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Wyświetlanie 1-15 z 66
Tytuł:
Determination of the Protein-Binding Properties of Camptothecins by Means of Optical Spectroscopy Methods
Autorzy:
Ziomkowska, B.
Cyrankiewicz, M.
Wybranowski, T.
Kruszewski, S.
Powiązania:
https://bibliotekanauki.pl/articles/1197530.pdf
Data publikacji:
2014-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
87.64.K-
87.64.kv
87.15.kp
02.50.Sk
Opis:
Optical spectroscopy methods are widely used in studies of drugs. The affinity of camptothecins - anticancer agents - to human serum albumin (HSA) was determined in this work. Camptothecins (CPTs) exist in two forms: active lactone and open ring inactive carboxylate. In blood, the hydrolysis process of lactone form occurs which leads to deactivation of CPTs. Research is being done on biophysical properties of synthesized CPT compounds, in particular on binding to albumin. The affinity to plasma proteins is an important determinant of stability of CPTs in blood. The following analogues of CPT were tested in this paper: irinotecan, SN-38, topotecan, and 9-amino camptothecin. Using the method of fluorescence anisotropy measurement, the association constants of the studied compounds to HSA were determined. The authors attempted to determine the deactivation rate of topotecan in HSA solution using Principal Component Analysis and Factor Analysis of absorption spectra recorded during hydrolysis process of lactone form.
Źródło:
Acta Physica Polonica A; 2014, 125, 4A; A-61-A-65
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
EXAFS Studies of Zn$\text{}_{1-x}$Mn$\text{}_{x}$S Ternary Compounds
Autorzy:
Zimnal-Starnawska, M.
Łażewski, J.
Kisiel, A.
Boscherini, F.
Pascareli, S.
Giriat, W.
Powiązania:
https://bibliotekanauki.pl/articles/1931726.pdf
Data publikacji:
1994-11
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
78.70.Dm
87.64.Fb
Opis:
We performed extended X-ray absorption fine structure (EXAFS) measurements of Zn$\text{}_{1-x}$Mn$\text{}_{x}$S solid solution for various concentrations x in the range of 0 ≤ x ≤ 0.4. Data were collected on Zn and Mn K-edges with the use of synchrotron radiation from the ADONE storage ring in Frascati utilizing the Si(111) channel-cut monochromator. Applying the usual procedure of data reduction described elsewhere, we found well-defined different nearest-neighbor Zn-S and Mn-S distances, according to the previous results, almost independent on x. For Mn-S distances in the range of 0.1 ≤ x ≤ 1.0 we found, within the limit of experimental error, a constant value equal to 2.430±0.008 Å. For Zn-S distances for concentration changing from x = 0.0 to x = 0.4 we observed a weak, linear increase from 2.343±0.008 Å to 2.354 ± 0.008 Å, respectively.
Źródło:
Acta Physica Polonica A; 1994, 86, 5; 763-766
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synchrotron Radiation Photoemission Studies of Fe 3d States in Cd$\text{}_{1-x}$Fe$\text{}_{x}$Se
Autorzy:
Zema, N.
Lama, F.
Piacentini, M.
Felici, A. C.
Dębowska, D.
Kisiel, A.
Mycielski, A.
Olson, C. G.
Powiązania:
https://bibliotekanauki.pl/articles/1931775.pdf
Data publikacji:
1994-11
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
87.64.Lg
79.60.-i
Opis:
The angle integrated resonant photoemission measurements of Cd$\text{}_{1-x}$Fe$\text{}_{x}$Se were performed for different Fe concentrations (x = 0.00, 0.07, 0.14) in the photon energy range between 30 eV and 70 eV using synchrotron radiation. The ternary compound valence band photoemission spectra show, in comparison to the CdSe results, two additional structures, whose intensity depends on Fe content, which were assigned to Fe 3d states of e symmetry with spin up and down, respectively. The hybridization of the t$\text{}_{2}$ component of the 3d electrons of Fe in the valence band is discussed.
Źródło:
Acta Physica Polonica A; 1994, 86, 5; 861-867
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Methodology for FTIR Imaging of Individual Cells
Autorzy:
Yao, Seydou
Cestelli Guidi, M.
Delugin, M.
Della-Ventura, G.
Marcelli, A.
Petibois, C.
Powiązania:
https://bibliotekanauki.pl/articles/1398831.pdf
Data publikacji:
2016-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
82.80.-d
87.85.Pq
87.64.-t
Opis:
FTIR imaging is a novel spectroscopic technique able to provide cell imaging, in vivo and in real-time. However, one key issue is developing methodologies for cell culture on IR-transparent substrates fitting cell biology requirements. In this work we tested different IR-transparent substrates in terms of biotoxicity, surface properties, and spectral image acquisition qualities. Only a few substrates, namely Si₃N₄, Ge, GLS, LaF₃, Si, SrF₂, ZnS/C, ZnS/F, were found to provide cell culture conditions comparable to those observed on usual polycarbonate Petri dishes, the main limiting parameter being the toxicity of the material (ZnS, GLS, PbF₂, PbCl₂) or a poor adhesiveness (notably diamond, AgCl, CaF₂, ZnS). From substrates eligible for a good-quality cell culture, the spectral acquisition quality is mainly affected by the refractive index value. Finally, the best compromise between cell culture quality and image spectral quality could be obtained using Si and Ge substrates. This rationalization of the available IR-transparent substrates for bioimaging is particularly relevant for live cell analyses, where cell culture conditions must remain unaffected by substrate properties.
Źródło:
Acta Physica Polonica A; 2016, 129, 2; 250-254
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Molecular Interaction between Bacterial Antigens and Macrophage Receptors Studied by Atomic Force Microscopy
Autorzy:
Targosz, M.
Czuba, P.
Biedroń, R.
Strus, M.
Gamian, A.
Marcinkiewicz, J.
Szymoński, M.
Powiązania:
https://bibliotekanauki.pl/articles/2044777.pdf
Data publikacji:
2006-03
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
82.37.Rs
87.64.Dz
87.15.Kg
Opis:
Atomic force spectroscopy was used to study interaction strengths between bacterial antigens and receptors on macrophages. This method allowed for a direct comparison of the interaction strengths in different systems studied at the level of single molecules.
Źródło:
Acta Physica Polonica A; 2006, 109, 3; 421-426
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Micro-Raman Spectroscopy of Natural and Synthetic Ferritins and Their Mimetics
Autorzy:
Szybowicz, M.
Koralewski, M.
Karoń, J.
Melnikova, L.
Powiązania:
https://bibliotekanauki.pl/articles/1386994.pdf
Data publikacji:
2015-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
87.15.-v
87.64.Je
Opis:
Micro-Raman spectroscopy was used to studies of naturally occurring biogenic ferritin, synthetic ferritin with magnetic core (magnetoferritin) as well as their several mimetics. We demonstrate the ability of micro-Raman spectroscopy to discriminate between ferritin and magnetoferritin used in the studies. The results are promising for further use of the Raman spectroscopy as potential tool to distinguish between the forms of iron present in biogenic materials and biological tissues.
Źródło:
Acta Physica Polonica A; 2015, 127, 2; 534-536
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Corrosion Behavior of Crofer 22APU for Metallic Interconnects in Single and Dual Atmosphere Exposures at 1073 K
Autorzy:
Stygar, M.
Matsuda, K.
Lee, S.
Brylewski, T.
Powiązania:
https://bibliotekanauki.pl/articles/1032920.pdf
Data publikacji:
2017-05
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.05.Bx
81.65.Mq
81.70.-q
87.64.Ee
88.30.pn
Opis:
To determine the impact of an oxidizing Ar-H₂-H₂O/air dual atmosphere on the kinetics and mechanism of oxidation of the Crofer 22APU steel as compared to oxidation in a single atmosphere (Ar-H₂-H₂O or air), the oxidation kinetics of this steel were investigated both in single and dual reaction atmospheres at 1073 K during 100, 250, 500, and 1000 h of oxidation. Detailed morphological observations and the results of chemical composition analyses carried out using transmission electron microscopy combined with energy-dispersive X-ray spectroscopy revealed the presence of Fe in the scale formed on the cathode side in the dual atmosphere. Based on morphological observations (scanning- and transmission electron microscopies) and chemical and phase composition analyses (energy-dispersive X-ray spectroscopy and X-ray diffraction, respectively) of the products of oxidation of the Crofer 22APU steel, and on the determined oxidation kinetics, a mechanism describing scale growth on both sides of the steel during its oxidation in conditions involving a gradient of the chemical potential of oxygen and hydrogen was proposed.
Źródło:
Acta Physica Polonica A; 2017, 131, 5; 1394-1398
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
AFM Investigation of Biological Nanostructures
Autorzy:
Strzelecki, J.
Dąbrowski, M.
Strzelecka, J.
Tszydel, M.
Mikulska, K.
Nowak, W.
Balter, A.
Powiązania:
https://bibliotekanauki.pl/articles/1419535.pdf
Data publikacji:
2012-08
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
87.64.Dz
81.07.-b
Opis:
Nanostructures created by living organisms, optimized through millions of years of evolution, can be a valuable inspiration for nanotechnology. We employ atomic force microscopy to examine such structures in materials created by common organisms - caddisfly and diatoms. Caddisfly larvae are well known for their ability to spin silk, which serves as an "adhesive tape" to glue various materials and collect food in aqueous environment. Atomic force microscopy imaging of caddisfly silk, performed for the first time by our team, has shown that its surface is patterned with 150 nm extensions - a feature related to its exceptional underwater sticking abilities. Results of force spectroscopy of protein structures found on the surface are also shown. A characteristic feature of diatoms is that they are encased within a unique silica cell wall called frustules, patterned with 200 nm pores, which allow cellular interaction with the environment. We perform atomic force microscopy imaging of frustules in living diatoms as well as adhesion measurements inside pores.
Źródło:
Acta Physica Polonica A; 2012, 122, 2; 329-332
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Hydrothermal Synthesis of Hydroxyapatite on Titanium after Anodic Oxidation
Autorzy:
Strzała, A.
Simka, W.
Marszałek, M.
Powiązania:
https://bibliotekanauki.pl/articles/1490260.pdf
Data publikacji:
2012-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
85.85.+j
81.20.Ka
82.80.Gk
87.64.Bx
87.85.J-
Opis:
Hydrothermal synthesis of hydroxyapatite (HA) is a method which is relatively easy to apply and enables HA precipitation on substrates of various shapes, which is vital to endoprostheses fabrication. Anodic oxidation facilitates HA precipitation, making the coating thicker and more uniform. In this paper the influence of anodic oxidation of titanium substrates on HA precipitation in hydrothermal synthesis is discussed. To determine chemical composition and coating uniformity of anodised and polished Ti substrates the Raman microspectroscopy was employed. The composition was also confirmed using X-ray diffraction method. HA coatings on Ti after anodic oxidation exhibit higher uniformity in comparison to untreated Ti. The X-ray diffraction patterns showed that the HA coating was partly amorphous. Also influence of additional treatment (soaking in NaOH and/or HBSS) after anodic oxidation is discussed in the present paper. It seems that pretreatment may be favourable in some cases, but if the anodic oxidation was conducted in the presence of calcium phosphates the pretreatment seems to prevent the HA precipitation.
Źródło:
Acta Physica Polonica A; 2012, 121, 2; 561-564
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of Various Impurities on the Optical Properties of YbF$\text{}_{3}$-Doped CaF$\text{}_{2}$ Crystals
Autorzy:
Stef, M.
Pruna, A.
Pecingina-Garjoaba, N.
Nicoara, I.
Powiązania:
https://bibliotekanauki.pl/articles/2047870.pdf
Data publikacji:
2007-11
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
52.25.Os
76.30.Kg
87.64.kv
42.55.Rz
Opis:
Calcium fluoride crystals doped with YbF$\text{}_{3}$ and co-doped with LiF and NaF were grown using the vertical Bridgman method. Several of rare-earth ions (such as Eu, Sm, Ho, Tm, and Yb) can be stabilized in the divalent state in the CaF$\text{}_{2}$. The change of valence was attained by various methods. The optical absorption spectra reveal the characteristic absorption bands of the Yb$\text{}^{3+}$ and Yb$\text{}^{2+}$ ions. This means that the developed crystal growth process achieves a good Yb$\text{}^{3+}$ to Yb$\text{}^{2+}$ conversion in the as-grown crystals. The influence of other impurities, such as Na$\text{}^{+}$ or Li$\text{}^{+}$, on the absorption and emission spectrum of YbF$\text{}_{3}$-doped CaF$\text{}_{2}$ was studied. The Li$\text{}^{+}$ and Na$\text{}^{+}$ ions drastically decrease the absorption coefficient of the Yb$\text{}^{2+}$ ions in the UV band and the emission intensity by excitation in 230 nm.
Źródło:
Acta Physica Polonica A; 2007, 112, 5; 1007-1012
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Preliminary Analysis of Size Distribution of Objects Suspended in Normal Cerebrospinal Fluid in Case of Venticular Hydrocephalic Enlargement and Internal Hydrocephalus
Autorzy:
Staroń, W.
Kubisz, L.
Herbowski, L.
Powiązania:
https://bibliotekanauki.pl/articles/1490409.pdf
Data publikacji:
2012-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
87.64.M-
02.50.-r
61.20.-p
Opis:
The paper presents preliminary analysis of normal non-coloured cerebrospinal fluid obtained from patients diagnosed due to suspicion of cerebrospinal fluid malabsorption. According to the findings, the normal cerebrospinal fluid was classified into two groups: A - with clinical diagnosis of ventricular hydrocephalic enlargement and B - with clinical diagnosis of internal hydrocephalus. The analysis of microscopic pictures of normal cerebrospinal fluid in both groups according to numbers and sizes of suspended objects was performed with the aid of Eclipse 600 microscope (with magnification of 1200×) working with a computer by a digital video camera. The authors observed that there is a significant difference in a shape of the distribution curve of objects' diameters between groups A and B. The maximum number of objects in group A was recorded within the range from 5 to 10 μm in diameter size whereas in group B the maximum was recorded within the range from 0.5 to 5 μm in diameter size.
Źródło:
Acta Physica Polonica A; 2012, 121, 1A; A-046-A-048
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Distribution of Biological Particles Suspended in Normal Cerebrospinal Fluid (CSF)
Autorzy:
Staroń, W.
Herbowski, L.
Powiązania:
https://bibliotekanauki.pl/articles/1537551.pdf
Data publikacji:
2010-07
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
87.64.M-
02.50.-r
61.20.-p
Opis:
Cerebrospinal fluid's functions are protecting, expelling and transporting which are influenced by properties of the fluid. Disorder of one of the functions may bring a disease. Cerebrospinal fluid mainly consists of water (99%), cells and proteins suspended in it. Due to the suspension it can be considered as dispersion medium. Every dispersion medium is characterized by the parameters of particles suspended in it. Parameters of dispersion medium may be classified as single or cumulative parameters. Hence, there is possible to determine additional parameters which characterize CSF in order to give full description of the fluid. The authors present results of research on suspension in normal cerebrospinal fluid worked out on the basis of 2500 microscoping pictures and they also give a statistical analysis of particle diameters. The paper is a part of research project on "Physico-chemical processes in cerebrospinal fluid obtained by puncture from patients diagnosed with the disorders of cerebrospinal fluid (CSF) circulation" realized by Institute of Physics, University of Szczecin in co-operation with Neurosurgery Ward of Public Provincial Hospital Complex in Szczecin.
Źródło:
Acta Physica Polonica A; 2010, 118, 1; 159-160
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
ESR Studies of Paramagnetic Centers in Pharmaceutical Materials - Cefaclor and Clarithromycin as an Example
Autorzy:
Skowronska, A.
Wojciechowski, M.
Ramos, P.
Pilawa, B.
Kruk, D.
Powiązania:
https://bibliotekanauki.pl/articles/1490205.pdf
Data publikacji:
2012-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
87.15.La
87.64.kj
87.64.kh
75.10.Dg
Opis:
Electron spin resonance (ESR) studies of two antibiotics, Cefaclor and Clarithromycin, have been performed in order to investigate concentration and dynamics of free radicals generated in these compounds due to thermal sterilization. For Cefaclor three combinations of temperature and heating time have been applied: 160°C, 170°C, 180°C for 120 min, 60 min, and 30 min, respectively, according to the pharmaceutical sterilization norm. Clarithromycin has been heated at 160°C for 120 min. The ESR lineshape has been investigated versus microwave power ranging from 2.2 mW to 70 mW. Electron spin-spin relaxation time has been estimated from the ESR lineshape analysis. Concentrations of radicals generated due to different sterilization procedures have been compared with the purpose to select the best sterilization scheme.
Źródło:
Acta Physica Polonica A; 2012, 121, 2; 514-517
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Optical Mini-Disk Resonator Integrated into a Compact Optoelectronic Oscillator
Autorzy:
Salzenstein, P.
Tavernier, H.
Volyanskiy, K.
Kim, N.
Larger, L.
Rubiola, E.
Powiązania:
https://bibliotekanauki.pl/articles/1795637.pdf
Data publikacji:
2009-10
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
06.30.Ft
43.50.Yw
87.64.M-
87.57.cm
Opis:
This work consists in the design, fabrication and characterization of mini-disk $MgF_{2}$ resonators for integration into optoelectronic oscillator and first experimental results of implementation in microwave free spectral range oscillator with taper coupling optoelectronic oscillator.
Źródło:
Acta Physica Polonica A; 2009, 116, 4; 661-663
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Realization of a Phase Noise Measurement Bench Using Cross Correlation and Double Optical Delay Line
Autorzy:
Salzenstein, P.
Cussey, J.
Jouvenceau, X.
Tavernier, H.
Larger, L.
Rubiola, E.
Sauvage, G.
Powiązania:
https://bibliotekanauki.pl/articles/2047892.pdf
Data publikacji:
2007-11
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
06.30.Ft
43.50.Yw
87.64.M-
87.57.cm
Opis:
In this paper there are presented first results obtained with a phase noise measurement bench operating in X-band, realized in our laboratory, using double optical delay line and cross correlation. Phase noise floor using a microwave sapphire oscillator is better than -160 dB rad$\text{}^{2}$/Hz at 10 kHz from the 10 GHz carrier, using a 2 km optical delay line.
Źródło:
Acta Physica Polonica A; 2007, 112, 5; 1107-1111
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 66

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