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Tytuł:
Improving the Adhesion Strength of Polypropylene Nonwoven Laminated Fabrics Using Low-Pressure Plasma
Badanie właściwości fizycznych i geometrycznych dzianin pojedynczych lewo-prawych z udziałem przędz rdzeniowych elastomerowych
Autorzy:
Armağan, O. G.
Kayaoğlu, B. K.
Karakaş, H. C.
Güner, F. S.
Powiązania:
https://bibliotekanauki.pl/articles/233275.pdf
Data publikacji:
2013
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Biopolimerów i Włókien Chemicznych
Tematy:
plasma treatment
adhesion strength
polypropylene
nonwoven
laminated fabric
obróbka plazmowa
siły adhezji
polipropylen
włóknina
laminowana tkanina
Opis:
In this study, the adhesion strength properties of laminated polypropylene nonwoven fabrics treated with low-temperature, low-pressure, radio frequency argon plasma were investigated. The change in wettability was determined by water contact angle measurements. In order to observe the effect of plasma treatment on the washing resistance of the laminated samples, washing treatment by means of 10 wash cycles was also carried out. After the peel-off test, the remaining adhesives on the peeled surfaces were examined by SEM images in order to see the effect of plasma treatment. Contact angles of highly hydrophobic polypropylene nonwoven samples decreased by increasing the plasma exposure time and discharge power. The peel bond strength of the plasma treated laminated fabrics improved by up to 150% compared to the untreated fabrics. SEM and AFM analyses also showed that the surface roughness increased due to the etching effect of the plasma treatment, leading to the improvement of the mechanical adhesion of the polypropylene nonwoven fabrics.
Głównym celem badań była ocena możliwości zastosowania przy produkcji dzianin na maszynach cylindrycznych bawełnianych przędz rdzeniowych elastomerowych jako alternatywę dla stosowania gołych przędz elastomerowych. Badano również wpływ długości splotu na geometrie i jakość dzianin, w tym na gęstość rządków i kolumienek, gęstość splotów i gęstość powierzchniową przy rożnych stanach relaksacji. Uzyskane wyniki wyraźnie wskazują, że proponowana przędza nadaje się jak najbardziej do projektowanego zastosowania. Stwierdzono również, że zmiany długości splotu nie mają wyraźnego wpływu na gęstość kolumienkową. Jednocześnie stwierdzono, że geometryczne właściwości próbek są odwrotnie proporcjonalne do długości splotu. Badano również zdolność próbek do osiągnięcia geometrycznej równowagi po kolejnych powtarzanych cyklach prania i suszenia. Stwierdzono, że wszystkie wyprodukowane próbki uzyskiwały stabilność wymiarową przed piątym cyklem prania i suszenia, w tym również te, które miały najmniejszą długość splotu.
Źródło:
Fibres & Textiles in Eastern Europe; 2013, 3 (99); 96-101
1230-3666
2300-7354
Pojawia się w:
Fibres & Textiles in Eastern Europe
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Shot Peening With Glass Microspheres on the Fatigue Behavior of a Low Carbon Steel
Autorzy:
de Lacerda, J. C.
Pereira, I. R.
Costa, J. M. G.
Pinto, J. S.
Souza, H. F. M.
Fonseca, M. A.
Powiązania:
https://bibliotekanauki.pl/articles/352156.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
fatigue
shot peening
Wöhler curve
low carbon steel
glass microspheres
Opis:
The present work has the objective of studying the effect of shot peening with glass microspheres on SAE 1020 steel in its resistance to fatigue. Fatigue tests were carried out by rotary bending with load control and loading on balance in specimens with and without shot peening. A rotation speed of approximately 750 rpm (12.5 Hz) was employed in the fatigue tests. Vickers microhardness tests were performed in order to verify the surface hardening produced by shot peening with glass microspheres. Analysis of the steel surface and fatigue fractures was performed using scanning electron microscopy (SEM). Fatigue tests were performed in order to obtain S-N curves (Wöhler curves). It was observed that shot peening with glass microspheres improved the fatigue strength of the steel at high cycle.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 4; 1513-1518
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fluorescence Correlation and Low Temperature Linewidth of Single Defect Centers in Diamond
Autorzy:
Dräbenstedt, A.
Tietz, C.
Jelezko, F.
Wrachtrup, J.
Kilin, S.
Nizovtzev, A.
Powiązania:
https://bibliotekanauki.pl/articles/2011145.pdf
Data publikacji:
1999-11
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
78.20.-e
42.30.Yc
Opis:
Low temperature fluorescence excitation spectroscopy was carried out on single nitrogen vacancy defect centers. At temperatures below 90 K the fluorescence intensity of individual centers drastically diminishes because of the population of a metastable singlet state in near resonance with the optically excited state. Low temperature fluorescence excitation spectroscopy down to 5 K becomes possible via deshelving of this state with a second laser source. Surprisingly individual centers reveal low temperature fluorescence excitation line widths around 0.6 meV.
Źródło:
Acta Physica Polonica A; 1999, 96, 5; 665-675
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Hardening pretreatment by drought and low temperature enhanced chilling stress tolerance of cucumber seedlings
Autorzy:
Ghanbari, F.
Kordi, S.
Powiązania:
https://bibliotekanauki.pl/articles/12297131.pdf
Data publikacji:
2019
Wydawca:
Uniwersytet Przyrodniczy w Lublinie. Wydawnictwo Uniwersytetu Przyrodniczego w Lublinie
Tematy:
plant cultivation
cucumber plant
plant seedling
plant hardening
plant tolerance
pretreatment
chilling stress
drought
low temperature
Opis:
Chilling stress is of major limiting factors influencing the growth and development of warm-season crops like cucumber. In this research, the possibility of chilling tolerance of cucumber seedlings was investigated through employing the drought and low-temperature pretreatments. The factorial experiment consisted of two factors including cucumber cultivars (i.e. ‘Super Dominos’ and ‘Super Star’) and hardening treatments (control, low temperatures at 10°C, and 15°C and drought simulated by 10% and 20% PEG) based on completely randomized design (CRD) in 3 replications. After applying treatments and providing them 48 h opportunity to be recovered, the seedlings were subjected to 3°C for a six-day period and 6 h for each day. All hardening treatments improved seedlings’ growth, chlorophyll content, total phenol (TP) and antioxidant enzyme activities, while reducing chilling injury index and malondialdehyde (MDA) content. Comparing to temperature hardening, the drought pretreatment showed to have a better effect on inducing the chilling tolerance into cultivars. Overall, the results of this experiment showed that employing drought and low-temperature pretreatments enabled cucumber seedlings to mitigate the harmful effects of chilling.
Źródło:
Acta Scientiarum Polonorum. Hortorum Cultus; 2019, 18, 2; 29-37
1644-0692
Pojawia się w:
Acta Scientiarum Polonorum. Hortorum Cultus
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Magnetic Properties of GaMnAs Single Layers and GaInMnAs Superlattices Investigated at Low Temperature and High Magnetic Field
Autorzy:
Hernandez, C.
Terki, F.
Charar, S.
Sadowski, J.
Maude, D.
Stanciu, V.
Svedlindh, P.
Powiązania:
https://bibliotekanauki.pl/articles/2036030.pdf
Data publikacji:
2003-06
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.50.Pp
75.70.-i
Opis:
Magnetotransport properties of GaMnAs single layers and InGaMnAs/InGaAs superlattice structures were investigated at temperatures from 4 K to 300 K and magnetic fields up to 23 T to study the influence of carriers confinement through different structures. Both single layers and superlattice structures show paramagnetic-to-ferromagnetic phase transition. In GaMnAs/InGaAs superlattice beside the Curie temperature (T$\text{}_{c}$≈40 K), a new phase transition is observed close to 13 K.
Źródło:
Acta Physica Polonica A; 2003, 103, 6; 613-619
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
LMPP Effects on Morphology, Crystallization, Thermal and Mechanical Properties of iPP/LMPP Blend Fibres
Wpływ polipropylenu o małej masie cząsteczkowej (LMPP) na morfologię, krystalizację, właściwości termiczne i mechaniczne włókien mieszanych iPP/LMPP.
Autorzy:
Hussain, M.
Zhu, F.
Yu, B.
Han, J.
Memon, H.
Yasin, S.
Powiązania:
https://bibliotekanauki.pl/articles/232887.pdf
Data publikacji:
2018
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Biopolimerów i Włókien Chemicznych
Tematy:
polypropylene
iPP/LMPP blends
morphology
crystallinity
low molecular low modulus polypropylene
polipropylen
mieszanki iPP-LMPP
morfologia
krystaliczność
niski poziom cząsteczkowy
polipropylen o niskim module sprężystości
Opis:
The thermal properties and morphological characterisation of isotactic polypropylene (iPP) homopolymer and its blends with low molecular low modulus polypropylene (LMPP) were studied. Firstly blends were prepared with variant LMPP contents, and their properties were characterised using SEM, DSC, XRD, and DMA. Later the mechanical properties of iPP/LMPP blend fibres were investigated. SEM results showed that the iPP/LMPP blends produced smoother surfaces when the LMPP content was increased, as well as the miscibility. All the Tg values with different LMPP percentages were in-between pure iPP and LMPP. The XRD results indicated the LMPP percentage decreased along with the degree of crystallinity of the iPP/LMPP blends (5% to 15%), which increased and then decreased as compared to pure iPP. The elongation at break increased when the LMPP content increased, with the maximum elongation at break of the LMPP 25% blend reaching 12.95%, which showed great stretch-ability, whereas the elastic modulus of iPP/LMPP blends decreased.
W pracy badano właściwości termiczne i morfologię homopolimeru izotaktycznego polipropylenu (iPP) i jego mieszanek z polipropylenem o małej masie cząsteczkowej (LMPP). Zastosowano następujące proporcje mieszania iPP/LMPP (wt/wt): 95/5, 90/10, 85/15, 80/20 i 75/25, zdefiniowano je odpowiedni: 5%, 10%, 15 %, 20% i 25%. Właściwości włokien mieszanych iPP/LMPP porównano do właściwości czystego PP i LMPP. Włókna mieszane zbadano za pomocą SEM, DSC, XRD i DMA. Następnie zbadano mechaniczne właściwości włókien iPP/LMPP. Wyniki SEM wykazały, że wraz ze zwiększeniem zawartości LMPP powierzchnia włókien charakteryzowała się większą gładkością. Wszystkie wartości Tg włókien mieszanych były pośrednie pomiędzy czystym iPP i LMPP. Stwierdzono, że wydłużenie przy zerwaniu zwiększyło się wraz ze wzrostem zawartości LMPP, przy maksymalnym wydłużeniu przy zerwaniu 12,95%, dla włókien z zawartością 25% LMPP, co wskazywało na dużą rozciągliwość, podczas gdy moduł sprężystości wzdłużnej włókien iPP / LMPP zmniejszył się.
Źródło:
Fibres & Textiles in Eastern Europe; 2018, 2 (128); 26-31
1230-3666
2300-7354
Pojawia się w:
Fibres & Textiles in Eastern Europe
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Development of a Low Noise and Low Energy Consumption Alpha Spectroscopy Amplifier for ²²²Rn Gas Detection
Autorzy:
Kuluöztürk, M. F.
Özgen, S.
Doğru, M.
Powiązania:
https://bibliotekanauki.pl/articles/1047518.pdf
Data publikacji:
2017-09
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
29.30.Aj
Opis:
²²²Rn gas is a member of ²³⁸U decay chain, which is the most abundant in nature, and decays by releasing alpha particles with energy of 5.49 MeV. Various detection systems are used for radon gas detection in the research of natural radioactivity, health, geophysics etc. The detection systems need some electronics layers, like amplifier, analyser and data storage unit. These systems generally use mains voltage or self-battery and they are not useful for long-term field research because of energy consumption, which is relatively high. In this study, the development of a low energy consumption and low noise spectroscopy amplifier system for the detection of α radiation emitted by ²²²Rn and its daughters is presented. Amplifying and pulse shaping stages were developed with nuclear electronic methods. Operating performance of amplifying and pulse shaping stages has been demonstrated with a series of electronic and radioactive tests (gain test, signal to noise ratio measurement, electronics calibration and energy calibration). Additionally, nuclear spectroscopic studies were performed for comparison of this system with other alpha spectroscopy systems.
Źródło:
Acta Physica Polonica A; 2017, 132, 3; 789-791
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A novel high-swing high-speed with 187 µW power consumption Common-Mode Feedback Block (CMFB) based on rail-to-rail technique
Autorzy:
Mahdavi, S.
Noruzpur, F.
Ghadimi, E.
Khanshan, T. M.
Powiązania:
https://bibliotekanauki.pl/articles/397734.pdf
Data publikacji:
2017
Wydawca:
Politechnika Łódzka. Wydział Mikroelektroniki i Informatyki
Tematy:
common-mode feedback
high-speed
low voltage
folded cascode
high swing
sprzężenie zwrotne dla sygnału wspólnego
niskie napięcie
kaskoda odwrócona
Opis:
This paper presents a new high-swing, high-speed and low power continuous-time Common-Mode Feedback Block (CMFB) based on rail-to-rail technique. The main purposes of the proposed idea are to achieve high-speed, low settling time error, large output swing, and low power as well. Moreover, applying the worst case simulation (initial condition 0 and 1.8 volts) on the proposed CMFB circuit, the output voltage can be settled in the desired level just after 1.18ns noticeably. The settling time error and the power consumption of the suggested common-mode feedback circuit are just 103|iV and 187µW with the power supply of 1.8 volts respectively. Meanwhile, DC gain and phase margin of the amplifier are 74dB and 67 degree correspondingly, and 0.5pF capacitor load is applied to the output nodes of the amplifier. It is noteworthy that, the proposed idea is a good candidate for low voltage applications too. Because it just needs 2 overdrive voltage (AV) to start its performance. Applying the proposed idea on the folded cascode amplifier it achieves SNDR of 68.68dB with the Effective Number of Bits (ENOB) 11.15 bits respectively. The proposed CMFB occupies an active area of 155.58µm2 (10.56µm*14.73µm). Finally, the proposed structure is simulated in whole process corner condition and different temperatures from -70°C to +70°C. Simulation results are performed using the HSPICE BSIM3 model of a 0.18µm CMOS technology.
Źródło:
International Journal of Microelectronics and Computer Science; 2017, 8, 2; 50-56
2080-8755
2353-9607
Pojawia się w:
International Journal of Microelectronics and Computer Science
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Design and Noise Analysis of a Novel Auto-Zeroing Structure for Continuous-Time Instrumentation Amplifiers
Autorzy:
Maréchal, S.
Nys, O.
Krummenacher, F.
Chevroulet, M.
Kayal, M.
Powiązania:
https://bibliotekanauki.pl/articles/226106.pdf
Data publikacji:
2013
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
front-end
instrumentation amplifier
low-noise
low power
chopper
auto-zero
Opis:
This paper introduces a low-noise, low-power amplifier for high-impedance sensors. An innovative circuit using an auto-zeroed architecture combined with frequency modulation to reject offset and low-frequency noise is proposed and analysed. Special care was given to avoid broadband noise aliasing and chopping in the signal path, and to minimize both the resulting equivalent input offset voltage and equivalent input biasing current. The theoretical noise analysis of the proposed topology covers most of the noise sources of the circuit. Simulations show that the input-referred noise level of the circuit is 13.4nV/√Hz for a power consumption of 85µA with a power supply from 1.8V to 3.6V.
Źródło:
International Journal of Electronics and Telecommunications; 2013, 59, 4; 397-404
2300-1933
Pojawia się w:
International Journal of Electronics and Telecommunications
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Uranium and neodymium partitioning in alkali chloride melts using low-melting gallium-based alloys
Autorzy:
Melchakov, S. Y.
Maltsev, D. S.
Volkovich, V. A.
Yamshchikov, L. F.
Lisienko, D. G.
Osipenko, A. G.
Rusakov, M. A.
Powiązania:
https://bibliotekanauki.pl/articles/146407.pdf
Data publikacji:
2015
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
neodymium
uranium
gallium
separation factor
reductive extraction
pyrochemical reprocessing
Opis:
Partitioning of uranium and neodymium was studied in a ‘molten chloride salt – liquid Ga-X (X = In or Sn) alloy’ system. Chloride melts were based on the low-melting ternary LiCl-KCl-CsCl eutectic. Nd/U separation factors were calculated from the thermodynamic data as well as determined experimentally. Separation of uranium and neodymium was studied using reductive extraction with neodymium acting as a reducing agent. Efficient partitioning of lanthanides (Nd) and actinides (U), simulating fission products and fissile materials in irradiated nuclear fuels, was achieved in a single stage process. The experimentally observed Nd/U separation factor valued up to 106, depending on the conditions.
Źródło:
Nukleonika; 2015, 60, No. 4, part 2; 915-920
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Progress in stellarator research at IPP-Kharkov
Autorzy:
Moiseenko, V. E.
Lozin, O. V.
Shapoval, A. M.
Dreval, M. B.
Kulyk, Y. S.
Mironov, Y. K.
Romanov, V. S.
Pashnev, V. K.
Sorokovoy, E. L.
Petrushenya, A. A.
Ozherel’ev, F. I.
Kozulya, M. M.
Konovalov, V. G.
Maznichenko, S. M.
Garkusha, I. E.
Powiązania:
https://bibliotekanauki.pl/articles/146173.pdf
Data publikacji:
2016
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
stellarator
radio-frequency heating
low frequency modes
magnetic diagnostics
Opis:
A new antenna of ‘crankshaft’ type has been installed in the Uragan-2M device in order to increase the plasma density and heating below the ion cyclotron frequency. Antenna operation is modelled by 1D code, which solves boundary problem for time-harmonic Maxwell’s equations in radially non-uniform plasma cylinder. In recent experiments with this antenna, the SXR, CV, OV and OII emission measurements indicate that the light impurity radiation barrier is overcame at this device. Plasma with a temperature of ~50 eV exists during a short period of a few milliseconds. Then the radiation collapse comes owing to strong infl ux of impurities to the plasma column. A new magnetic diagnostics has been installed at Uragan-3M. Using it the poloidal magnetic fi eld is measured and the shift of toroidal current in major radius is registered. A miniature pinhole camera array for spatially and temporally resolved measurements of soft X-ray (SXR) plasma emission has been recently installed on the U-3M. Different shapes of the SXR emission profi le has been observed in different discharge conditions.
Źródło:
Nukleonika; 2016, 61, 2; 91-97
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A longitudinal assessment of myoelectric activity, postural sway, and low-back pain during pregnancy
Autorzy:
Moreira, L. S.
Elias, L. A.
Gomide, A. B.
Vieira, M. F.
Do Amaral, W. N.
Powiązania:
https://bibliotekanauki.pl/articles/307463.pdf
Data publikacji:
2017
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
elektromiografia
stabilność postawy
bóle kręgosłupa
electromyography
low back pain
postural balance
pregnancy trimesters
stabilometry
Opis:
The present study aimed at investigating the control of upright quiet standing in pregnant women throughout pregnancy, and whether low-back pain exerts influence on this motor task. Methods: Myoelectric signals from postural muscles and stabilometric data were collected from 15 non-pregnant and 15 pregnant women during upright quiet standing. Electromyogram envelopes and center of pressure metrics were evaluated in the control group, as well as in pregnant women in their first and third trimester of pregnancy. A correlation analysis was performed between the measured variables and a low-back pain disability index. Results: Pregnant women exhibited a decreased maximum voluntary isometric activity for all postural muscles evaluated. Additionally, the activity of lumbar muscles during the postural task was significantly higher in the pregnant women in comparison to the non-pregnant controls. The soleus muscle maintained its activity at the same level as the gestation progressed. Higher postural oscillations were observed in the anteroposterior direction while mediolateral sway was reduced in the third trimester of pregnancy. No correlation was detected between the lowback pain disability index and neuromechanical variables. Conclusion: This study provides additional data regarding the functioning and adaptations of the postural control system during pregnancy. Also, we provide further evidence that postural control during quiet standing cannot be used to predict the occurrence of low-back pain. We hypothesize that the modifications in the neural drive to the muscles, as well as in postural sway may be related to changes in the biomechanics and hormonal levels experienced by the pregnant women.
Źródło:
Acta of Bioengineering and Biomechanics; 2017, 19, 3; 77-83
1509-409X
2450-6303
Pojawia się w:
Acta of Bioengineering and Biomechanics
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Hygiene condition of water use and sanitation facilities at urban slums: analysis of port city Chittagong, Bangladesh
Wyposażenie sanitarne w slamsach miejskich - analiza na podstawie miasta portowego Chittagong, Bangladesh
Autorzy:
Muhit, I. B.
Chowdhury, S. T.
Nahid, N.
Zaman, M. F.
Powiązania:
https://bibliotekanauki.pl/articles/396534.pdf
Data publikacji:
2015
Wydawca:
Uniwersytet Zielonogórski. Oficyna Wydawnicza
Tematy:
sanitation condition
hygiene
low income community
water supply
latrine systems
warunki sanitarne
higiena
zaopatrzenie w wodę
system odprowadzania ścieków
niskie dochody
Opis:
Low income community development is the prerequisite for the overall development of a society. There are different kinds of parameters to widen community development, such as health, economic, social, a living pattern, etc. Sanitation condition is the crucial aspect that is directly or indirectly inter bond with all the parameters. To see the exact reasons behind brutal unhygienic sanitation conditions of water supply and latrine system in a low cost community, the Chittagong City Corporation area has been picked. Relevant data have been collected from field survey, consultancy with inhabitants, Chittagong City Corporation, Power Development Board, and WASA. To know the possible reasons behind the water supply and germ-infested sanitation, state of a low cost community, this paper attempts to shed some light on the tribulations behind the scarcity of safe drinking water, dirt free a as well as sustainable latrine and drainage system and offensive water management.
Obszary takie jak rozwój gospodarczy, bariery społeczne, standard życia i zdrowie, ściśle związane są ze stanem wyposażenia sanitarnego. W artykule dokonano analizy warunków sanitarnych związanych z zaopatrzeniem w wodę i odprowadzeniem ścieków dla społeczności o niskich dochodach w obszarze Chittagong City Corporation. Dane zostały zebrane podczas ankietowych badań terenowych, rozmów z mieszkańcami, z bazy Chittagong City Corporation, Power Development Board i WASA.
Źródło:
Civil and Environmental Engineering Reports; 2015, 16; 153-166
2080-5187
2450-8594
Pojawia się w:
Civil and Environmental Engineering Reports
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Magnetic Response of Mn(III)F(salen) at Low Temperatures
Autorzy:
Park, J.
Risset, O.
Shiddiq, M.
Peprah, M.
Knowles, E.
Andrus, M.
Beedle, C.
Ehlers, G.
Podlesnyak, A.
Čižmár, E.
Nagler, S.
Hill, S.
Talham, D.
Meisel, M.
Powiązania:
https://bibliotekanauki.pl/articles/1368508.pdf
Data publikacji:
2014-07
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.50.Ee
78.70.Nx
76.30.-v
75.10.Jm
Opis:
The low temperature magnetic response of Mn(III)F(salen), salen = $H_{14}C_{16}N_{2}O_{2}$, an S=2 linear-chain system, has been studied. Using a single crystal with the field applied perpendicular to the chain direction, torque magnetometry, down to 20 mK and up to 18 T, revealed a feature at 3.8 T when T ≤ 400 mK. ESR ( ≈200 GHz) studies, using single crystals at 4 K and in 5 T, have not detected any signal. In 10 mT, the temperature dependence of the susceptibility of powder-like samples can be reasonably fit when J/$k_{B}$=50 K and g=2. In addition, these data are unchanged for P ≤1.0 GPa. Using a randomly-oriented, powder-like, deuterated (12 of 14 H replaced by D) sample of 2.2 g at 270 mK, neutron scattering data, acquired with the Cold Neutron Chopper Spectrometer at the Spallation Neutron Source, show several well defined excitations that may be from the zero-field energy levels of antiferromagnetic S=2 spins with g=2, J/$k_{B}$=50 K, D/$k_{B}$=2.8 K, and E/$k_{B}$=0.5 K.
Źródło:
Acta Physica Polonica A; 2014, 126, 1; 228-229
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
In situ thermal decomposition route: Preparation and characterization of nano nickel, cobalt, and copper oxides using an aromatic amine complexes as a low-cost simple precursor
Autorzy:
Refat, Moamen S.
Mohamed, Soha F.
Altalhi, Tariq A.
Bakare, Safyah B.
Al-Hazmi, Ghaferah H.
Powiązania:
https://bibliotekanauki.pl/articles/1849310.pdf
Data publikacji:
2021
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
o-tolidine
NiO
Co3O4
CuO
XRD
TEM
nanoparticles
complexation
Opis:
The main interest now is the development of metallic or inorganic-organic compounds to prepare nanoparticle materials. The use of new compounds could be beneficial and open a new method for preparing nanomaterials to control the size, shape, and size of the nanocrystals. In this article, the thermal decomposition of [M2(o-tol)2(H2O)8]Cl4 (where o-tol is ortho-tolidine compound, M = Ni2+, Co2+, Cu2+) new precursor complex was discussed in solid-state conditions. The thermal decomposition route showed that the synthesized three complexes were easily decomposed into NiO, Co3O4 and CuO nanoparticles. This decomposition was performed at low temperatures (~600°C) in atmospheric air without using any expensive and toxic solvent or complicated equipment. The obtained product was identified by Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD), transmission electron microscopy (TEM) and energy-dispersive X-ray spectroscopy (EDX). FT-IR, XRD and EDX analyses revealed that the NiO nanoparticles exhibit a face-centered-cubic lattice structure with a crystallite size of 9–12 nm. The formation of a highly pure spinel-type Co3O4 phase with cubic structure showed that the Co3O4 nanoparticles have a sphere-like morphology with an average size of 8–10 nm. The XRD patterns of the CuO confirmed that the monoclinic phase with the average diameter of the spherical nanoparticles was approximately 9–15 nm.
Źródło:
Polish Journal of Chemical Technology; 2021, 23, 2; 47-53
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 23

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