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Wyświetlanie 1-10 z 17
Tytuł:
Fabrication and microstructure of layers containing intermetallic phases on magnesium
Autorzy:
Mola, R.
Powiązania:
https://bibliotekanauki.pl/articles/381749.pdf
Data publikacji:
2013
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
heat treatment
magnesium
Al-enriched surface layer
intermetallic phases
hardness
obróbka cieplna
warstwa wierzchnia
faza międzymetaliczna
twardość
magnez
Opis:
Al- and Al/Zn-enriched layers containing intermetallic phases were deposited on the Mg substrate by heating the Mg specimens in contact with the powdered materials in a vacuum furnace. The Al-enriched surface layers were produced using Al powder, whereas the Al/Zn-enriched layers were obtained from an 80 wt.% Al + 20 wt.% Zn powder mixture. The microstructure and composition of the layers were analyzed by optical microscopy, scanning electron microscopy and X-ray diffraction. The results showed that the Al-enriched layer comprised an Mg17Al12 intermetallic phase and a solid solution of Al in Mg. The layer obtained from the Al+Zn powder mixture was composed of Mg-Al-Zn intermetalic phases and a solid solution of Al and Zn in Mg. Adding 20% of Zn into the Al powder resulted in the formation of a considerably thicker layer. Moreover, the hardness of the surface layers was much higher than that of the Mg substrate.
Źródło:
Archives of Foundry Engineering; 2013, 13, 1; 99-102
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Properties of Al/Zn-enriched Surface Layers on Mg
Autorzy:
Mola, R.
Powiązania:
https://bibliotekanauki.pl/articles/381256.pdf
Data publikacji:
2014
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
magnesium
surface modification
intermetallic phases
microstructure
corrosion resistance
wear resistance
magnez
modyfikacja powierzchni
faza międzymetaliczna
mikrostruktura
odporność na korozję
odporność na zużycie
Opis:
The Al/Zn-enriched surface layers were fabricated on Mg substrate by heating the specimens in contact with an Al + 40 wt.% Zn powder mixture at 445oC for 60 min. The microstructure and corrosion and wear resistance of the layers were investigated and discussed. The experimental results show that the layers were composed of Mg17(Al,Zn)12 and Mg5Al2Zn2 intermetallic phases and a solid solution of Al and Zn in Mg. They were integrated with the substrate trough a zone of a solid solution of Al and Zn in Mg. The potentiodynamic polarization measurements indicated that the specimens with Al/Zn-enriched layer had better corrosion resistance than the bare Mg. The microhardness of the layers containing Mg-Al-Zn intermetallic phases was much higher than that of the Mg substrate. The sliding wear tests showed that the wear resistance of the specimens with a surface layer containing intermetallic phases was also superior to that of untreated Mg.
Źródło:
Archives of Foundry Engineering; 2014, 14, 3 spec.; 45-48
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication and Microstructure of Diffusion Alloyed Layers on Pure Magnesium Substrate
Wytwarzanie i struktura dyfuzyjnych stopowych warstw na magnezie
Autorzy:
Mola, R.
Powiązania:
https://bibliotekanauki.pl/articles/352037.pdf
Data publikacji:
2014
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
magnesium
alloyed coating
Mg-Al-Zn intermetallic phases
hardness
magnez
warstwy stopowe
fazy międzymetaliczne Mg-Al-Zn
twardość
Opis:
Alloyed layers on pure magnesium were created by means of the heating of the magnesium sample covered with Al+Zn powders mixture containing 20 wt.% Zn and 40 wt.% Zn in vacuum furnace. The microstructure and related composition of the alloyed layers were investigated using optical microscopy and scanning electron microscopy equipped with an energy dispersive X-ray system (EDS). The results revealed that the microstructure, thickness and microhardness of the obtained layers depended on the Zn content in the powder mixture. The alloyed layers were composed of the Mg-Al-Zn intermetallic phases and Mg-based solid solution containing Al and Zn. The multi-phase layer was diffusion bonded with magnesium substrate. The thickness of the layer fabricated by the heat treatment in contact with a powder mixture containing 40 wt.% Zn was twice as high as compared to that obtained with the powder mixture containing 20 wt.% Zn. The hardness value of the alloyed layers was much higher than that of the magnesium substrate.
Warstwy stopowe na magnezie zostały wytworzone poprzez wygrzewanie próbek w kontakcie z mieszankami proszków Al+Zn zawierajacymi 20% mas. Zn i 40% mas. Zn w piecu próżniowym (oznaczone jako: Al20Zn i Al40Zn). Badania struktury i składu chemicznego przeprowadzono na mikroskopie optycznym oraz elektronowym mikroskopie skaningowym wyposażonym w mikroanalizator rentgenowski. Wyniki badań wykazały, że mikrostruktura, grubość oraz mikrotwardość otrzymanych warstw zależą od zawartości Zn w mieszankach proszków. Warstwy stopowe składały się z faz międzymetalicznych Mg-Al-Zn i roztworu stałego Al i Zn w Mg i były dyfuzyjnie połączone z podłożem-magnezem. Grubość warstwy wytworzonej na podłożu magnezowym poprzez wygrzewanie próbek w kontakcie z mieszanką proszków zawierającą 40% mas. Zn była dwa razy większa w porównaniu do warstwy otrzymanej w mieszance zawierającej 20% mas. Zn. Twardość otrzymanych warstw stopowych była znacznie wyższa w porównaniu do twardości podłoża.
Źródło:
Archives of Metallurgy and Materials; 2014, 59, 4; 1409-1412
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Magnez – kierunki kształtowania własności mechanicznych
Magnesium – trends of development of mechanical properties
Autorzy:
Dziadoń, A.
Mola, R.
Powiązania:
https://bibliotekanauki.pl/articles/211468.pdf
Data publikacji:
2013
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Obróbki Plastycznej
Tematy:
magnez
stopy magnezu
umacnianie wydzieleniowe
warstwa wierzchnia
magnesium
magnesium alloy
precipitation strengthening
surface layer
Opis:
Praca przedstawia w formie przeglądowej aktualny stan rozwoju technologii stopów magnezu. Zainteresowanie stopami magnezu ciągle rośnie, głównie z tego względu, że posiadają one dobrą wytrzymałość w połączeniu z niską gęstością. Artykuł zawiera charakterystykę podstawowych stopów magnezu i przegląd głównych metod, które pozwalają wpływać na ich własności. Przede wszystkim przeanalizowano proces starzenia stopów magnezu. Wykazano, na przykładzie stopu AZ91, że poddane obróbce cieplnej stopy magnezu wykazują słabsze umocnienie w porównaniu do stopów o osnowie aluminium. Z drugiej strony, rozdrobnienie ziarna wywiera znacznie większy niż w przypadku stopów aluminium i stopów innych metali wpływ na umocnienie magnezu i jego stopów. Artykuł zawiera także przegląd najnowszych prac dotyczących kompozytów o osnowie magnezu. W szczególności przedstawiono sposób wytwarzania makro-kompozytu warstwowego magnez-fazy międzymetaliczne. Pokazano również, że istnieje możliwość znaczącej zmiany mikrostruktury i własności warstwy wierzchniej magnezu za pomocą obróbki laserowej.
The work gives an overview on the actual status of the technology development of magnesium alloys. Interest in the magnesium alloys is still growing mainly because they combine good strength and low density. Article contains characteristics of fundamental magnesium alloys and review of main methods of influencing on their properties. First of all, ageing behaviour of magnesium alloys was analyzed. It has been shown, giving an example AZ91 alloy, that the heat treated magnesium alloys exhibit weaker strengthening effect compared to aluminum-base alloys. On the other hand, effect of the grain refining on strengthening in magnesium and magnesium alloys is much higher than that for aluminum alloys and for alloys of other metals. A paper contains a review of the recent works concerning the magnesium matrix composites. In particularly, a method of manufacturing magnesium-intermetallic phases layered macro-composite was presented. It was also shown that there exists possibility of significant modification of the microstructure and properties of the surface layer of magnesium using the laser treatment.
Źródło:
Obróbka Plastyczna Metali; 2013, 24, 4; 253-277
0867-2628
Pojawia się w:
Obróbka Plastyczna Metali
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Microstructure and Properties of the Bimetallic AZ91/AlSi17 Joint Produced by Compound Casting
Autorzy:
Mola, R.
Bucki, T.
Powiązania:
https://bibliotekanauki.pl/articles/381472.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
innovative foundry technologies
innovative foundry materials
casting process
microstructure
mechanical properties
innowacyjne technologie odlewnicze
innowacyjne materiały odlewnicze
proces odlewania
mikrostruktura
właściwości mechaniczne
Opis:
Bimetallic AZ91/AlSi17 samples were produced by compound casting. The casting process involved pouring the AZ91 magnesium alloy heated to 650ºC onto a solid AlSi17 aluminum alloy insert placed in a steel mould. Prior to casting, the mould with the insert inside was heated to about 370ºC. The bonding zone formed between AZ91 and AlSi17 had a thickness of about 200 μm; it was characterized by a non-homogeneous microstructure. Two different areas were distinguished in this zone: the area adjacent to the AZ91 and the area close to the AlSi17. In the area closest to the AZ91 alloy, a eutectic composed of an Mg17Al12 intermetallic phase and a solid solution of Al in Mg was observed. In bonding zone at a certain distance from the AZ91 alloy an Mg2Si phase co-occurred with the eutectic. In the area adjacent to the AlSi17 alloy, the structure consisted of Al3Mg2, Mg17Al12 and Mg2Si. The fine Mg2Si phase particles were distributed over the entire Mg-Al intermetallic phase matrix. The microhardness of the bonding zone was much higher than those of the materials joined; the microhardness values were in the range 203-298 HV. The shear strength of the AZ91/AlSi17 joint varied from 32.5 to 36 MPa.
Źródło:
Archives of Foundry Engineering; 2018, 18, 1; 71-76
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microscopic Analysis of Layers Containing Mg2Si and Mg17Al12 Phases Fabricated on AZ91 Through Thermochemical Treatment
Autorzy:
Mola, R.
Cieślik, M.
Powiązania:
https://bibliotekanauki.pl/articles/380750.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
surface treatment
magnesium alloy
modified surface layer
microstructure
obróbka powierzchniowa
stop magnezu
warstwa powierzchniowa zmodyfikowana
mikrostruktura
Opis:
The thermochemical treatment applied to improve the surface properties of AZ91 consisted in heating the material in contact with AlSi10Mg powder at 445 oC for 30 min. During heat treatment process the powder was held under pressure to facilitate the diffusion of the alloying elements to the substrate and, accordingly, the formation of a modified layer. Two pressures, 1 MPa and 5 MPa, were tested. The resultant layers, containing hard Mg2Si and Mg17Al12 phases, were examined using an optical microscope and a scanning electron microscope equipped with an energy-dispersive X-ray spectrometer (EDS). The experimental data show that the layer microstructure was dependent on the pressure applied. A thicker, three-zone layer (about 200 μm) was obtained at 1 MPa. At the top, there were Mg2Si phase particles distributed over the Mg17Al12 intermetallic phase matrix. The next zone was a eutectic (Mg17Al12 and a solid solution of Al in Mg) with Mg2Si phase particles embedded in it. Finally, the area closest to the AZ91 substrate was a eutectic not including the Mg2Si phase particles. By contrast, the layer produced at a pressure of 5 MPa had lower thickness of approx. 150 μm and a two-zone structure. Mg2Si phase particles were present in both zones. In the upper zone, Mg2Si phase particles were regularly distributed over the Mg17Al12 intermetallic phase matrix. The lower zone, adjacent to the AZ91, was characterized by a higher volume fraction of Mg2Si phase particles distributed over the matrix composed mainly of Mg17Al12. The alloyed layers enriched with Al and Si had much higher hardness than the AZ91 substrate.
Źródło:
Archives of Foundry Engineering; 2019, 3; 119-124
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Characterization of the Bonding Zone in a ZE41/AlSi12 Joint Fabricated by Liquid- Solid Compound Casting
Autorzy:
Mola, R.
Bucki, T.
Powiązania:
https://bibliotekanauki.pl/articles/381097.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
innovative foundry technology
innovative foundry material
compound casting process
magnesium alloy
aluminum alloy
bonding zone
innowacyjna technologia odlewnicza
innowacyjny materiał odlewniczy
proces odlewania
stop magnezu
stop aluminium
strefa złącza
Opis:
The study involved using the liquid-solid compound casting process to fabricate a lightweight ZE41/AlSi12 bimetallic material. ZE41 melt heated to 660 °C was poured onto a solid AlSi12 insert placed in a steel mold. The mold with the insert inside was preheated to 300 °C. The microstructure of the bonding zone between the alloys was examined using optical microscopy and scanning electron microscopy. The chemical composition was determined through linear and point analyses with an energy-dispersive X-ray spectroscope (EDS). The bonding zone between the magnesium and aluminum alloys was about 250 μm thick. The results indicate that the microstructure of the bonding zone changes throughout its thickness. The structural constituents of the bonding zone are: a thin layer of a solid solution of Al and Zn in Mg and particles of Mg-Zn-RE intermetallic phases (adjacent to the ZE41 alloy), a eutectic region (Mg17(Al,Zn)12 intermetallic phase and a solid solution of Al and Zn in Mg), a thin region containing fine, white particles, probably Al-RE intermetallic phases, a region with Mg2Si particles distributed over the eutectic matrix, and a region with Mg2Si particles distributed over the Mg-Al intermetallic phases matrix (adjacent to the AlSi12 alloy). The microstructural analysis performed in the length direction reveals that, for the process parameters tested, the bonding zone forming between the alloys was continuous. Low porosity was observed locally near the ZE41 alloy. The shear strength of the AZ91/AlSi17 joint varied from 51.3 to 56.1 MPa.
Źródło:
Archives of Foundry Engineering; 2018, 18, 2; 203-208
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Formation of Al-alloyed Layer on Magnesium with Use of Casting Techniques
Autorzy:
Mola, R.
Bucki, T.
Dziadoń, A.
Powiązania:
https://bibliotekanauki.pl/articles/382549.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
surface layer
intermetallic phase
casting process
magnesium
warstwa powierzchniowa
faza międzymetaliczna
proces odlewania
Opis:
Al-enriched layer was formed on a magnesium substrate with use of casting. The magnesium melt was cast into a steel mould with an aluminium insert placed inside. Different conditions of the casting process were applied. The reaction between the molten magnesium and the aluminium piece during casting led to the formation of an Al-enriched surface layer on the magnesium substrate. The thickness of the layer was dependent on the casting conditions. In all fabricated layers the following phases were detected: a solid solution of Mg in Al, Al3Mg2, Mg17Al120 and a solid solution of Mg in Al. When the temperature of the melt and the mould was lower (variant 1 – 670oC and 310oC; variant 2 – 680oC and 310oC, respectively) the unreacted thin layer of aluminium was observed in the outer zone. Applying higher temperatures of the melt (685oC) and the mould (325oC) resulted in deep penetration of aluminium into the magnesium substrate. Areas enriched in aluminium were locally observed. The Al-enriched layers composed mainly of Mg-Al intermetallic phases have hardness from 187-256 HV0.1.
Źródło:
Archives of Foundry Engineering; 2016, 16, 1; 112-116
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Characterization of the Surface Layer of Mg Enriched with Al and Si by Thermochemical Treatment
Autorzy:
Mola, R.
Stępień, E.
Cieślik, M.
Powiązania:
https://bibliotekanauki.pl/articles/382030.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
enriched magnesium
surface modification
thermochemical treatment
layer microstructure
microhardness
magnez wzbogacony
modyfikacja powierzchni
obróbka cieplno-chemiczna
mikrotwardość
Opis:
The modified surface layers of Mg enriched with Al and Si were fabricated by thermochemical treatment. The substrate material in contact with an Al + 20 wt.% Si powder mixture was heated to 445ºC for 40 or 60 min. The microstructure of the layers was examined by OM and SEM. The chemical composition of the layer and the distribution of elements were determined by energy dispersive X-ray spectroscopy (EDS). The experimental results show that the thickness of the layer is dependent on the heating time. A much thicker layer (1 mm) was obtained when the heating time was 60 min than when it was 40 min (600 μm). Both layers had a non-homogeneous structure. In the area closest to the Mg substrate, a thin zone of a solid solution of Al in Mg was detected. It was followed by a eutectic with Mg17Al12 and a solid solution of Al in Mg. The next zone was a eutectic with agglomerates of Mg2Si phase particles; this three-phase structure was the thickest. Finally, the area closest to the surface was characterized by dendrites of the Mg17Al12 phase. The microhardness of the modified layer increased to 121-236 HV as compared with 33-35 HV reported for the Mg substrate.
Źródło:
Archives of Foundry Engineering; 2017, 17, 4; 195-199
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure of the Bonding Zone Between AZ91 and AlSi17 Formed by Compound Casting
Autorzy:
Mola, R.
Bucki, T.
Dziadoń, A.
Powiązania:
https://bibliotekanauki.pl/articles/379744.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
casting process
joining
magnesium alloys
aluminum alloys
intermetallic phases
microstructure
proces odlewania
łączenie
stop magnezu
stop aluminium
faza intermetaliczna
mikrostruktura
Opis:
This paper discusses the joining of AZ91 magnesium alloy with AlSi17 aluminium alloy by compound casting. Molten AZ91 was cast at 650oC onto a solid AlSi17 insert placed in a steel mould under normal atmospheric conditions. Before casting, the mould with the insert inside was heated up to about 370oC. The bonding zone forming between the two alloys as a result of diffusion had a multiphase structure and a thickness of about 200 μm. The microstructure and composition of the bonding zone were analysed using optical microscopy, scanning electron microscopy and energy dispersive X-ray spectroscopy. The results indicate that the bonding zone adjacent to the AlSi17 alloy was composed of an Al3Mg2 intermetallic phase with not fully consumed primary Si particles, surrounded by a rim of an Mg2Si intermetallic phase and fine Mg2Si particles. The bonding zone near the AZ91 alloy was composed of a eutectic (an Mg17Al12 intermetallic phase and a solid solution of Al and Si in Mg). It was also found that the compound casting process slightly affected the AZ91alloy microstructure; a thin layer adjacent to the bonding zone of the alloy was enriched with aluminium.
Źródło:
Archives of Foundry Engineering; 2017, 17, 1; 202-206
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-10 z 17

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