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Wyświetlanie 1-15 z 44
Tytuł:
Effect of Surfactant Addition on Bi2Te3 Nanostructures Synthesized by Hydrothermal Method
Autorzy:
Dharmaiah, P.
Lee, C. H.
Madavali, B.
Hong, S.-J.
Powiązania:
https://bibliotekanauki.pl/articles/351609.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
bismuth telluride
hydrothermal synthesis
spark plasma sintering
thermoelectric materials
X-ray diffraction
Opis:
In the present work, we have prepared Bi2Te3 nanostructures with different morphologies such as nano-spherical, nanoplates and nanoflakes obtained using various surfactant additions (EG, PVP, and EDTA) by a hydrothermal method. The shape of the nanoparticles can be controlled by addition of surfactants. The samples were characterized by x-ray diffraction (XRD) and scanning electron microscopy (SEM). It is found that the minority BiOCl phase disappears after maintained pH at 10 with EG as surfactant. SEM bulk microstructure reveals that the sample consists of fine and coarse grains. Temperature dependence of thermoelectric properties of the nanostructured bulk sample was investigated in the range of 300-450K. The presence of nanograins in the bulk sample exhibits a reduction of thermal conductivity and less effect on electrical conductivity. As a result, a figure of merit of the sintered bulk sample reached 0.2 at 400 K. A maximum micro Vickers hardness of 102 Hv was obtained for the nanostructured sample, which was higher than the other reported results.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1005-1010
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Characterization of Cladding Hull Wastes from Used Nuclear Fuels
Charakterystyka odpadów z okładzin reaktora wodnego ciśnieniowego
Autorzy:
Kang, K. H.
Lee, C. H.
Jeon, M. K.
Han, S. Y.
Park, G. I.
Hwang, S.-M.
Powiązania:
https://bibliotekanauki.pl/articles/357036.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
used nuclear fuels
metal waste
cladding hulls
zircaloy
radioactivity
reaktor wodny ciśnieniowy
odpady metalowe
odpady z okładzin
radioaktywność
Opis:
Used cladding hulls from pressurized water reactor (PWR) are characterized to provide useful information for the treatment and disposal of cladding hull wastes. The radioactivity and the mass of gamma emitting nuclides increases with an increase in the fuel burn-up and their removal ratios are found to be more than 99 wt.% except Co-60 and Cs-137. In the result of measuring the concentrations of U and Pu included in the cladding hull wastes, most of the residues are remained on the surface and the removal ratio of U and Pu are revealed to be over 99.98 wt.% for the fuel burn-up of 35,000 MWd/tU. An electron probe micro-analyzer (EPMA) line scanning shows that radioactive fission products are penetrated into the Zr oxide layer, which is proportional to the fuel burn-up. The oxidative decladding process exhibits more efficient removal ratio of radionuclides.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1199-1203
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Trace Elements (Co, Cr) on the Microstructure and Physical Properties of Al-Si-Cu-Mg-Fe Extruded Alloy
Autorzy:
Ahn, S. S.
Sharief, P.
Lee, C. H.
Son, H. T.
Kim, Y. H.
Kim, Y. C.
Hong, S.
Hong, S. J.
Powiązania:
https://bibliotekanauki.pl/articles/352787.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Al-Si alloy
microstructure
extrusion
coefficient of thermal expansion
trace elements
Opis:
Trace elements Co, Cr were added to investigate their influence on the microstructure and physical properties of Al-Si extruded alloy. The Co, Cr elements were randomly distributed in the matrix, forms intermetallic phase and their existence wereconfirmed by XRD, EDS and SEM analysis. With addition of trace elements, the microstructure was modified, Si particle size was reduced and the growth rate of β-(Al5 FeSi) phase limited. Compared to parent alloy, hardness and tensile strength were enhanced while the linear coefficient of thermal expansion (CTE) was significantly reduced by 42.4% and 16.05% with Co and Cr addition respectively. It is considered that the low CTE occurs with addition of Co was due to the formation of intermetallic compound having low coefficient of thermal expansion. The results suggested that Co acts as an effective element in improving the mechanical properties of Al-Si alloy.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 3; 857-862
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis, Structure, Photoluminescence, and Raman Spectrum of Indium Oxide Nanowires
Autorzy:
Kim, H.
Na, H.
Yang, J.
Lee,, C.
Powiązania:
https://bibliotekanauki.pl/articles/1505485.pdf
Data publikacji:
2011-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.07.-b
78.55.-m
Opis:
Production of indium oxide $(In_2O_3)$ whiskers at a very low temperature of 650°C was reported. The synthetic route was comprised of a thermal heating process of a mixture of In and Mg powders. We have investigated the structural properties of the as-synthesized nanowires by using X-ray diffraction and scanning electron microscopy. The product consisted of one-dimensional nanowires, with a crystalline cubic structure of $In_2O_3$. The photoluminescence measurement with the Gaussian fitting exhibited visible light emission bands centered at 2.1 eV and 2.8 eV. The peaks of the Raman spectrum were indexed to the modes being associated with cubic $In_2O_3$.
Źródło:
Acta Physica Polonica A; 2011, 119, 2; 143-145
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Development of a high-speed air bearing spindle
Autorzy:
Ha, Y.-H.
Lee, D.-W.
Hwang, Y.-K.
Lee, C.-M.
Powiązania:
https://bibliotekanauki.pl/articles/1429126.pdf
Data publikacji:
2008
Wydawca:
Wrocławska Rada Federacji Stowarzyszeń Naukowo-Technicznych
Tematy:
aerostatic bearing
metal foam
porous thrust bearing
porous radial bearing
Opis:
This paper investigates an air spindle with both radial and thrust air bearings of newly developing one-directional porous materials. At present, orifice type and porous type are adopted for thrust air bearings. Orifice type thrust air bearing is fabricated by machining several micro-holes on a bearing pad bearing, permeability significantly affected by particle size and machining conditions is an important factor of performance, but it is hard to c porosities is suggested. It has many micro-porosities through axial direction, so stable and plenty of air can be supplied to the thrust bearing pad. A radial air bearing also can be substituted by a radial direction porous bearing as the same reason. In case of driving parts, built-in motor type is widely applied. But it needs additional cooling parts to drop heat from a motor. So application of an air turbine drive with light-weight shaft is suggested and additionally it will reduce fabricating cost.
Źródło:
Journal of Machine Engineering; 2008, 8, 4; 25-31
1895-7595
2391-8071
Pojawia się w:
Journal of Machine Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Biological Evaluation of Anodized Biodegradable Magnesium-Calcium Alloys
Autorzy:
Kim, J.
Lee, J.
Lee, K.
Park, S.
Lim, H.
Park, C.
Bae, J.
Yun, K.
Powiązania:
https://bibliotekanauki.pl/articles/1398763.pdf
Data publikacji:
2016-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
87.85.jj
87.85.J-
Opis:
The objective of this study was to evaluate the biocompatibility of studied binary magnesium-calcium (Mg-Ca) alloys for biodegradable intraosseous implants. Mg is necessary for health and is a non-toxic biodegradable material that decomposes naturally in the body. Nevertheless, Mg has been implicated in problems including diminished physical properties and corrosion resistance when degradation is too rapid prior to bone healing. This study has explored the effect of Ca on the corrosion resistance and biological evaluation after anodizing treatment with different contents of Ca alloy. Binary Mg-0.5Ca, Mg-1Ca and Mg-5Ca alloys were prepared by the casting method under an argon atmosphere and cut into disc-shaped pieces. Pure Mg alloy was used as the control. Anodic oxidation was performed for 15 minutes at a voltage of 120 V using an electrolyte solution containing Ca gluconate, sodium hexametaphosphate, and sodium hydroxide at room temperature. Corrosion resistance was analyzed using a corrosion tester. After a hydrogen evolution test, the surface pattern and phase changes were observed on a scanning electron microscop (SEM) and energy dispersive spectroscop (EDS). Microscopic evaluation of the adhesion and cell biological functions of Mg was conducted by observing the response of human fetal osteoblastic 1.19 cells with regard to changes in surface film properties, depending on the amount of Ca. Our results support the view that in Mg-xCa alloys (x=0.5, 1, 5 wt.%) treated using anodic oxidation, the increasing Ca content controls the rate of decomposition and improves corrosion resistance.
Źródło:
Acta Physica Polonica A; 2016, 129, 4; 728-735
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
AC Microcalorimetry of Superconducting $MgCNi_3$ Single Crystals
Autorzy:
Kačmarčík, J.
Pribulová, Z.
Samuely, P.
Marcenat, C.
Klein, T.
Jang, D.
Lee, H.
Lee, S.
Powiązania:
https://bibliotekanauki.pl/articles/1813689.pdf
Data publikacji:
2008-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
74.70.Ad
74.25.Bt
Opis:
The low-temperature specific heat of single-crystal samples of superconducting $MgCNi_3$ with typical dimensions 200 μm were measured for the first time. A computer controlled ac microcalorimeter using an optical fiber and an infrared light-emitting diode as the heat source was used down to 2 K at magnetic fields up to 8 T. The specific heat data suggest a moderate coupling in $MgCNi_3$.
Źródło:
Acta Physica Polonica A; 2008, 113, 1; 363-366
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Safety Management in a Relationship-Oriented Culture
Autorzy:
Hsu, S. H.
Lee, C. C.
Powiązania:
https://bibliotekanauki.pl/articles/91057.pdf
Data publikacji:
2012
Wydawca:
Centralny Instytut Ochrony Pracy
Tematy:
safety management
safety climate
relationship-oriented culture
high-risk industry
safety culture
Opis:
A relationship-oriented culture predominates in the Greater China region, where it is more important than in Western countries. Some characteristics of this culture influence strongly the organizational structure and interactions among members in an organization. This study aimed to explore the possible influence of relationships on safety management in relationship-oriented cultures. We hypothesized that organizational factors (management involvement and harmonious relationships) within a relationship-oriented culture would influence supervisory work (ongoing monitoring and task instructions), the reporting system (selective reporting), and teamwork (team communication and co-ordination) in safety management at a group level, which would in turn influence individual reliance complacency, risk awareness, and practices. We distributed a safety climate questionnaire to the employees of Taiwanese high-risk industries. The results of structural equation modeling supported the hypothesis. This article also discusses the findings and implications for safety improvement in countries with a relationship-oriented culture.
Źródło:
International Journal of Occupational Safety and Ergonomics; 2012, 18, 1; 35-45
1080-3548
Pojawia się w:
International Journal of Occupational Safety and Ergonomics
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Photoluminescence Studies of Aluminum Nitride Nanowires
Autorzy:
Yang, J.
Na, H.
Kim, H.
Kebede, M.
Choi, R.
Jeong, J.
Lee, C.
Powiązania:
https://bibliotekanauki.pl/articles/1505466.pdf
Data publikacji:
2011-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.07.-b
78.55.-m
Opis:
We report the production of AlN nanowires by the thermal heating method, for exploring their photoluminescence properties. The room-temperature photoluminescence properties were investigated with different annealing environment. While broad emissions with peaks at around 2.45 and 2.95 eV were obtained from both unannealed and annealed samples, the additional 2.1 eV peak was found from the annealed samples. We have suggested the possible emission mechanisms based on the assumption that both 2.45 eV peak and 2.1 eV peak are ascribed to the nitrogen vacancies. Annealing in N_2 environment exhibited lower intensities of 2.45 eV peak and 2.1 eV peak in comparison to those in Ar environment, presumably due to the suppression of nitrogen vacancies.
Źródło:
Acta Physica Polonica A; 2011, 119, 2; 125-127
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Morphology Change Of Si Deposit In Molten Salt Electrorefining
Zmiana morfologii osadu Si podczas elektrorafinacji w stopionych solach
Autorzy:
Ryu, H. Y.
Kwon, S. C.
Han, M. H.
An, Y. S.
Lee, J. S.
Lee, J. H.
Powiązania:
https://bibliotekanauki.pl/articles/354346.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
molten salt
silicon
morphology
electrorefining
current density
sól stopiona
krzem
morfologia
elektrorafinacja
gęstość prądu
Opis:
The effects of processing parameters on the morphology change in a Si deposit recovered by means of molten salt electrorefining are evaluated using electrochemical techniques such as cyclic voltammetry and chronopotentiometry at 800°C. It was found that concentration of K2SiF6 and current density were important parameters in determining deposit size. Higher concentrations of K2SiF6 were effective in coarsening the silicon deposit and decreasing the cell potential. Silicon nanofiber was recovered at 5 wt% of K2SiF6 whereas dense particles were prepared at 30 and 50 wt% of K2SiF6. The morphology of the Si deposit was determined by the concentration of Si in the electrolyte which is related to the formation of crystal and growth of Si. The formation mechanism of the Si deposit was interpreted by using high resolution TEM as well as electrochemical properties.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1491-1497
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Surface Modification of Self-Consolidated Microporous Ti Implant Compacts Fabricated by Electro-Discharge-Sintering in Air
Autorzy:
Jo, Y. J.
Yoon, Y. H.
Kim, Y. H.
Chang, S. Y.
Kim, J. Y.
Lee, Y. K.
Van Tyne, C. J.
Lee, W. H.
Powiązania:
https://bibliotekanauki.pl/articles/356790.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
titanium
implant
porous
sintering
X-ray photoelectron spectroscopy (XPS)
Opis:
A single pulse of 0.75-2.0 kJ/0.7g of atomized spherical Ti powders from 300 mF capacitor was applied to produce a microporous Ti implant compact by electro-discharge-sintering (EDS). A solid core in the middle of the compact surrounded by a microporous layer was found. X-ray photoelectron spectroscopy was employed to study the surface characteristics of the EDS Ti compact and it revealed that Ti, C and O were the main constituents on the surface with a smaller amount of N. The surface was lightly oxidized and was primarily in the form of TiO2 resulting from the air oxidation during EDS processing. The lightly oxidized surface of the EDS compact also exhibited Ti nitrides such as TiN and TiON, which revealed that the reaction between air constituents and the Ti powders even in times as short as 128 msec.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1287-1291
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Supercontinuum fiber laser source for water quality and heavy metals detection
Autorzy:
Teh, P. C.
Ho, Y. H.
Ong, C. E.
Lee, S. C.
Lo, P. K.
Lai, K. C.
Yeap, K. H.
Loh, S. H.
Teh, P. S.
Tey, K. L.
Powiązania:
https://bibliotekanauki.pl/articles/174135.pdf
Data publikacji:
2017
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
supercontinuum generation
master oscillator power amplifier
nonlinear optics
transmittance measurement
heavy metal contaminants
Opis:
We report a compact, all fiber, 150 ps fiber master oscillator power amplifier operating at 1064 nm that has the ability of producing a maximum average output power of 2.16 W with peak power as high as 10 kW. The output from the master oscillator power amplifier is spliced with a highly nonlinear photonic crystal fiber, generating a supercontinuum with an average power of 250 mW at repetition rate of 1 MHz and spectrum bandwidth spanning from 600 to 1700 nm. The developed supercontinuum system is used to detect the presence of heavy metal contaminants in water by a simple light transmittance method to ensure that the water is free from heavy metal contaminants and safe for consumption. The supercontinuum laser source was shone onto a water sample with a detector placed at another end in order to measure the transmitted supercontinuum light. By measuring the amount of light attenuated at particular wavelength, the concentration of heavy metal contaminants present in the water sample could be determined.
Źródło:
Optica Applicata; 2017, 47, 3; 445-456
0078-5466
1899-7015
Pojawia się w:
Optica Applicata
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 44

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