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    Wyświetlanie 1-9 z 9
    Tytuł:
    Instrumental neutron activation analysis (INAA) for steel analysis and certification
    Autorzy:
    Polkowska-Motrenko, H.
    Chajduk, E.
    Danko, B.
    Powiązania:
    https://bibliotekanauki.pl/articles/147648.pdf
    Data publikacji:
    2011
    Wydawca:
    Instytut Chemii i Techniki Jądrowej
    Tematy:
    steel analysis
    neutron activation analysis (NAA)
    proficiency testing/interlaboratory comparison (PT/ILC)
    certification of steel reference materials
    Opis:
    Instrumental neutron activation analysis (INAA) procedure of elemental steel analysis has been elaborated. The reliability of results obtained by the described procedure has been proved in the frame of different proficiency testing/interlaboratory comparison (PT/ILC) programmes, in which the Institute of Nuclear Chemistry and Technology (INCT, Warsaw) took part since 2005. This work summarizes participation of INCT in these exercises and demonstrates the usefulness of INAA to the certification of steel reference materials.
    Źródło:
    Nukleonika; 2011, 56, 4; 311-315
    0029-5922
    1508-5791
    Pojawia się w:
    Nukleonika
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Application of neutron activation for investigation of Fe3O4 nanoparticles accumulation by plants
    Autorzy:
    Bystrzejewska-Piotrowska, G.
    Asztemborska, M
    Stęborowski, R.
    Polkowska-Motrenko, H.
    Danko, B.
    Ryniewicz, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/146840.pdf
    Data publikacji:
    2012
    Wydawca:
    Instytut Chemii i Techniki Jądrowej
    Tematy:
    iron (II,III) oxide
    nanoparticles
    neutron activation
    plants
    Opis:
    As a result of the rapid development of nanotechnology and increasing application of nanoproducts in many areas of everyday life, there is a growing risk of production of nanowastes potentially dangerous for the environment. This makes it necessary to investigate the accumulation and toxicity of nanoparticles (NPs) at different trophic levels. In the studies neutron activation was applied for the investigation of iron (II,III) oxide nanoparticle (Fe3O4-NPs) accumulation by Lepidium sativum and Pisum sativum L. Plants were cultivated on growth medium contaminated with different concentrations (0.01-10 mmolźL-1) of Fe3O4-NPs. For the identification of the presence of Fe3O4-NPs in plant tissues gamma spectrometry following iron oxide (II,III) nanoparticles irradiation was applied. Both plant species were found to accumulate iron (II,III) oxide nanoparticles. The highest content of NPs was found in plant roots, reaching 40 g/kg for Pisum sativum L. More than 90% of accumulated NPs were found in roots. Accumulation of Fe3O4-NPs was found to depend on the concentration of nanostructures in the growth medium. The transfer factor for Lepidium sativum roots and shoots and Pisum sativum L. shoots decreased with increasing NP concentration in the medium; for Pisum sativum L. roots the tendency was reversed. Neutron activation of nanoparticles was shown to be a powerful tool for tracing the environmental fate of NPs and their uptake and accumulation in organisms.
    Źródło:
    Nukleonika; 2012, 57, 3; 427-430
    0029-5922
    1508-5791
    Pojawia się w:
    Nukleonika
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    A study on chemical composition of Baszkówka and Mt. Tazerzait chondrites
    Autorzy:
    Dybczyński, R.
    Chwastowska, J.
    Danko, B.
    Kulisa, K.
    Polkowska-Motrenko, H.
    Samczyński, Z.
    Sterlińska, E.
    Szopa, Z.
    Powiązania:
    https://bibliotekanauki.pl/articles/2059297.pdf
    Data publikacji:
    2001
    Wydawca:
    Państwowy Instytut Geologiczny – Państwowy Instytut Badawczy
    Tematy:
    Baszkówka
    Tazerzait Mountains
    meteorites
    chondrites
    neutron activation analysis
    speciation
    cosmochemistry
    Opis:
    The elemental contents of two new meteorites, Baszkówka (Poland, 1994) and Mt.Tazerzait (Niger, 1991), were studied by instrumental and radiochemical neutron activation analysis (NAA), supplemented in the case of some elements by gravimetric, titrimetric, spectrophotometric and atomic absorption spectrometric measurements. In total 28 elements were determined for each meteorite. A striking similarity in the bulk chemical composition of the two meteorites was observed. In the case of Baszkówka some study of the elemental contents of the magnetic fraction and the distribution of elements between kamacite and taenite phases was also made. This study confirms that Baszkówka and Mt. Tazerzait are generally more similar to L chondrites than to any other class of chondrites. However both meteorites show also some distinctive features (e.g very low Hg content), distinguishing them from all other L chondrites known. Both meteorites may derive from a common parent body, which may be different from that typical for other chondrites.
    Źródło:
    Geological Quarterly; 2001, 45, 3; 289-302
    1641-7291
    Pojawia się w:
    Geological Quarterly
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Dictyonema black shale and Triassic sandstones as potential sources of uranium
    Autorzy:
    Kiegiel, K.
    Zakrzewska-Kołtuniewicz, G.
    Gajda, D.
    Miśkiewicz, A.
    Abramowska, A.
    Biełuszka, P.
    Danko, B.
    Chajduk, E.
    Wołkowicz, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/147500.pdf
    Data publikacji:
    2015
    Wydawca:
    Instytut Chemii i Techniki Jądrowej
    Tematy:
    uranium ores
    leaching
    extraction
    ion-exchange chromatography
    precipitation
    Opis:
    The main objective of the present study was an assessment of the possibility of uranium recovery from domestic resources in Poland. In the fi rst stage uranium was leached from the ground uranium ore by using acidic (sulfuric acid or hydrochloric acid) or alkaline (carbonate) solutions. The leaching efficiencies of uranium were dependent on the type of ore and it reached 81% for Dictyonemic shales and almost 100% for sandstones. The novel leaching routes, with the application of the helical membrane contactor equipped with rotating part were tested. The obtained postleaching solutions were concentrated and purifi ed using solvent extraction or ion exchange chromatography. New methods of solvent extraction, as well as hybrid processes for separation and purifi cation of the product, were studied. Extraction with the use of membrane capillary contactors that has many advantages above conventional methods was also proposed as an alternative purification method. The fi nal product U3O8 could be obtained by the precipitation of ‘yellow cake’, followed by calcination step. The results of precipitation of ammonium diuranate and uranium peroxide from diluted uranium solution were presented.
    Źródło:
    Nukleonika; 2015, 60, No. 3, part 2; 515-522
    0029-5922
    1508-5791
    Pojawia się w:
    Nukleonika
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Ion exchange investigation for recovery of uranium from acidic pregnant leach solutions
    Autorzy:
    Danko, B.
    Dybczyński, R. S.
    Samczyński, Z.
    Gajda, D.
    Herdzik-Koniecko, I.
    Zakrzewska-Kołtuniewicz, G.
    Chajduk, E.
    Kulisa, K.
    Powiązania:
    https://bibliotekanauki.pl/articles/147778.pdf
    Data publikacji:
    2017
    Wydawca:
    Instytut Chemii i Techniki Jądrowej
    Tematy:
    uranium recovery
    acidic pregnant leach solution
    ion exchange separation
    Opis:
    The article describes studies on the separation of uranium from acid pregnant leach solutions obtained from Polish uranium ores: dictyonema shales and sandstone rocks. Ion exchange chromatography was applied for uranium sorption, using commercially available, strongly basic anion exchanger, Dowex 1. In model experiments, the influence of degree of crosslinking of Dowex 1 on the efficiency of uranium extraction was investigated. The effect of H2SO4 concentration on the breakthrough curve of uranyl ions for the Dowex 1 resins, of different crosslinking: X4, X8 and X10, was examined. Unexpectedly high increase of exchange capacity of uranium was observed in case of Dowex 1X10. This gives potential opportunity of improving the effectiveness of uranium recovery process. Applying column packed with Dowex 1X10, ‘yellow cake’ with ca. 92% yield and high purity of recovered uranium was obtained. A block diagram of the procedure for uranium and lanthanides extraction from acidic leach liquor has been proposed.
    Źródło:
    Nukleonika; 2017, 62, 3; 213-221
    0029-5922
    1508-5791
    Pojawia się w:
    Nukleonika
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The reclamation of spent sand bonded by polymeric binder BioCo2
    Autorzy:
    Grabowska, B.
    Dańko, R.
    Kaczmarska, K.
    Powiązania:
    https://bibliotekanauki.pl/articles/264169.pdf
    Data publikacji:
    2013
    Wydawca:
    Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Wydawnictwo AGH
    Tematy:
    polymer binders
    moulding sands
    used sand
    reclamation
    spoiwo polimerowe
    masa formierska
    masa zużyta
    regeneracja
    Opis:
    Regeneracja zużytego piasku łączonego spoiwem polimerowym BioCo2
    Źródło:
    Metallurgy and Foundry Engineering; 2013, 39, 1; 33-38
    1230-2325
    2300-8377
    Pojawia się w:
    Metallurgy and Foundry Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Analysis of the compounds from the BTEX group, emitted during thermal decomposition of alkyd resin
    Autorzy:
    Kubecki, M.
    Holtzer, M.
    Bobrowski, A.
    Dańko, R.
    Grabowska, B.
    Żymankowska-Kumon, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/380216.pdf
    Data publikacji:
    2012
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    masa formierska
    wiązanie
    BTEX
    analiza termiczna
    GC-MS
    moulding sand
    binding
    thermal analysis
    Opis:
    Suitability of the given binding agent for the moulding sands preparation depends on the one hand on the estimation of technological properties of the sand and the mould made of it and the obtained casting quality and on the other hand on the assessment of this sand influence on the natural and working environment. Out of moulding sands used in the foundry industry, sands with organic binders deserve a special attention. These binders are based on synthetic resins, which ensure obtaining the proper technological properties and sound castings, however, they negatively influence the environment. If in the initial state these resins are not very dangerous for people and for the environment, thus under an influence of high temperatures they generate very harmful products, being the result of their thermal decomposition. Depending on the kind of the applied resin (phenol-formaldehyde, urea, furfuryl, urea-furfuryl, alkyd) under an influence of a temperature such compounds as: furfuryl alcohol, formaldehyde, phenol, BTEX group (benzene, toluene, ethylbenzene, xylene), and also polycyclic aromatic hydrocarbons (PAH) can be formed and released. The aim of the study was the development of the method, selection of analytical methods and the determination of optimal conditions of formation compounds from the BTEX group. An emission of these components constitutes one of the basic criteria of the harmfulness assessment of binders applied for moulding and core sands. Investigations were carried out in the specially designed set up for the thermal decomposition of organic substances in a temperature range: 5000C - 13000C at the laboratory scale. The object for testing was alkyd resin applied as a binding material for moulding sands. Within investigations the minimal amount of adsorbent necessary for the adsorption of compounds released during the decomposition of the resin sample of a mass app. 15 mg was selected. Also the minimal amount of solvent needed for the desorption of compounds adsorbed in the column with adsorbent was found. The temperature range, in which the maximal amounts of benzene, toluene, ethylobenzene and xylenes are released from the resin, was defined. The qualitative and quantitative analyses of compounds from the BTEX group were performed by means of the gas chromatography combined with the mass spectrometry (GC/MS).
    Źródło:
    Archives of Foundry Engineering; 2012, 12, 3; 69-74
    1897-3310
    2299-2944
    Pojawia się w:
    Archives of Foundry Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Analiza związków z grupy BTEX powstających podczas termicznego rozkładu żywicy alkidowej
    Analysis of the compounds from the BTEX group emitted during thermal decomposition of alkyd resin
    Autorzy:
    Kubecki, M.
    Holtzer, M.
    Bobrowski, A.
    Dańko, R.
    Grabowska, B.
    Żymankowska-Kumon, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/381040.pdf
    Data publikacji:
    2012
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    masa formierska
    żywica syntetyczna
    związek BTEX
    rozkład termiczny
    chromatografia gazowa
    spektrometria masowa
    moulding sand
    synthetic resin
    BTEX compounds
    thermal decomposition
    gas chromatography
    mass spectrometry
    Opis:
    Przydatność danego spoiwa do sporządzania mas formierskich obejmuje z jednej strony ocenę właściwości technologicznych samej masy i wykonanej z niej formy i jakości otrzymanego odlewu, a z drugiej strony ocenę wpływu tej masy na środowisko naturalne i środowisko pracy. Z pośród mas stosowanych w przemyśle odlewniczym na szczególną uwagę zasługują masy ze spoiwami organicznymi. Spoiwa te oparte są na żywicach syntetycznych, które z jednej strony zapewniają uzyskanie przez masę odpowiednich właściwości technologicznych i otrzymanie dobrych odlewów, ale z drugiej negatywnie oddziałują na środowisko. O ile w stanie wyjściowym żywice te tylko w niewielkim stopniu stanowią zagrożenie zarówno dla ludzi jak i środowiska, to pod wpływem temperatury generują bardzo szkodliwe produkty, będące wynikiem ich termicznego rozkładu. W zależności od rodzaju stosowanej żywicy (fenolowo-formaldehydowej, mocznikowej, furfurylowej, furfurylowo–mocznikowej, alkidowej) pod wpływem temperatury mogą tworzyć się i uwalniać takie związki jak: alkohol furfurylowy, formaldehyd, fenol, związki z grupy BTEX (benzen, toluen, etylobenzen, ksyleny), a także wielopierścieniowe węglowodory aromatyczne (WWA). [...]
    Suitability of the given binding agent for the moulding sands preparation depends on the one hand on the estimation of technological properties of the sand and the mould made of it and the obtained casting quality and on the other hand on the assessment of this sand influence on the natural and working environment. Out of moulding sands used in the foundry industry, sands with organic binders deserve a special attention. These binders are based on synthetic resins, which ensure obtaining the proper technological properties and sound castings, however, they negatively influence the environment. If in the initial state these resins are not very dangerous for people and for the environment, thus under an influence of high temperatures they generate very harmful products, being the result of their thermal decomposition. Depending on the kind of the applied resin (phenol-formaldehyde, urea, furfuryl, urea–furfuryl, alkyd) under an influence of a temperature such compounds as: furfuryl alcohol, formaldehyde, phenol, BTEX group (benzene, toluene, ethylbenzene, xylene), and also polycyclic aromatic hydrocarbons (PAH) can be formed and released. [...]
    Źródło:
    Archives of Foundry Engineering; 2012, 12, 1s; 119-124
    1897-3310
    2299-2944
    Pojawia się w:
    Archives of Foundry Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-9 z 9

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