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Wyszukujesz frazę "82.80.Ms" wg kryterium: Wszystkie pola

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    Wyświetlanie 1-13 z 13
    Tytuł:
    Atmospheric Pressure Plasma Jet for Mass Spectrometry
    Autorzy:
    Babij, M.
    Gotszalk, T.
    Kowalski, Z.
    Nitsch, K.
    Silberring, J.
    Smoluch, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/1198872.pdf
    Data publikacji:
    2014-06
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    52.50.Dg
    82.80.Ms
    Opis:
    The atmospheric pressure plasma is much advantageous over low pressure plasmas in various aspects, e.g. vacuum-free operation, relative low cost, flexibility of a continuous process. Among various plasmas generated in atmospheric pressure discharges there are cold plasma jets that represent a technology of great application promise (industry, medicine, biology). To generate low-temperature plasmas at atmospheric pressure the dielectric barrier discharge can be used. It is suitable for the atomization of volatile species and can also be served as a ionization source for ambient mass and ion mobility spectrometry. As the discharge is generated in a restricted electrode structure, a plasma jet (plume) is usually formed outside the electrode region (that provides spatial separation of the plasma generation and surface processing regions). The paper presents a source based on a plasma jet established at the end of a capillary dielectric barrier discharge at atmospheric pressure and its application to mass spectrometry. The structure of the jet generator consists of piezoelectric transformer and two concentric and symmetric electrodes, between which the working gas flows at definite rate. Besides the source description early results of spectroscopic analysis are also given.
    Źródło:
    Acta Physica Polonica A; 2014, 125, 6; 1260-1262
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Molecular Dynamics Simulations of Energetic Ar Cluster Bombardment of Ag(111)
    Autorzy:
    Palka, G.
    Rzeznik, L.
    Paruch, R.
    Postawa, Z.
    Powiązania:
    https://bibliotekanauki.pl/articles/1400436.pdf
    Data publikacji:
    2013-05
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    68.49.Sf
    82.80.Ms
    83.10.Rs
    79.20.Rf
    Opis:
    Large-scale molecular dynamics computer simulations are used to investigate the dynamics of material ejection during high-energy $Ar_n$ cluster bombardment of Ag(111) at normal incidence. The silver sample containing 7 million atoms is bombarded with $Ar_n$ projectiles (n=45-30000) with kinetic energy spanning from a few keV up to 1 MeV. Such a wide range of projectile parameters allows probing processes taking place during low-density collision cascade as well as during high-density events characteristic of micrometeorite bombardment in space. The material modifications and total sputtering yield of ejected particles are investigated. While at low-energy impacts, ejection of individual silver atoms is the main emission channel, the ejection of large clusters from the corona of the created crater dominates for the high-energy impacts.
    Źródło:
    Acta Physica Polonica A; 2013, 123, 5; 831-833
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Depth Profile Analysis of Phosphorus Implanted SiC Structures
    Autorzy:
    Konarski, P.
    Król, K.
    Miśnik, M.
    Sochacki, M.
    Szmidt, J.
    Turek, M.
    Żuk, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/1402214.pdf
    Data publikacji:
    2015-11
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    68.49.Sf
    68.55.Ln
    82.80.Ms
    85.40.Ry
    Opis:
    Secondary ion mass spectrometry depth profile analyses were performed on two sets of 4H-SiC(0001) substrate samples implanted with phosphorus. Both sets were processed under the same conditions. We implanted the samples with 100 keV (10¹¹-10¹⁴ cm¯²) phosphorus ions through the thin chemical vapor deposition deposited silicon dioxide stopping mask in order to obtain an ultra-shallow implantation profile. After phosphorus implantation, secondary ion mass spectrometry depth profile analysis was performed on the first set of samples and the second set was subjected to thermal oxidation procedure at 1200°C in order to create a dielectric layer. The aim of the oxidation process was formation of the silicon dioxide layer enriched with phosphorus: the element, which is considered to be suitable for trap density reduction. Ion implantation parameters as well as oxidation and chemical etching procedures were examined for the proper incorporation of phosphorus into the subsurface structure of the silicon oxide. Secondary ion mass spectrometry depth profile analysis was performed with Physical Electronics 06-350E sputter ion gun and QMA-410 Balzers quadrupole mass analyser. The analytical parameters such as: 1.7 keV Ar⁺ ion beam digitally scanned over 3×3 mm² area and ion erosion rate of 1.4 nm/min and sampling rate of 0.3 nm, were suitable for samples oxidized after ion implantation.
    Źródło:
    Acta Physica Polonica A; 2015, 128, 5; 864-866
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Analysis of the elemental composition of the artefacts from the Kosewo archaeological site
    Autorzy:
    Gójska, A.M.
    Miśta, E.
    Powiązania:
    https://bibliotekanauki.pl/articles/1058171.pdf
    Data publikacji:
    2016-12
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.05.Bx
    82.80.Ej
    82.80.Dx
    82.80.Ms
    82.80.Pv
    Opis:
    The Migration Period on the present Polish territories is considered as a time of depopulation of Oder, Warta, and Vistula basins. The prerequisite for such assumption is lack of the archaeological finds in these regions. In contrast, on the Mrągowo Lake District and in the Lyna basin, one can find wealth of burial crematory equipped with items from the Roman period and made in the Germanic style. The analyses using the physics techniques gives an opportunity to the meeting of history with the contemporary times and the lost things may see the light of present day. The discovered artefacts may constitute a source of knowledge, which, after analysis, will be able to fill the gaps on the map of settlements in the Polish territories. The energy-dispersive X-ray fluorescence system was used to analyze the set of Polish archaeological artefacts found in an excavation in Masurian Lakes District. The compact X-ray tube developed in the National Centre for Nuclear Research (NCBJ) was used as an X-ray source in the system designed for the energy-dispersive X-ray fluorescence studies. The X-ray fluorescence spectra of the artefacts were registered with the Amptek SDD spectrometer and the concentrations of elements were determined. The measurements show that the X-ray system developed in NCBJ with transmission type X-ray tube and the Amptek SDD spectrometer is an effective tool for chemical composition analyses of archaeological objects and can be successfully applied in archaeometry.
    Źródło:
    Acta Physica Polonica A; 2016, 130, 6; 1415-1419
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Materials Research on Archaeological Objects Using PIXE and Other Non-Invasive Techniques
    Autorzy:
    Miśta, E.
    Stonert, A.
    Korman, A.
    Milczarek, J.
    Fijał-Kirejczyk, I.
    Kalbarczyk, P.
    Wiśniewska, A.
    Powiązania:
    https://bibliotekanauki.pl/articles/1402188.pdf
    Data publikacji:
    2015-11
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.05.Bx
    82.80.Ej
    82.80.Dx
    82.80.Ms
    82.80.Pv
    Opis:
    An interdisciplinary study of metallic objects from selected archaeological sites in Poland was performed. The aim of the project was to obtain information about the chemical composition and structural changes of the objects. Furthermore, the research results provided information about the technological process which was used to manufacture the artifacts. The materials research had a non- and micro-invasive character which is very important in this type of investigation. The main experimental tools were particle-induced X-ray emission supplemented with nuclear reaction thermal neutron (white beam) radiography, scanning electron microscopy with X-ray energy dispersive analysis, and laser ablation inductively coupled plasma mass spectrometry techniques. The results show that the artifacts were made by a secondary smelting process used in local metallurgy manufactures.
    Źródło:
    Acta Physica Polonica A; 2015, 128, 5; 815-817
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Sputtering of Benzene Sample by Large Ne, Ar and Kr Clusters - Molecular Dynamics Computer Simulations
    Autorzy:
    Rzeznik, L.
    Paruch, R.
    Garrison, B.
    Postawa, Z.
    Powiązania:
    https://bibliotekanauki.pl/articles/1400433.pdf
    Data publikacji:
    2013-05
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    68.49.Sf
    82.80.Ms
    83.10.Rs
    61.82.Pv
    79.20.Rf
    Opis:
    Molecular dynamics simulations are employed to probe the role of an impact angle on emission efficiency of organic molecules sputtered from benzene crystal bombarded by 15 keV $Ne_{2953}$, $Ar_{2953}$, and $Kr_{2953}$ clusters. It is found that both the cluster type and the angle of incidence have significant effect on the emission efficiency. The shape of the impact angle dependence does not resemble the dependence characteristic for medium size clusters ($C_{60}$, $Ar_{366}$), where sputtering yield only moderately increases with the impact angle, has a shallow maximum around 40° and then decreases. On the contrary, for the large projectiles ($Ne_{2953}$, $Ar_{2953}$, and $Kr_{2953}$) the emission efficiency steeply increases with the impact angle, has a pronounced maximum around 55° followed by rapid signal decay. It has been found that the sputtering yield is the most sensitive to the impact angle change for Kr cluster projectiles, while change of the impact angle of Ne projectile has the smallest effect on the efficiency of material ejection.
    Źródło:
    Acta Physica Polonica A; 2013, 123, 5; 825-827
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Structures in Multicomponent Polymer Films: Their Formation, Observation and Applications in Electronics and Biotechnology
    Autorzy:
    Budkowski, A.
    Bernasik, A.
    Moons, E.
    Lekka, M.
    Zemła, J.
    Jaczewska, J.
    Haberko, J.
    Raczkowska, J.
    Rysz, J.
    Awsiuk, K.
    Powiązania:
    https://bibliotekanauki.pl/articles/1808304.pdf
    Data publikacji:
    2009-02
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.16.Dn
    61.25.H-
    68.37.-d
    82.80.Ms
    85.60.-q
    85.65.+h
    82.37.Rs
    Opis:
    Several strategies to form multicomponent films of functional polymers, with micron, submicron and nanometer structures, intended for plastic electronics and biotechnology are presented. These approaches are based on film deposition from polymer solution onto a rotating substrate (spin-casting), a method implemented already on manufacturing lines. Film structures are determined with compositional (nanometer) depth profiling and (submicron) imaging modes of dynamic secondary ion mass spectrometry, near-field scanning optical microscopy (with submicron resolution) and scanning probe microscopy (revealing nanometer features). Self-organization of spin-cast polymer mixtures is discussed in detail, since it offers a one-step process to deposit and align simultaneously domains, rich in different polymers, forming various device elements: (i) Surface segregation drives self-stratification of nanometer lamellae for solar cells and anisotropic conductors. (ii) Cohesion energy density controls morphological transition from lamellar (optimal for encapsulated transistors) to lateral structures (suggested for light emitting diodes with variable color). (iii) Selective adhesion to substrate microtemplates, patterned chemically, orders lateral structures for plastic circuitries. (iv) Submicron imprints of water droplets (breath figures) decorate selectively micron-sized domains, and can be used in devices with hierarchic structure. In addition, selective protein adsorption to regular polymer micropatterns, formed with soft lithography after spin-casting, suggests applications in protein chip technology. An approach to reduce lateral blend film structures to submicron scale is also presented, based on (annealed) films of multicomponent nanoparticles.
    Źródło:
    Acta Physica Polonica A; 2009, 115, 2; 435-440
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Damage Accumulation in Nuclear Ceramics
    Autorzy:
    Thomé, L.
    Moll, S.
    Jagielski, J.
    Debelle, A.
    Garrido, F.
    Sattonnay, G.
    Powiązania:
    https://bibliotekanauki.pl/articles/1503742.pdf
    Data publikacji:
    2011-07
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    61.80.-x
    61.80.Jh
    61.82.Ms
    61.43.-j
    61.85.+p
    68.37.Lp
    Opis:
    Ceramics are key engineering materials in many industrial domains. The evaluation of radiation damage in ceramics placed in a radiative environment is a challenging problem for electronic, space and nuclear industries. Ion beams delivered by various types of accelerators are very efficient tools to simulate the interactions involved during the slowing-down of energetic particles. This article presents a review of the radiation effects occurring in nuclear ceramics, with an emphasis on new results concerning the damage build-up. Ions with energies in the keV-GeV range are considered for this study in order to explore both regimes of nuclear collisions (at low energy) and electronic excitations (at high energy). The recovery, by electronic excitation, of the damage created by ballistic collisions (swift heavy ion beam induced epitaxial recrystallization process) is also reported.
    Źródło:
    Acta Physica Polonica A; 2011, 120, 1; 7-12
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Modified Positron Annihilation Model for Glassy-Like As$\text{}_{2}$Se$\text{}_{3}$
    Autorzy:
    Kozdras, A.
    Shpotyuk, O.
    Kovalskiy, A.
    Filipecki, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/2043337.pdf
    Data publikacji:
    2005-05
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    61.80.Ed
    61.82.Ms
    78.70.Bj
    Opis:
    An approach to structural characterization of chalcogenide glasses based on the study of void distribution is discussed. The results of positron annihilation lifetime spectra measurements for glassy-like g-As$\text{}_{2}$Se$\text{}_{3}$ are compared with nano-void distribution data obtained from Monte Carlo simulation. In this consideration perspectives to involve the parameters of nano-voids calculated from the first sharp diffraction peak in the framework of known Elliott's model are analyzed.
    Źródło:
    Acta Physica Polonica A; 2005, 107, 5; 832-836
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Identification and Fragmentation of Cefalosporins, Lincosamides, Levofloxacin, Doxycycline, Vancomycin by ESI-MS
    Autorzy:
    Sapon, A.
    Luhin, V.
    Sovastei, O.
    Spanik, P.
    Bondariev, V.
    Powiązania:
    https://bibliotekanauki.pl/articles/1030206.pdf
    Data publikacji:
    2017-08
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    32.10.Bi
    33.15.Ta
    82.80.-d
    Opis:
    The aim of the paper is the identification of the most frequently used antibiotics such as cefazolin, cefuroxime, cefotaxime, ceftriaxone, ceftazidime, lyncomycin, clindamycin, levofloxacin, doxycycline and vancomycin by electrospray ionization mass spectrometry interface in positive and negative modes. The fragmentation pathways of the group of antibiotics were colligated on the basis of the obtained ESI mass spectra. Generally, the positive ion spectra of antibiotics are higher in intensity including an [M+H]⁺ ion and producing less fragmentation as well as more informative compared to the negative ion spectra. Only ESI of levofloxacin in positive and negative modes with the chosen tune parameters leads to degradation of molecular ion, so the parent ion does not appear in the mass spectra. The group of antibiotics (cephalosporins and lincosamides) shows the same characteristic fragmentation. These setup parameters were successfully applied for the routine determination of antibiotics in their pharmaceutical dosage forms and other objects. Data base was developed for identification of antibiotics by comparison of their molecular and fragment ions.
    Źródło:
    Acta Physica Polonica A; 2017, 132, 2; 236-239
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Application of HPLC-MS with Electrospray Ionization for the Qualitative and Quantitative Analysis of Antibiotics in Pharmaceutical Formulation
    Autorzy:
    Likhtarovich, A.
    Luhin, V.
    Sovastei, O.
    Zukowski, P.
    Dado, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/1402227.pdf
    Data publikacji:
    2015-11
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    32.10.Bi
    33.15.Ta
    82.80.-d
    Opis:
    This study describes the application of electrospray ionization mass spectrometry in order to identify ten antibiotics (macrolides, penicillins, aminoglycosides). An optimum procedure was developed for determination of antibiotics of different grade. Positive ion spectra of most antibiotics are higher in intensity including an [M+H]⁺ ion and produce less fragmentation and are more informative compared to the negative ion spectra. The group of antibiotics exhibits the same characteristic fragmentation. The data base was developed for identification of antibiotics comparing of their molecular and fragment ions. The results of the study showed that the method with electrospray ionization is simple and quick which is useful in the routine determination of antibiotics and in their pharmaceutical dosage forms.
    Źródło:
    Acta Physica Polonica A; 2015, 128, 5; 901-904
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Phase Transformations in Pyrochlores Irradiated with Swift Heavy Ions: Influence of Composition and Chemical Bonding
    Autorzy:
    Sattonnay, G.
    Thomé, L.
    Sellami, N.
    Monnet, I.
    Grygiel, C.
    Legros, C.
    Tetot, R.
    Powiązania:
    https://bibliotekanauki.pl/articles/1400452.pdf
    Data publikacji:
    2013-05
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    61.80.-x
    61.82.Ms
    61.05.cp
    05.10.-a
    Opis:
    $Gd_2Ti_2O_7$ and $Gd_2Zr_2O_7$ pyrochlores were irradiated with swift heavy ions in order to investigate the effects of the chemical composition on the structural changes induced by high electronic excitation. The XRD results show that the structural modifications induced by irradiation with 93 MeV Xe ions are strongly dependent on the sample composition: $Gd_2Ti_2O_7$ is readily amorphized, whereas $Gd_2Zr_2O_7$ is transformed into a radiation-resistant anion-deficient fluorite structure. Atomistic simulations with the second-moment tight-binding QEq model allow us to calculate the lattice properties of both $Gd_2Ti_2O_7$ and $Gd_2Zr_2O_7$, and also to quantify the degree of covalency and ionicity in these compounds. These calculations clearly show that $Gd_2Ti_2O_7$ is more covalent than $Gd_2Zr_2O_7$, thus confirming that the amorphization resistance can be related to the covalent character of insulators.
    Źródło:
    Acta Physica Polonica A; 2013, 123, 5; 862-866
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect of Grain Size on Mechanical Properties of Irradiated Mono- and Polycrystalline $MgAl_2O_4$
    Autorzy:
    Jagielski, J.
    Piatkowska, A.
    Aubert, P.
    Labdi, S.
    Maciejak, O.
    Romaniec, M.
    Thomé, L.
    Jozwik, I.
    Debelle, A.
    Wajler, A.
    Boniecki, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/1503999.pdf
    Data publikacji:
    2011-07
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    61.80.Jh
    61.82.Ms
    62.20.Qp
    68.37.Ps
    Opis:
    The influence of the size of crystalline regions on mechanical properties of irradiated oxides has been studied using a magnesium aluminate spinel $MgAl_2O_4$. The samples characterized by different dimensions of crystalline domains, varying from sintered ceramics with grains of few micrometers in size up to single crystals, were used in the experiments. The samples were irradiated at room temperature with 320 keV $Ar^{2+}$ ions up to fluences reaching 5 × $10^{16} cm^{-2}$. Nanomechanical properties (nanohardness and Young's modulus) were measured by using a nanoindentation technique and the resistance to crack formation by measurement of the total crack lengths made by the Vickers indenter. The results revealed several effects: correlation of nanohardness evolution with the level of accumulated damage, radiation-induced hardness increase in grain-boundary region and significant improvement of material resistance to crack formation. This last effect is especially surprising as the typical depth of cracks formed by Vickers indenter in unirradiated material exceeds several tens of micrometers, i.e. is more than hundred times larger than the thickness of the modified layer.
    Źródło:
    Acta Physica Polonica A; 2011, 120, 1; 118-121
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-13 z 13

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