica A; 2013, 123, 2; 265-267
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
An Electrochemical Study of the Corrosion Resistance of Niobium-Aluminum Carbonitride Coating Produced on Steels by Thermo-Reactive Diffusion Technique
Autorzy:
Abakay, E.
Durmaz, M.
Sen, S.
Sen, U.
Powiązania:
https://bibliotekanauki.pl/articles/1031643.pdf
Data publikacji:
2017-09
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.65.Lp
81.65.Kn
87.64.Ee
Opis:
Thermo-reactive diffusion/deposition technique is an alternative to physical vapor deposition and chemical vapor deposition techniques for obtaining wear and corrosion resistant coatings on steel parts. In this work, thermo-reactive diffusion/deposition technique was used to produce niobium aluminum carbonitride-based coatings on AISI M2 steel. Characterization of the coatings was done by X-ray diffraction analysis, scanning electron microscopy and energy dispersive spectroscopy. The corrosion resistance of the produced coatings was investigated by using potentiodynamic polarization in a solution of 0.5 M NaCl. Hard, compact and adherent coatings, mainly consisting of NbC and NbN phases were obtained. The corrosion behavior of the samples was investigation by potentiodynamic polarization measurements.
Źródło:
Acta Physica Polonica A; 2017, 132, 3; 682-684
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Bond Strength of Basalt Based Glass-Ceramic Coatings
Autorzy:
Bayrak, G.
Ercenk, E.
Sen, U.
Yilmaz, S.
Powiązania:
https://bibliotekanauki.pl/articles/1194582.pdf
Data publikacji:
2014-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.43.Fs
62.20.-x
61.05.cp
Opis:
In the present study, powders produced from the volcanic basalt rocks were coated on pre-coated AISI 1040 steel with Ni-5% Al bond coat by atmospheric plasma spray coating technique. The coated specimens were characterized by optical microscopy, scanning electron microscopy, metallography and X-ray diffraction. Bonding strength of coatings was evaluated in accordance with the ASTM C-633 method. Coated basalt material from the APS coating system was determined in the glassy amorphous state by X-ray diffraction analysis. The coated samples were heat-treated at 800C for 1-4 h for crystallization. The phases formed in the basalt base glass-ceramic coatings were augite, Fe-diopside, anorthite, and andesine which were detected by X-ray diffraction analysis. Basalt based glass-ceramic coatings include splat, porosity and un-melted particles which were the characteristic of plasma sprayed coatings. Experiment result showed that the crystallization time increase caused the decrease of the bond strengths of the coatings.
Źródło:
Acta Physica Polonica A; 2014, 125, 2; 620-622
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Characterization of Fe-Nb-B Base Hardfacing of Steel
Autorzy:
Kilinc, B.
Cegil, O.
Abakay, E.
Sen, U.
Sen, S.
Powiązania:
https://bibliotekanauki.pl/articles/1311693.pdf
Data publikacji:
2014-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.65.Kn
68.55.J-
81.65.Lp
Opis:
Recently hardfacing by welding has become a commonly used technique for improvement of material performance in extreme (high temperature, impact/abrasion, erosion, etc.) conditions. In the present study, three different alloy compositions of the Fe-Nb-B were used for hardfacing of the AISI 1020 steel by tungsten inert gas welding process and analyzed. The coatings were produced from a mixture of ferrous niobium, ferrous boron and iron powders in the range of - 45 μm particle size with different ratio. The coatings' thickness was set to 2-3 mm on the substrate. Microstructure, phase analysis and hardness of the manufactured hardfacing alloys were characterized. Deposition results indicate good quality thick coating and porosity free of the hardfacings. X-ray diffraction analyses showed that the alloyed layers include iron borides, FeNbB and iron phases. It was shown that surface alloyed layer has composite structure including steel matrix and well distributed boride phases.
Źródło:
Acta Physica Polonica A; 2014, 125, 2; 656-658
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Corrosion Behavior of Nitride and Cr-Al-N Coatings Formed on AISI D2 Steel
Autorzy:
Kılınc, B.
Demirkiran, S.
Sen, U.
Sen, S.
Powiązania:
https://bibliotekanauki.pl/articles/1399749.pdf
Data publikacji:
2013-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.65.Kn
68.55.J-
81.65.Lp
Opis:
In the present work, the corrosion behavior of Cr-Al-N coating formed on the pre-nitrided AISI D2 cold work tool steel by thermo-reactive diffusion technique in the powder mixture consisting of ferro-chromium, aluminum, ammonium chloride and alumina at 1000C for 2 h was investigated. The phases formed in the coating layers were $Cr_2N$, $(Cr,Fe)_2N_{1-x}$, $AlN$, and $Fe_2N$ which were confirmed by X-ray diffraction analysis. The uncoated, nitrided, and Cr-Al-N coated specimens were placed in corrosive media (3.5 wt% salt solution). A standard saturated calomel electrode was used as a reference and graphite as a counter or auxiliary electrode. The effectiveness of the coatings in preventing corrosion was tested in the NaCl solution by electrochemical impedance studies using the Nyquist plots and potentiodynamic studies as well. Conclusively, the application of nitride and Cr-Al-N layers on AISI D2 steel increased its surface hardness and corrosion resistance. The corrosion resistance of Cr-Al-N coatings is higher than that of uncoated and nitrided steels.
Źródło:
Acta Physica Polonica A; 2013, 123, 2; 268-270
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Corrosion Properties of CrAlN and TiAlN Coatings Deposited by Thermoreactive Deposition Process
Autorzy:
Cegil, O.
Kılınc, B.
Sen, S.
Sen, U.
Powiązania:
https://bibliotekanauki.pl/articles/1194669.pdf
Data publikacji:
2014-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
82.45.Bb
81.65.Kn
81.15.-z
Opis:
In the present study, the corrosion behaviors of chromium aluminum nitride (CrAlN) and titanium aluminum nitride (TiAlN) coatings deposited on AISI D2 steel samples are reported. Steel samples were pre-nitrided at 575C for 8 h in the first step of the coating process, and then TiAlN and CrAlN coatings were performed by thermoreactive deposition process in a powder mixture consisting of alumina, ammonium chloride, aluminum and ferrous titanium or ferrous chromium for TiAlN or CrAlN, respectively. Coating treatments were realized at 1000C for 2 h. Coated samples were characterized by X-ray diffraction analysis, optical microscopy, scanning electron microscopy, and microhardness tester. The corrosion properties of uncoated and coated samples were characterized by potentiostatic polarization test. CrAlN and TiAlN coated steel specimens exhibited the higher corrosion resistance than uncoated steels in a 0.5 M NaCl solution.
Źródło:
Acta Physica Polonica A; 2014, 125, 2; 359-361
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of aluminum addition to Nb-Al-C-N coatings on AISI M2 steel obtained by thermo-reactive deposition technique
Autorzy:
Abakay, E.
Sen, S.
Sen, U.
Powiązania:
https://bibliotekanauki.pl/articles/1061918.pdf
Data publikacji:
2016-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.40.Gh
81.40.Ef
62.20.Qp
81.05.-t
Opis:
In this study, aluminum-doped (1 and 2 wt.%) and Al-free niobium carbo-nitride coatings were applied to the surface of AISI M2 high speed steel using the process of thermo-reactive deposition technique (TRD) at 1000°C during 1-4 h. The obtained coatings were characterized by scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDS), X-ray diffraction (XRD) analysis and micro hardness test. Nb-Al-C-N layers were compact and homogeneous. X-ray diffraction analysis has shown that the major phases formed in the coating layer are Nb₂CN and NbN. The depth of the coating layer had increased with the treatment time and ranged from 6.65 to 9.05 μm. The measured values of the hardness of the coating layers were ranging between 2136 and 2636 HK_{0.005}.
Źródło:
Acta Physica Polonica A; 2016, 129, 4; 653-655
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of combinations of intravenous small-volume hypertonic sodium chloride, acetate Ringer, sodium bicarbonate, and lactate Ringer solutions along with oral fluid on the treatment of calf diarrhea
Autorzy:
Aydogdu, U.
Yildiz, R.
Guzelbektes, H.
Naseri, A.
Akyuz, E.
Sen, I.
Powiązania:
https://bibliotekanauki.pl/articles/2087718.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
calves
diarrhea
metabolic acidosis
fluid therapy
Źródło:
Polish Journal of Veterinary Sciences; 2018, 21, 2; 273-280
1505-1773
Pojawia się w:
Polish Journal of Veterinary Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of H₃BO₃ on the Corrosion Properties of Ni-B Based Electroplating Coatings
Autorzy:
Karabulut, A.
Durmaz, M.
Kilinc, B.
Sen, U.
Sen, S.
Powiązania:
https://bibliotekanauki.pl/articles/1032526.pdf
Data publikacji:
2017-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.15.Pq
Opis:
In this study the effect of H₃BO₃ on the properties of Ni-B coating formed on the AISI 1020 steel surface produced with electroplating process was investigated. Synthesis of the coatings was done using acidic electro plating bath. Coating process was carried out within a standard cell with three electrode system using platinum as auxiliary and Ag/AgCl electrode as a reference electrode onto AISI 1020 steel substrate. Then, heat treatment was applied to coatings at 400°C during a period of 1 h. The coated samples were analyzed by optical microscope, scanning electron microscope, and X-ray diffraction. Micro hardness measurements of the coatings were realized. The study reveals that the Ni-B anti corrosion coating is amorphous in their as-plated condition and upon heat treatment at 400°C for 1 h, Ni-B coatings crystallize and produce nickel borides and nickel in the coatings. The results indicated the presence of Ni₂B, Ni₃B and Ni phases.
Źródło:
Acta Physica Polonica A; 2017, 131, 1; 147-149
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effects of B₂O₃ Addition on the Sintering Behavior of 0-5-10% ZrO₂ Doped BaTiO₃ Based Ceramics
Autorzy:
Öksüz, K.
Şen, Ş.
Şen, U.
Powiązania:
https://bibliotekanauki.pl/articles/1401289.pdf
Data publikacji:
2015-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
77.84.Cg
77.84.-s
Opis:
In this study, the effect of B₂O₃ addition on the sintering behavior of 0-5-10% ZrO₂ doped barium titanate based microwave dielectric ceramics were investigated. For this purpose, the powder mixtures consisting of BaCO₃, TiO₂ and ZrO₂ were prepared by ball milling technique in alcohol using ZrO₂ balls at 200 cycle/min for 20 h. The prepared powders were calcined at 900°C for 2 h. Produced powders were mixed 0.5% B₂O₃ and 5% PVA and pressed as green body under the pressure of 100 MPa. The disc-shaped die-pressed samples were sintered at 1250°C, 1350°C and 1450°C for 4 h. X-ray diffraction analysis showed that the main phases formed in the sintered samples are BaTiO₃ and $Ba(Ti_{1-x}Zr_{x})O_3$. The scanning electron microscope (SEM) and energy-dispersive X-ray spectroscopy (EDS) were used to investigate microstructure of the sintered samples. The bulk densities of the sintered samples increased with the addition of B₂O₃ content due to the low number of pores trapped between the grains.
Źródło:
Acta Physica Polonica A; 2015, 127, 4; 1086-1089
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Glass and Glass-Ceramics Produced from Fly Ash and Boron Waste
Autorzy:
Ercenk, E.
Sen, U.
Bayrak, G.
Yilmaz, S.
Powiązania:
https://bibliotekanauki.pl/articles/1181592.pdf
Data publikacji:
2014-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.43.Fs
64.70.P-
61.05.cp
81.70.Pg
62.20.Qp
Opis:
In the current study, the effect of boron waste addition on some properties of fly ash based glass and glass-ceramics were investigated. The powder compositions including 10, 30, and 50 wt% boron waste was prepared. All the investigated compositions were melted at 1500C by using electrical furnaces. Melting structures were cast into the graphite mold. Thus, fly ash-boron waste based glass materials were produced. To transform the glass-ceramic, crystallization process was performed. Crystallization and glass-transition temperatures were determined by differential thermal analysis. Highly dense and crystalline materials, predominantly composed of diopside and augite together with tincalconite and residual glassy phase, were detected by X-ray diffraction analysis after heat treatment at 800, 900, and 1000C for 1 h. For the glass and glass-ceramic samples, mechanical tests such as hardness and fracture toughness were realized. A boron waste addition has a positive effect on the hardness of the specimens unlike the fracture toughness results. Furthermore, produced glass-ceramic materials were characterized via scanning electron microscopy.
Źródło:
Acta Physica Polonica A; 2014, 125, 2; 626-628
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of ZrO₂ Addition on the Structure and Dielectric Properties of BaTiO₃ Ceramics
Autorzy:
Oksuz, K.
Sen, S.
Sen, U.
Powiązania:
https://bibliotekanauki.pl/articles/1032539.pdf
Data publikacji:
2017-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
85.50.-n
77.84.-s
82.45.Xy
81.30.-t
Opis:
Ba(Ti_{1-x}Zr_{x})O₃ (x=0÷0.3) ceramics were prepared by the standard solid state reaction method and were sintered at 1450°C for 4 h. The structural and dielectric properties of the samples were studied. The phases formed in the ZrO₂ doped BaTiO₃ were tetragonal and of cubic symmetry. Increase in ZrO₂ content in the BaTiO₃ caused to increase of the lattice parameter and crystallite size of the perovskite structure. The evolution of the Raman spectra was studied for various compositions and the spectroscopic signature of the corresponding phase was determined. The scanning electron microscope was used to investigate the microstructure and surface morphology of the sintered samples. Scanning electron microscope observations revealed enhanced microstructural uniformity and retarded grain growth with increase of ZrO₂ content. Dielectric characteristics of ZrO₂ doped barium titanate were studied using a Hioki 3532-50 LCR meter in the frequency range of 1 kHz-1 MHz. It is found that the dielectric constant (ε_{r}) increases while the dielectric loss (tan δ) decreases with increase in zirconium oxide content (x<0.3).
Źródło:
Acta Physica Polonica A; 2017, 131, 1; 197-199
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Maturation of bovine oocytes under low culture temperature decreased glutathione peroxidase activity of both oocytes and blastocysts
Autorzy:
Şen, U.
Powiązania:
https://bibliotekanauki.pl/articles/2087228.pdf
Data publikacji:
2021
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
bovine
temperature
antioxidant activity
oxidative stress
oocytes
blastocysts
Źródło:
Polish Journal of Veterinary Sciences; 2021, 24, 1; 93-99
1505-1773
Pojawia się w:
Polish Journal of Veterinary Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Photocatalytic efficiencies of alternate heterogeneous catalysts: Iron modified minerals and semiconductors for removal of an azo dye from solutions
Autorzy:
Yatmaz, H. C.
Sen, U. D. K.
Powiązania:
https://bibliotekanauki.pl/articles/208158.pdf
Data publikacji:
2018
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
heterogeneous photocatalysis
Fenton process
textile industries
fotokataliza heterogeniczna
proces Fentona
przemysł tekstylny
Opis:
Photocatalytic degradation of reactive dye solutions have been compared using two types of heterogeneous catalysts, i.e., semiconductors and iron modified clays. Decolorization and mineralization efficiencies of the catalysts were performed in a slurry batch reactor with UVA and UVC (365 and 254 nm, respectively) light sources using reactive azo dye solutions. Two natural minerals (zeolites and beidellites) modified with Fe3+, Fe2+and semiconductors (TiO2-P25 and ZnO) were used as photocatalysts. Iron modified minerals produced similar results compared to homogeneous photo-Fenton reactions under UVC radiation. Fe2+-beidellite and Fe3+-zeolite showed the best efficiency for dye removal with 98.5% at 75 min and 96.3% at 90 min, respectively, which is higher than the other iron modified minerals under UVA radiation. ZnO and TiO2 exhibited initial dye removal rates under UVA as 98.9% and 95.5% at 45 min, respectively. Mineralization efficiencies for TiO2, ZnO and Fe2+-beidellite, Fe3+ -zeolite under UVA were 86.2%, 74.5% and 76.9%, 67.8%, respectively. However mineral catalysts performed 99% dye removal rates within 15 min with respect to semiconductor catalyst values (over 97% within 45min) under UVC radiation. Mineral catalysts and TiO2 provided higher initial TOC removal rates as 92% in 60 min under UVC radiation.
Źródło:
Environment Protection Engineering; 2018, 44, 1; 5-17
0324-8828
Pojawia się w:
Environment Protection Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Propagation of Flacourtia jangomas: an approach towards the domestication of wild fruit species in Bangladesh
Autorzy:
Hossain, M.A.
Sen, M.
Jewell, M.I.U.
Kabir, M.A.
Powiązania:
https://bibliotekanauki.pl/articles/40995.pdf
Data publikacji:
2011
Wydawca:
Polska Akademia Nauk. Instytut Dendrologii PAN
Tematy:
propagation
Flacourtia jangomas
domestication
wild species
fruit species
germination
rooting ability
seedling
stem cutting
wild fruit
Bangladesh
Opis:
The study was carried out to investigate the domestication potential of Flacourtia jangomas (Lour.) Raeusch, a wild fruit species in Bangladesh, through nursery raising from seeds and clonal propagation by stem cutting. Air dried seeds were treated with four different pre-sowing treatments i.e., control (T0), seeds soakedin coldwater for 24 h (T1), 48 h (T2), or 72 h (T3) to explore the seedgermination ability of the species. Pre-sowing treatments significantly enhancedthe germination period, germination percentage andbiomass production of seedlings. The early germination (least imbibition period), highest germination percentage (81.3) and total dry biomass (0.52 g) was observed in T2 (seeds soaked in cold water for 48 h) while the lowest germination percentage (53.7) andtotal dry biomass (0.23 g) was observedin T3 andT0 respectively. The plant species was highly amenable for rooting for clonal propagation. However, the rooting ability of cuttings was significantly affectedby the application of IBA. The highest rooting percentage (100), maximum root number (5.63), the longest root length (3.28 cm) andbest survival (85.0%) were obtainedfrom the cuttings treatedwith 0.4% IBA solution followed by 0.2% IBA andthe lowest was in cuttings without treatment. Therefore, pre-sowing treatment ‘soaking of seeds in cold water for 48 h for nursery raising and ‘0.4% IBA treatment’ of stem cuttings for clonal propagation may be recommended for mass production of quality planting stocks for the domestication of the species through homestead agroforestry or in fruit orchards.
Źródło:
Dendrobiology; 2011, 65
1641-1307
Pojawia się w:
Dendrobiology
Dostawca treści:
Biblioteka Nauki
Artykuł

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