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Tytuł:
Synthesis and Characterization of PolyNIMMO-HTPB-polyNIMMO Triblock Copolymer as a Potential Energetic Binder
Autorzy:
Wang, X.
Shu, Y.
Lu, X.
Mo, H.
Xu, M.
Powiązania:
https://bibliotekanauki.pl/articles/358529.pdf
Data publikacji:
2018
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
triblock copolymer
cationic ring opening polymerization
polymer
DSC
Opis:
Triblock copolymer polyNIMMO-HTPB-polyNIMMO was synthesized by cationic ring opening polymerization of NIMMO (3-nitratomethyl-3-methyloxetane) in the presence of hydroxyl-terminated polybutadiene catalyzed by BF3·OEt2. The polymer was characterized by FT-IR, 1H NMR, 13C NMR spectroscopy, and GPC. DSC was used to investigate the thermal behaviour of the triblock copolymer and its exothermic decomposition peak was found to be at 215 °C. All of the results indicated that the triblock copolymer polyNIMMO-HTPB-polyNIMMO might serve as a potential energetic propellant binder.
Źródło:
Central European Journal of Energetic Materials; 2018, 15, 3; 456-467
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Preparation and Characterisation of Polylactic acid (PLA)/Polycaprolactone (PCL) Composite Microfibre Membranes
Otrzymywanie i charakterystyka kompozytowych membran z mikrowłókien PLA/PCL
Autorzy:
Lu, Y.
Chen, Y.-C.
Zhang, P.-H.
Powiązania:
https://bibliotekanauki.pl/articles/233499.pdf
Data publikacji:
2016
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Biopolimerów i Włókien Chemicznych
Tematy:
PLA/PCL
electrospinning
microfibre membrane
property
elektroprzędzenie
membrana z mikrofibry
mikrowłókno
Opis:
Biodegradable polymers like PLA and PCL have wide application in tissue engineering because of their biocompatibility, degradation and mechanical properties. In this study, the optimised electrospinning parameters of PLA/PCL composite membranes were determined with scanning electron microscopy to obtain smooth and relatively fine microfibre. The properties and structure of electrospinning PLA, PCL and PLA/PCL(70/30) membranes were investigated by scanning electron microscopy (SEM), differential scanning calorimetry (DSC), X-ray diffraction (XRD), the water contact angle, water absorption degree and tensile strength. The results revealed that PLA/PCL composite membranes possessed better mechanical and hydrophilic properties when compared to single component microfibre membranes like PLA and PCL. The improvements above are conducive to microfibre membrane application in the biomedical sector.
Biodegradowalne polimery, takie jak PLA i PCL znajdują wiele zastosowań w inżynierii tkankowej ze względu na swoją biokompatybilność, oraz właściwości mechaniczne. W badaniach, wyznaczono optymalne parametry elektroprzędzenia błon kompozytowych PLA/PCL stosując metodę skaningowej mikroskopii elektronowej, w celu otrzymania gładkich i cienkich mikrowłókien. Właściwości i strukturę elektroprzędzionych błon PLA, PCL i PLA/PCL(70/30) badano za pomocą elektroskopii skaningowego (SEM), różnicowej kalorymetrii skaningowej (DSC), dyfrakcji rentgenowskiej (XRD), metody kąta zwilżania wody, współczynnika absorpcji wody i wytrzymałości na rozciąganie. Wyniki wykazały, że błony kompozytowe PLA/PCL posiadają lepsze właściwości mechaniczne i hydrofilowe, w porównaniu do jednoskładnikowych błon z mikrowłókien, takich jak PLA i PCL. Powyższe ulepszenia sprzyjają zastosowaniu membran z mikrowłókien w branży biomedycznej.
Źródło:
Fibres & Textiles in Eastern Europe; 2016, 3 (117); 17-25
1230-3666
2300-7354
Pojawia się w:
Fibres & Textiles in Eastern Europe
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Phase features of several typical blood cells and their identification without unwrapping
Autorzy:
Wang, Y.
Chen, Y
Lü, C.
Shang, X.
Xu, Y.
Wu, H.
Zhu, X.
Jin, W.
Powiązania:
https://bibliotekanauki.pl/articles/173588.pdf
Data publikacji:
2013
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
digital holographic phase
nucleated cell
phase model
wrapped phase features
identification
Opis:
The digital holographic phase microscopy (DHPM) technique which has been proposed for cellular morphology and dynamic analysis yielded highly desirable results. However, for nucleated cells (especially white blood cells (WBCs)), their submicroscopic structure has not yet been deconstructed through a phase unwrapping method due to the heterogeneity of an internal phase. By analyzing the phase heterogeneity of subclasses of WBCs, the typical phase models of them are built first in this paper; using the simulation method, the wrapped phase distributions of these models are obtained. However, by optimizing the wrapped phase maps and analyzing the relationships between them and typical blood cells, their features are selected and extracted. Then the models built are sorted out from each other successfully without unwrapping via analyzing these extracted features, which provides a valuable approach and technological base for the classification and identification of blood cells.
Źródło:
Optica Applicata; 2013, 43, 3; 505-514
0078-5466
1899-7015
Pojawia się w:
Optica Applicata
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Optical and Scintillation Properties of $Bi_{4}(Ge_{x}S_{1-x})_{3}O_{12}$ Single Crystal
Autorzy:
Xiao, X.
Xu, J.
Lu, B.
Cai, W.
Zhang, Y.
Shen, H.
Yang, B.
Xiang, W.
Powiązania:
https://bibliotekanauki.pl/articles/1399369.pdf
Data publikacji:
2015-03
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.10.Fq
61.05.C-
78.20.Ci
78.70.Ps
Opis:
The solid solution crystals, $Bi_{4}(Ge_{x}Si_{1-x})_{3}O_{12}$ (BGSO) with x=0, 0.05, and 0.15, have been grown by the modified vertical Bridgman method. The as-grown crystals show 80% of transmittance with an absorption edge of 285 nm. The relative light yields of BGSO crystals are found to be 7.2%, 6.3%, and 4.2% of CsI(Tl) crystal for x=0, 0.05, and 0.15, respectively. The energy resolutions of these crystals are 18.9%, 21.3%, and 24.7%, respectively, with PMT for 662 keV gamma rays at room temperature when exposed to $\text{}^{137}Cs$ γ -ray. The scintillation performance of BGSO crystals clearly deteriorates with the increase of Ge content. However, the appropriate number of germanium ions doped to BSO crystal can improve its crystallization behavior and effectively restrain component segregation. It is expected that large size crystals of BGSO will be grown and applied to the dual readout calorimeter in the nearest future.
Źródło:
Acta Physica Polonica A; 2015, 127, 3; 854-858
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Neogene seismites and seismic volcanic rocks in the Linqu area, Shandong Province, E China
Autorzy:
Tian, H. S.
Zhang, B. H.
Zhang, S. H.
Lü, M. Y.
Powiązania:
https://bibliotekanauki.pl/articles/94331.pdf
Data publikacji:
2014
Wydawca:
Uniwersytet im. Adama Mickiewicza w Poznaniu
Tematy:
seismite
seismic volcanic rock
Neogene
tectonic extension
Linqu
sejsmity
skała wulkaniczna
neogen
Opis:
The Yishu Fault Zone runs through the centre of Shandong Province (E China); it is a deep-seated large fault system that still is active. Two volcanic faulted basins (the Shanwang and Linqu Basins) in the Linqu area, west of the fault zone, are exposed to rifting, which process is accompanied by a series of tectonic and volcanic earthquakes with a magnitude of 5–8. Lacustrine sediments in the basins were affected by these earthquakes so that seismites with a variety of softsediment deformation structures originated. The seismites form part of the Shanwang Formation of the Linqu Group. Semi-consolidated fluvial conglomerates became deformed in a brittle way; these seismites are present at the base of the Yaoshan Formation. Intense earthquakes triggered by volcanic activity left their traces in the form of seismic volcanic rocks associated with liquefied-sand veins in the basalt/sand intercalations at the base of the Yaoshan Formation. These palaeo-earthquake records are dated around 14–10 Ma; they are responses to the intense tectonic extension and the basin rifting in this area and even the activity of the Yishu Fault Zone in the Himalayan tectonic cycle.
Źródło:
Geologos; 2014, 20, 2; 125-137
1426-8981
2080-6574
Pojawia się w:
Geologos
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Magnolol inhibits Streptococcus suis-induced inflammation and ROS formation via TLR2/MAPK/NF-κB signaling in RAW264.7 cells
Autorzy:
Wang, J.
Sun, Y.
Zhang, L.
Xu, W.
You, J.
Lu, H.
Song, Y.
Wei, J.
Li, L.
Powiązania:
https://bibliotekanauki.pl/articles/2087779.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
magnolol
Streptococcus suis
Toll-like receptor2
mitogen-activated protein kinase
nuclear factor Kappa B
Źródło:
Polish Journal of Veterinary Sciences; 2018, 21, 1; 111-118
1505-1773
Pojawia się w:
Polish Journal of Veterinary Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Improving spodumene flotation using a mixed cationic and anionic collector
Autorzy:
Wang, Y.
Zhu, G.
Yu, F.
Lu, D.
Wang, L.
Zhao, Y.
Zheng, H.
Powiązania:
https://bibliotekanauki.pl/articles/109883.pdf
Data publikacji:
2018
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
spodumene
lithium
silicates
flotation
anionic surfactant
cationic surfactant
Opis:
Lithium, a rare-earth element, has been in increasing demand. Spodumene flotation is an important and challenging step for lithium extraction and production from lithium ore. In the present work, flotation tests for three pure minerals (i.e., spodumene, quartz and feldspar) and a real spodumene ore were carried out at laboratory scale. The results showed that YOA, a mixture of oleic acid and dodecylamine with the molar ration of 10:1, could be used as collector to produce a spodumene concentrate with grade of 5.59% Li2O from the feed ore with grade of 1.48% Li2O where 85.24% of Li2O was recovered to the concentrate. The measured zeta potential, contact angle and adsorption capacity indicated that YOA was preferentially adsorbed on spodumene instead of on quartz or feldspar, with the spodumene surface being more hydrophobic than that of feldspar or quartz. The adsorption energies of YOA on spodumene were calculated and the results provided insights into the superior flotation performance obtained in the present work.
Źródło:
Physicochemical Problems of Mineral Processing; 2018, 54, 2; 567-577
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Genetic diversity and relationship of Hunan province of China local tree peonies based on SSR markers
Autorzy:
Zhang, M.-H.
Jin, X.-L.
Wen, Y.-F.
Shen, S.
Wen-Xing
Wu, S.
Lu, J.-H.
Ye-Ye
Powiązania:
https://bibliotekanauki.pl/articles/12665369.pdf
Data publikacji:
2019
Wydawca:
Uniwersytet Przyrodniczy w Lublinie. Wydawnictwo Uniwersytetu Przyrodniczego w Lublinie
Tematy:
China
Hunan Province
plant cultivation
tree peony
Paeonia suffruticosa
ornamental plant
genetic diversity
genetic relationship
SSR marker
Opis:
Paeonia sect. Moutan is a wide known ornamental plant in the world. The objective of this study was to provide the theoretical basis for scientific preservation and utilization of tree peony resources of Hunan province of China. Simple sequence repeat (SSR) markers were applied to reveal the genetic diversity and relationship of 21 tree peony resources and 45 domestic and foreign tree peony cultivars. Clear bands, the size of which ranged from 115 bp to 379 bp, were detected with 14 primers. In total, 90 alleles were detected and the number of alleles detected with one primer varied between 5 and 13; the number of effective alleles ranged from 1.183 to 2.070; the polymorphism ratio of each locus was 100%. The observed heterozygosity, which ranged from 0.120 to 0.851 with an average of 0.532, was larger than the expected one, which ranged from 0.090 to 0.470 with an average of 0.300. Shannon index ranged from 0.137 to 0.695 and fixation index ranged from −0.332 to −0.869. The results show abundant genetic diversity in tree peony of Hunan province and SSR markers distinguishing homonymous tree peony resources successfully.
Źródło:
Acta Scientiarum Polonorum. Hortorum Cultus; 2019, 18, 4; 213-223
1644-0692
Pojawia się w:
Acta Scientiarum Polonorum. Hortorum Cultus
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Functional Properties and Electromagnetic Shielding Behaviour of Elastic Warp-knitted Fabrics
Właściwości funkcyjne i ekranowanie elektromagnetyczne elastycznych dzianin kolumienkowych
Autorzy:
Yu, Z. C.
He, H. L.
Lu, Y. H.
Zhang, J. F.
Lou, C. W.
Chen, A. P.
Lin, J. H.
Powiązania:
https://bibliotekanauki.pl/articles/232038.pdf
Data publikacji:
2015
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Biopolimerów i Włókien Chemicznych
Tematy:
functional properties
electromagnetic shielding effectiveness
protective clothing
elastic warp-knitted fabric
electromagnetic wave
właściwości funkcjonalne
skuteczność ekranowania elektromagnetycznego
odzież ochronna
elastyczna osnowa-dzianina
fala elektromagnetyczna
Opis:
An investigation was made on the electromagnetic shielding behaviour and other functional properties for manufactured multifunctional elastic warp-knitted fabrics. Bamboo charcoal polyester/Crisscross-section polyester (BC-PET/CSP) blended yarns were used as the back of the warp-knitted fabric while conductive composite yarns were used as the front. The variation in the far infrared emissivity and anion density of elastic-warp knitted fabrics produced with different proportions of BC-PET content were studied in detail. Moreover the electromagnetic shielding effectiveness (EMSE) of the fabrics with different elongation was measured in this study. The experimental results showed that increased elongation almost did not significantly affect the EM shielding behaviour of fabric K1 in the elongation range of 0 - 40%. Finally to increase the EMSE of the fabric, the lamination method was used in this study. EMSE measurement results showed that two layer K1 warpknitted fabrics with 90° interval displayed a better shielding effect against the EM wave compared to that with a 0° interval.
Przeprowadzono badania właściwości ekranujących przed polem elektromagnetycznym i innych właściwości funkcyjnych wyprodukowanych wielofunkcyjnych elastycznych dzianin kolumienkowych. Zastosowano przędze kompozytowe z mieszanek zawierających drut ze stali kwasoodpornej, ciągłe włókna poliamidowe i poliestrowe oraz cięte włókna ze regenerowanej celulozy z surowca bambusowego. Badano emisyjność w dalekiej podczerwieni i gęstość anionową dzianin kolumienkowych wytworzonych przy rożnych proporcjach zastosowanych składników. Poza tym badano efektywność ochrony elektromagnetycznej dzianin przy rożnych wydłużeniach. Wyniki eksperymentów pokazują, że zwiększone wydłużenie prawie nie wpływa istotnie na właściwości ekranujące. Dla zwiększenia efektu ekranowania zastosowano metodę laminacji.
Źródło:
Fibres & Textiles in Eastern Europe; 2015, 5 (113); 78-83
1230-3666
2300-7354
Pojawia się w:
Fibres & Textiles in Eastern Europe
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fatigue Behavior and Mechanism of FV520B-I Owing to the Effect of Loading Frequency on the Fatigue Property in HCF and VHCF Regime
Autorzy:
Wang, J.
Zhang, Y.
Shi, B.
Zhao, Q.
Sun, Q.
Zhang, Z.
Lu, H.
Powiązania:
https://bibliotekanauki.pl/articles/353784.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
ultrahigh loading frequency
FV520B-I
fatigue strength
fatigue conversion model
Opis:
Fatigue property of FV520B-I is affected by the ultrahigh loading frequency significantly, and the ultrasonic fatigue experimental data can’t be employed directly to analyze the fatigue failure in the actual remanufacturing engineering. However few theories about the effect of loading frequency on the fatigue property of FV520B-I has ever been proposed. In this paper, both ultrasonic experiment and conventional experiment are conducted out to obtain the fatigue data. The effect of loading frequency on the fatigue data distribution is discussed firstly, its fatigue limit declines with the increase of the loading frequency. Then the fracture surface observations are captured, the fatigue property and fatigue behavior mechanism of FV520B-I is examined by analyzing the fracture surface features, crack initiation and failure observations. A new material frequency correction factor is proposed and introduced to eliminate the influence of the loading frequency on the FV520B-I fatigue property. FV520B-I empirical fatigue life conversion model and fatigue strength conversion model are established with comprehensive use of a fitting algorithm based on the combination of experimental data and classic formula. A clear understand of the effect of loading frequency on the fatigue property of FV520B-I is novel and has an important significance in guaranteeing the accuracy of the actual fatigue analysis of FV520B-I in the remanufacturing engineering.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 1; 347-357
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Characterization of monochlorobenzene contamination in soils using geostatistical interpolation and 3D visualization for agrochemical industrial sites in southeast China
Autorzy:
Ren, L.
Lu, H.
He, L.
Zhang, Y.
Powiązania:
https://bibliotekanauki.pl/articles/204614.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
soil pollution
monochlorobenzene
POPs
persistent organic pollutants
geostatistical interpolation
3D visualization
Opis:
Persistent organic pollutants (POPs) originating from agrochemical industries have become an urgent environmental problem worldwide. Ordinary kriging, as an optimal geostatistical interpolation technique, has been proved to be sufficiently robust for estimating values with finite sampled data in most of the cases. In this study, ordinary kriging interpolation integrate with 3D visualization methods is applied to characterize the monochlorobenzene contaminated soil for an agrochemical industrial site located in Jiangsu province. Based on 944 soil samples collected by Geoprobe 540MT and monitored by SGS environmental monitoring services, 3D visualization in terms of the spatial distribution of pollutants in potentially contaminated soil, the extent and severity of the pollution levels in different layers, high concentration levels and isolines of monochlorobenzene concentrations in this area are provided. From the obtained results, more information taking into account the spatial heterogeneity of soil area will be helpful for decision makers to develop and implement the soil remediation strategy in the future.
Źródło:
Archives of Environmental Protection; 2016, 42, 3; 17-24
2083-4772
2083-4810
Pojawia się w:
Archives of Environmental Protection
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Catalytic oxidation of lignin to aromatics over salen-porphyrin complex as a biomimetic catalyst
Autorzy:
Lu, X.-J.
Zhou, X.-F.
Zhu, Z.-L.
Sun, Y.
Tang, K.
Lei, F.-H.
Liu, Z.-G.
Wang, T.
Powiązania:
https://bibliotekanauki.pl/articles/52771.pdf
Data publikacji:
2019
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Technologii Drewna
Źródło:
Drewno. Prace Naukowe. Doniesienia. Komunikaty; 2019, 62, 203
1644-3985
Pojawia się w:
Drewno. Prace Naukowe. Doniesienia. Komunikaty
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Aluminum-Doped Zinc Oxide Thin Films Prepared by Sol-Gel and~RF Magnetron Sputtering
Autorzy:
Wu, G.
Chen, Y.
Lu, H.
Powiązania:
https://bibliotekanauki.pl/articles/1504062.pdf
Data publikacji:
2011-07
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.15.Cd
82.70.Gg
77.55.hf
Opis:
Zinc oxide (ZnO) thin films have become technologically important materials due to their wide range of electrical and optical properties. The characteristics can be further adjusted by adequate doping processes. In this paper, aluminum-doped zinc oxide thin films have been prepared on glass substrates using a sol-gel route and the radio-frequency magnetron sputtering process. The stoichiometry could be easily adjusted by controlling the nanosized precursor concentration and the thickness by dip-coating cycles. On the other hand, the mixed $N_2O//Ar$ plasma gas provided adequate N doping for the RF sputtering process. The results showed the low electrical resistivity of 21.5 Ω cm with the carrier concentration of - 3.21 × $10^{18} cm^{-3}$ for the n-type aluminium-doped zinc oxide film. They were 34.2 Ω cm and + 9.68 × $10^{16} cm^{-3}$ for the p-type aluminium-doped zinc oxide film. The optical transmittance has been as high as 85-90% in the 400-900 nm wavelength range. The aluminium-doped zinc oxide (2 at.% Al) films exhibited the hexagonal wurzite structure with (002) preferred crystal orientation. The electrical characteristics were depicted by the gradual increase in N and NO that occupy the oxygen vacancies.
Źródło:
Acta Physica Polonica A; 2011, 120, 1; 149-152
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A study of bubble-particle interactions in a column flotation process
Autorzy:
Cheng, G.
Shi, C.
Yan, X.
Zhang, Z.
Xu, H.
Lu, Y.
Powiązania:
https://bibliotekanauki.pl/articles/109635.pdf
Data publikacji:
2017
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
particle
bubble
column flotation
collision
attachment
detachment
Opis:
Bubble-particle interactions play an important role in flotation. This study examines the behaviour of bubble clusters in a turbulent flotation cell. Particularly, the bubble-particle interaction characteristics in flotation are investigated. The bubble size in a flotation column was measured using an Olympus i-SPEED 3 high-speed camera. Relationships between the circulating volume, bubble size and bubble terminal velocity were discussed. Probabilities of collision, attachment, detachment and acquisition between bubbles and particles in different circulating volumes were calculated based on the flotation kinetic theory. Using the extended Derjaguin–Landau–Verwey–Overbeek (EDLVO) theory, the relationship between the potential energy and distance in bubble-particle interaction was analysed. The results demonstrated that as the circulating volume increased, the bubble size and velocity decreased. When the circulating volume increased from 0.253 to 0.495 m3/h, the bubble diameter decreased from 511 to 462 μm, and the corresponding bubble velocity decreased from 43.1 to 37.5 mm/s. When the circulating volume remained constant as the particle size increased, probabilities of collision, attachment, detachment and acquisition increased. When the particle size remained constant as the circulating volume increased, these probabilities also increased. At a constant circulating volume as the particle size increased, the absolute value of the total potential energy between the particle and bubble increased. When the distance between the bubble and particle was 30 nm, the energy barrier appeared.
Źródło:
Physicochemical Problems of Mineral Processing; 2017, 53, 1; 17-33
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A Facile Synthesis of 3,3'-Dinitro-5,5'-diamino-bi-1,2,4-triazole and a Study of Its Thermal Decomposition
Autorzy:
Ma, Q.
Lu, H.
Qu, Y.
Liao, L.
Li, J.
Fan, G.
Chen, Y.
Powiązania:
https://bibliotekanauki.pl/articles/358272.pdf
Data publikacji:
2017
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
3,3’-dinitro-5,5’-diamino-bi-1,2,4-triazole
facile synthesis
DSC-TG
RSFTIR
TG-IR
thermolysis
Opis:
3,3’-Dinitro-5,5’-diamino-bi-1,2,4-triazole (DABNT) was synthesized by a facile method and its crystalline density was determined as 1.839 g·cm−3 at 293(2) K by X-ray diffraction. Its thermal decomposition kinetics and mechanism were studied by means of differential scanning calorimetry-thermogravimetry (DCS-TG), in situ thermolysis by rapid-scan Fourier transform infrared spectroscopy (RSFTIR) and simultaneous TG-IR technology. The results showed that the apparent activation energies obtained by the Kissinger, Ozawa and Starink methods were 122.9 kJ·mol−1, 123.2 kJ·mol−1 and 123.5 kJ·mol−1, respectively. The thermodynamic parameters of ΔS≠, ΔH≠ and ΔG≠ were −37.5 J·K−1·mol−1, 118.4 kJ·mol−1 and 138.7 kJ·mol−1, respectively. The decomposition reaction process of DABNT starts with the transformation from a primary amine to a secondary amine and then the loss of one nitro-group from the DABNT structure. Gaseous products, such as N2O and H2O, were detected from decomposition in the range of 50-300 °C. Density functional theory (DFT) calculations were further employed to illustrate the decomposition mechanism. The above-mentioned information on the synthesis and thermal behaviour is quite useful for the scale-up and evaluation of the thermal safety of DABNT.
Źródło:
Central European Journal of Energetic Materials; 2017, 14, 2; 281-295
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 16

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