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    Wyświetlanie 1-8 z 8
    Tytuł:
    Fabrication and Shape Memory Characteristics of Highly Porous Ti-Nb-Mo Biomaterials
    Autorzy:
    Kim, Y.-W.
    Mukarati, T. W.
    Powiązania:
    https://bibliotekanauki.pl/articles/351933.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Ti-Nb-Mo alloys
    porous scaffolds
    biomedical materials
    shape memory alloys
    Opis:
    Non-toxic Ti-Nb-Mo scaffolds were fabricated by sintering rapidly solidified alloy fibers for biomedical applications. Microstructure and martensitic transformation behaviors of the porous scaffolds were investigated by means of differential scanning calorimetric and X-ray diffraction. The α″ – β transformation occurs in the as-solidified fiber and the sintered scaffolds. According to the compressive test of the sintered scaffolds with 75% porosity, they exhibit good superelasticity and strain recovery ascribed to the stress-induced martensitic transformation and the shape memory effect. Because of the high porosity of the scaffolds, an elastic modulus of 1.4 GPa, which matches well with that of cancellous bone, could be obtained. The austenite transformation finishing temperature of 77Ti-18Nb-5Mo alloy scaffolds is 5.1°C which is well below the human body temperature, and then all mechanical properties and shape memory effect of the porous 77Ti-18Nb-5Mo scaffolds are applicable for bon replacement implants.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1367-1370
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Fabrication Of Porous Ti By Thermal Decomposition And Sintering Of PMMA/TiH2 Powder Compact
    Wytwarzanie porowatego tytanu przez rozkład termiczny i spiekanie wyprasek PMMA/TiH2
    Autorzy:
    Jeon, K. Ch.
    Kim, Y. D.
    Suk, M.-J.
    Oh, S.-T.
    Powiązania:
    https://bibliotekanauki.pl/articles/352341.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    porous Ti
    PMMA powders
    thermal decomposition of TiH2
    pore structure
    porowaty tytan
    PMMA
    rozkład termiczny
    struktura porów
    Opis:
    Porous Ti with controlled pore structure was fabricated by thermal decomposition and sintering process using TiH2 powders and Polymethylmethacrylates (PMMA) beads as pore forming agent. The beads sizes of 8 and 50 μm were used as a template for fabricating the porous Ti. The TiH2 powder compacts with 20 and 70 vol% PMMA were prepared by uniaxial pressing and sintered for 2 h at 1100°C. TGA analysis revealed that the PMMA and TiH2 were thermally decomposed at about 400°C forming pores and at about 600°C into metallic Ti phase. The porosity increased with increase in the amount of PMMA addition. Also, the microstructure observation showed that the pore size and shape were strongly dependent on the PMMA shapes.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1375-1377
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Self-Consolidation Mechanism Of Porous Ti-6Al-4V Implant Prototypes Produced By Electro-Discharge-Sintering Of Spherical Ti-6Al-4V Powders
    Mechanizm autokonsolidacji prototypów porowatych implantów wytworzonych przez spiekanie sferycznych proszków Ti-6Al-4V
    Autorzy:
    Lee, W. H.
    Jo, Y. J.
    Kim, Y. H.
    Jo, Y. H.
    Seong, J. G.
    Van Tyne, C. J.
    Chang, S. Y.
    Powiązania:
    https://bibliotekanauki.pl/articles/356277.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Ti-6Al-4V
    implant
    porous
    sintering
    electrodischarge
    porowatość
    spiekanie
    proszki spiekane
    Opis:
    Electro-Discharge-Sintering (EDS) was employed to fabricate Ti-6Al-4V porous implant prototypes from atomized powders (100 – 150 μm), that were subjected to discharges of 0.75 to 2.0 kJ/0.7g-powder from 150, 300, and 450 μF capacitors. Both fully porous and porous-surfaced Ti-6Al-4V compacts with various solid core sizes were self-consolidated in less than 86 – 155 μsec. It is known that EDS can simultaneously produce the pinch pressure to squeeze and deform powder particles and the heat to weld them together. The formation of a solid core in these prototypes depends on the amounts of both the pinch pressure and heat generated during a discharge. The size of the solid core and the thickness of the porous layer can be successfully controlled by manipulating the discharge conditions such as input energy and capacitance.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1185-1189
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Plasma Electrolytic Oxidation as a modern method to form porous coatings enriched in phosphorus and copper on biomaterials
    Autorzy:
    Rokosz, Krzysztof
    Hryniewicz, Tadeusz
    Powiązania:
    https://bibliotekanauki.pl/articles/1190116.pdf
    Data publikacji:
    2016
    Wydawca:
    Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
    Tematy:
    Plasma Electrolytic Oxidation (PEO)
    Niobium
    Ti6Al4V
    TNZ
    Porous coatings
    Opis:
    In the paper, the porous coatings obtained on niobium and two titanium alloys (Ti6Al4V, and TNZ) after Plasma Electrolytic Oxidation (PEO), known also as Micro Arc Oxidation, were studied. The samples were treated at the voltage of 450 V for 3 minutes in the electrolyte consisting of 300 g and 600 g of copper nitrate Cu(NO3)2 in 1 litre of concentrated phosphoric acid H3PO4, consecutively. SEM and EDS studies were performed on the samples. Based on the obtained results it may be concluded that enriched in copper porous coatings on all studied materials were created in the electrolyte within copper nitrate amounting for 600 g. The proposed by the Authors factor to evaluate the obtained coatings, i.e. copper-to-phosphorus ratio, which for the studied materials amounted to 0.21, clearly indicates that the performed electrochemical PEO treatment for surface modification especially of bioimplants may be advised.
    Źródło:
    World Scientific News; 2016, 35; 44-61
    2392-2192
    Pojawia się w:
    World Scientific News
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect of Controlled Porosity on the Mechanical Properties of Ti-Zr-Sn-Mo Biomedical Alloys
    Autorzy:
    Kim, Yeon-Wook
    Erlangga, Bagus D.
    Do, Dalhyun
    Lee, Seong-Min
    Powiązania:
    https://bibliotekanauki.pl/articles/352474.pdf
    Data publikacji:
    2020
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Ti-Zr-Sn-Mo alloy
    porous scaffolds
    biomedical materials
    shape memory alloys
    Opis:
    In this study, a simple and effective way to fabricate highly porous scaffolds with controlled porosity and pore size is demonstrated. Ti-7Zr-6Sn-3Mo shape memory alloy fibers were prepared through a melt overflow process. The scaffolds with porosity of 65-85% and large pores of 100-700 μm in size were fabricated by sintering the as-solidified fibers. Microstructures and transformation behaviors of the porous scaffolds were investigated by means of SEM, DSC and XRD. The scaffolds were composed of β phase at room temperature. Superelasticity with the superelastic recovery strain of 7.4% was achieved by β↔α”phase transformation. An effect of porosity on mechanical properties of porous scaffolds was investigated by using compressive test. As the porosity increased from 65% to 85%, elastic modulus and compressive strength decreased from 0.95 to 0.06 GPa and from 27 to 2 MPa, respectively.
    Źródło:
    Archives of Metallurgy and Materials; 2020, 65, 4; 1341-1344
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Fabrication and characterisation of porous coatings obtained by plasma electrolytic oxidation
    Autorzy:
    Rokosz, K.
    Hryniewicz, T.
    Raaen, S.
    Malorny, W.
    Powiązania:
    https://bibliotekanauki.pl/articles/95249.pdf
    Data publikacji:
    2017
    Wydawca:
    Politechnika Koszalińska. Wydawnictwo Uczelniane
    Tematy:
    Plasma Electrolytic Oxidation
    PEO
    micro arc oxidation
    MAO
    CP Titanium Grade 2
    niobium
    Ti2448
    Ti6Al4V
    TNZ
    plazmowe utlenianie elektrolityczne
    utlenianie mikro-łukowe
    tytan
    stopy tytanu
    niob
    Opis:
    In the paper, characteristics of porous coatings enriched in copper on pure Titanium and its alloys (NiTi, Ti6Al4V, TNZ, Ti2448) as well as on niobium obtained by Plasma Electrolytic Oxidation (PEO) in electrolyte containing H3PO4 within Cu(NO3)2, are presented. All obtained surfaces of PEO coatings have different shapes and diameters of pores. The binding energies of main peaks for titanium Ti2p3/2, niobium Nb3d5/2, zirconium Zr3d5/2, phosphorus (P2p) and oxygen (O1s) suggest the presence of titanium Ti4+, niobium Nb5+ and zirconium Zrx+ (x≤2) as well as PO4 3–.
    Źródło:
    Journal of Mechanical and Energy Engineering; 2017, 1, 1; 23-30
    2544-0780
    2544-1671
    Pojawia się w:
    Journal of Mechanical and Energy Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Morphology and surface topography of Ti6Al4V lattice structure fabricated by selective laser sintering
    Autorzy:
    Maszybrocka, J.
    Stwora, A.
    Gapiński, B.
    Skrabalak, G.
    Karolus, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/202149.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    metal porous implant
    selective laser sintering
    surface roughness
    X-ray microtomography
    selektywne spiekanie laserowe
    chropowatość powierzchni
    Mikrotomografia
    Opis:
    Construction of metallic implants with a porous structure that mimics the biomechanical properties of bone is one of the challenges of orthopedic regenerative medicine. The selective laser sintering technique (SLS) allows the production of complex geometries based on three-dimensional model, which offers the prospect of preparing porous metal implants, in which stiffness and porosity can be precisely adjusted to the individual needs of the patient. This requires an interdisciplinary approach to design, manufacturing and testing of porous structures manufactured by selective sintering. An important link in this process is the ability to assess the surface topography of the struts of porous structure. The paper presents a qualitative assessment of the surface morphology based on SEM studies and methodology that allows for quantitative assessment of stereometric structure based on micro-tomographic measurements.
    Źródło:
    Bulletin of the Polish Academy of Sciences. Technical Sciences; 2017, 65, 1; 85-92
    0239-7528
    Pojawia się w:
    Bulletin of the Polish Academy of Sciences. Technical Sciences
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Surface Modification of Self-Consolidated Microporous Ti Implant Compacts Fabricated by Electro-Discharge-Sintering in Air
    Autorzy:
    Jo, Y. J.
    Yoon, Y. H.
    Kim, Y. H.
    Chang, S. Y.
    Kim, J. Y.
    Lee, Y. K.
    Van Tyne, C. J.
    Lee, W. H.
    Powiązania:
    https://bibliotekanauki.pl/articles/356790.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    titanium
    implant
    porous
    sintering
    X-ray photoelectron spectroscopy (XPS)
    Opis:
    A single pulse of 0.75-2.0 kJ/0.7g of atomized spherical Ti powders from 300 mF capacitor was applied to produce a microporous Ti implant compact by electro-discharge-sintering (EDS). A solid core in the middle of the compact surrounded by a microporous layer was found. X-ray photoelectron spectroscopy was employed to study the surface characteristics of the EDS Ti compact and it revealed that Ti, C and O were the main constituents on the surface with a smaller amount of N. The surface was lightly oxidized and was primarily in the form of TiO2 resulting from the air oxidation during EDS processing. The lightly oxidized surface of the EDS compact also exhibited Ti nitrides such as TiN and TiON, which revealed that the reaction between air constituents and the Ti powders even in times as short as 128 msec.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1287-1291
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-8 z 8

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