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Tytuł:
Effects of Mechanical Activation on the Structure of Nickeliferous Laterite
Autorzy:
Tunç, T.
Apaydın, F.
Yıldız, K.
Powiązania:
https://bibliotekanauki.pl/articles/1399882.pdf
Data publikacji:
2013-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.20.Wk
61.43.Gt
91.60.Ed
Opis:
The lateritic nickel ore was activated mechanically in a planetary ball mill and mineralogical analyses of nickeliferous laterite have been studied by particle size analysis, scanning electron microscopy, X-ray diffraction, and the Fourier transform infrared spectroscopy. The results show that the activation procedure led to amorphisation, phase transformation and structural disordering in the laterite structure.
Źródło:
Acta Physica Polonica A; 2013, 123, 2; 349-351
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Control of Natural Zeolite Properties by Mechanical Activation in Stirred Media Mill
Autorzy:
Bohács, K.
Faitli, J.
Bokányi, L.
Mucsi, G.
Powiązania:
https://bibliotekanauki.pl/articles/353482.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
zeolite
mechanical activation
zeta-potential
suspension rheology
FTIR
Opis:
Due to the special characteristics of zeolites, they can be applied in a very wide range of industries, i.e. agricultural, environmental or water treatment purposes. Generally, high added value zeolite products are manufactured by micro- or nanogrinding. However, these processes require high energy input and cause significant wearing of the mill parts. Therefore, the optimization of zeolite grinding, as well as the control of its properties are of a great importance. In the present paper a Hungarian natural zeolite was mechanically activated in stirred media mill for various residence times in distilled water, meanwhile the particle size distribution and the grinding energy were measured. Additionally, on-line tube rheometer was used to study the rheology of the suspension during the grinding process. The particle interaction and the suspension aggregation stability were detected by zeta-potential measurements. Structural changes due to the mechanical activation process were monitored by FTIR. It was found that the material structure of the zeolite, as well as the rheological behaviour of the zeolite suspension and its aggregation stability had been altered due to the mechanical activation in the stirred media mill. It can be concluded that the zeolite product properties can be modified by mechanical activation in order to produce a high added value tailored material.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1399-1406
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of mechanical activation on carbothermic reduction and nitridation of titanomagnetite concentrates
Autorzy:
Wen, Xiaojin
Yu, Wen
Zeng, Danliang
Zhu, Liang Liang
Chen, Jiangan
Powiązania:
https://bibliotekanauki.pl/articles/1446680.pdf
Data publikacji:
2021
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
titanomagnetite concentrates
carbothermic reduction
mechanical activation
titanium nitride
Opis:
The carbothermic reduction and nitridation process of titanomagnetite concentrates with the help of mechanical activation were investigated by particle size analysis, thermodynamic calculation, thermogravimetric analysis, X-ray diffraction analysis, scanning electron microscopy, and energy-dispersive spectroscopy analysis. The thermogravimetric and X-ray diffraction results indicated that either the reduction of iron oxide or the reduction and nitridation of M3O5 to TiN could be promoted significantly with the increase in activation time. The results obtained from scanning electron microscopy and energy-dispersive spectroscopy showed that, when samples were not activated, chunks of and thin M3O5 were derived from the reduction of ilmenite and titanomagnetite. They were severely sintered with impurities to form a dense structure. As a result, M3O5 was difficult to be converted to TiN, especially chunks of M3O5. However, when samples were activated, the sintering degrees of the impurity and M3O5 were mitigated, and the particle size of the iron as a medium for delivering C to M3O5 was decreased in the roasted product. This condition enhanced the diffusion of C to the surface of M3O5. Meanwhile, the bulk of ilmenite was broken in the activation process, which prevented the formation of chunks of M3O5. Thus, the conversion of M3O5 to TiN was promoted.
Źródło:
Physicochemical Problems of Mineral Processing; 2021, 57, 5; 33-45
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Mechanical Activation of Deposited Brown Coal Fly Ash in Stirred Media Mill
Autorzy:
Molnár, Z.
Kristály, F.
Mucsi, G.
Powiązania:
https://bibliotekanauki.pl/articles/1375549.pdf
Data publikacji:
2014-10
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.20.Wk
Opis:
Present paper deals with the mechanical activation of deposited brown coal fly ash in a high energy density mill. The mechanical activation was carried out in a laboratory scale stirred media mill using various rotor circumferential speed (5 and 7 m/s), and different grinding time (from 1 min up to 180 min). The consumed energy was measured during the grinding process. Furthermore, particle size distribution and specific surface area were determined using laser particle size analyzer. The structural changes were detected by Fourier transform infrared spectroscopy. Additionally, transformation in mineralogical phases was measured by X-ray diffraction, as well as particle morphology and crystal defects were determined by transmission electron microscopy. As a result of the investigation, relationship between the technological parameters of the grinding and the properties of the ground material was created. It was found that there is a certain mechanochemical effect on the crystal structure of fly ash components in the stirred media mill, as it was revealed by X-ray diffraction and transmission electron microscopy. The most efficient grinding parameters were determined.
Źródło:
Acta Physica Polonica A; 2014, 126, 4; 988-993
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Comparative analysis of process parameters of talc mechanical activation in centrifugal and attrition mill
Autorzy:
Andric, L.
Terzic, A.
Acimovic-Pavlovic, Z.
Pavlovic, L.
Petrov, M.
Powiązania:
https://bibliotekanauki.pl/articles/110391.pdf
Data publikacji:
2014
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
talc
mechanical activation
ultra fine grinding
ultra-centrifugal mill
attrition mill
Opis:
The efficiency of talc mechanical activation by means of two different mechano-activators - centrifugal and attrition mill is investigated in this study and the comparative analysis of the characteristics of obtained talc powders is presented. A new approach for obtaining high-grade talc concentrate with low Fe2O3 content is achieved through effect of mechanical activation of talc accompanied by hydrometallurgical process. The applied mechanical activation process conditions of ultra-centrifugal mill were defined by number of rotor revolutions, sieve mesh size, and current intensity. These operating parameters of the ultra-centrifugal mill were variable. Ultra fine grinding of talc in attrition mill (attritor) was carried out in various time intervals - from 5 to 15 min. The following technological parameters of the mechanical activation were monitored: time of mechanical activation, circumferential rotor speed, capacity of ultra-centrifugal mill, and specific energy consumption. The investigation was based on a kinetic model. The structure and behavior of activated samples were characterized by scanning electron microscopy (SEM), X-ray diffraction (XRD) analysis, and differential thermal analysis (DTA).
Źródło:
Physicochemical Problems of Mineral Processing; 2014, 50, 2; 433-452
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A comparative study of hyperfine interactions in Aurivillius compounds prepared by mechanical activation and solid-state sintering
Autorzy:
Mazurek, M.
Jartych, E.
Powiązania:
https://bibliotekanauki.pl/articles/146528.pdf
Data publikacji:
2017
Wydawca:
Instytut Chemii i Techniki Jądrowej
Opis:
X-ray diffraction and Mössbauer spectroscopy techniques were used to study the structure and hyperfine interactions of multiferroic Aurivillius compounds Bim+1Ti3Fem–3O3m+3. Samples were synthesized by two methods, that is, the solid-state sintering at various temperatures and mechanical activation in a high-energy ball mill. The compounds were obtained from a mixture of three polycrystalline powder oxides, that is, TiO2, Fe2O3 and Bi2O3. At room temperature, the Aurivillius compounds are paramagnetic materials with orthorhombic crystal structure. The c lattice parameter of the unit cell depends linearly on the m − number of layers with perovskite--like structure. Based on the Mössbauer studies, it is concluded that the hyperfine interactions parameters do not change with m number.
Źródło:
Nukleonika; 2017, 62, 2; 153-157
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Mechanical Activation of Al/MoO3 Thermite as a Component of Energetic Condensed Systems to Increase Its Effciency
Autorzy:
Meerov, D.
Ivanov, D.
Monogarov, K.
Muravyev, N.
Pivkina, A.
Frolov, Y.
Powiązania:
https://bibliotekanauki.pl/articles/358816.pdf
Data publikacji:
2009
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
thermites
burning rate
nano-MoO3
Opis:
In the present work a stoichiometric energetic compositions Al+MoO3 prepared by dry mixing and by reactive milling of micro-scale particles were investigated. Morphology, particle size and surface structure of produced powders were examined using scanning electron microscopy, atomic-force microscopy, laser diffractometry and BET analysis. DSC/TG data were processed to obtain kinetic mechanism of the reaction between Al and MoO3. The combustion rate of Al+MoO3 thermite mixture increases with pressure, reaching a maximum at ~10 atm, and then decreases with further pressure increase. The rise of combustion rate at the low range of pressure is associated with the rise in the extent of the vapour phase penetrating the pores of the pressed sample as the ambient pressure increases. However, at a higher pressure the gas formation is suppressed, and the melt formed in the combustion process can selectively wet the pores resulting in inhibition of reaction. Burning rates of mechanical activated system Al+MoO3 are two times higher then not-activated system at ambient pressure ~10 atm and 8 times higher at ~40 atm. In additional experiments, nano-scale MoO3 powder was prepared by evaporation with a subsequent condensation onto cooled plate in an inert-gas fow. Scanning electron microscopy showed that nano-MoO3 particles are absolutely spherical with mean diameter ~100 nm, and atomic-force microscopy 278 D. Meerov et al. reveals smaller particles with mean diameter ~5-30 nm. DSC/TG data showed that the nano-MoO3 starts to sublime earlier than micro MoO3. The use of nano-sized components could considerably increase the burning rates of energetic condensed systems, because of its large specifc surface, lower temperature of sublimation, and high reaction ability.
Źródło:
Central European Journal of Energetic Materials; 2009, 6, 3-4; 277-289
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Mössbauer Spectroscopy Studies of Multiferroic $(BiFeO_3)_{1 - x}-(BaTiO_3)_{x}$ Solid Solutions Prepared by Mechanical Activation
Autorzy:
Jartych, E.
Malesa, B.
Antolak-Dudka, A.
Oleszak, D.
Powiązania:
https://bibliotekanauki.pl/articles/1341859.pdf
Data publikacji:
2014-03
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.85.+t
81.20.-n
61.05.cp
76.80.+y
Opis:
X-ray diffraction and $\text{}^{57}Fe$ Mössbauer spectroscopy were applied as complementary methods in order to investigate the structure and hyperfine interactions of $(BiFeO_3)_{1-x}-(BaTiO_3)_{x}$ solid solutions prepared by mechanical activation and subsequent heat treatment.
Źródło:
Acta Physica Polonica A; 2014, 125, 3; 837-839
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structure and Magnetic Properties of Bi5Ti3FeO15 Ceramics Prepared by Sintering, Mechanical Activation and Edamm Process. A Comparative Study
Autorzy:
Jartych, E.
Pikula, T.
Mazurek, M.
Franus, W.
Lisinska-Czekaj, A.
Czekaj, D.
Oleszak, D.
Surowiec, Z.
Aksenczuk, A.
Calka, A.
Powiązania:
https://bibliotekanauki.pl/articles/352172.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Aurivillius compounds
sintering
mechanical activation
magnetic properties
Opis:
Three different methods were used to obtain Bi5Ti3FeO15 ceramics, i.e. solid-state sintering, mechanical activation (MA) with subsequent thermal treatment, and electrical discharge assisted mechanical milling (EDAMM). The structure and magnetic properties of producedBi5Ti3FeO15 samples were characterized using X-ray diffraction and Mössbauer spectroscopy. The purest Bi5Ti3FeO15 ceramics was obtained by standard solid-state sintering method. Mechanical milling methods are attractive because the Bi5Ti3FeO15 compound may be formed at lower temperature or without subsequent thermal treatment. In the case of EDAMM process also the time of processing is significantly shorter in comparison with solid-state sintering method. As revealed by Mössbauer spectroscopy, at room temperature theBi5Ti3FeO15 ceramics produced by various methods is in paramagnetic state.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 2A; 869-874
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Mechanical Activation on the Structural Properties of Mn-Doped $Na_{0.5}Bi_{0.5}TiO_3$ Ceramics
Autorzy:
Kırsever, D.
Özkan Toplan, H.
Powiązania:
https://bibliotekanauki.pl/articles/1398731.pdf
Data publikacji:
2016-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.05.Je
Opis:
Piezoelectric ceramics $(Na_{0.5}Bi_{0.5})TiO_3$ + 0.5 mol.% Mn (Mn-NBT) have been synthesized by mechanical activation of mixed oxides BiO₂, Na₂CO₃, TiO₂ and MnO for 1 h at room temperature. Non-activated and activated Mn-NBT powders were characterized by using X-ray diffraction and scanning electron microscopy. Also, the mechanical activation-derived Mn-NBT powders were uniaxially pressed and all pellets were sintered at 1000°C and 1200°C for 2 h in air atmosphere. The microstructure and phase analysis of sintered pellets was investigated by using scanning electron microscopy and X-ray diffraction.
Źródło:
Acta Physica Polonica A; 2016, 129, 4; 610-612
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
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