- Tytuł:
- Effects of B₂O₃ Addition on the Sintering Behavior of 0-5-10% ZrO₂ Doped BaTiO₃ Based Ceramics
- Autorzy:
-
Öksüz, K.
Şen, Ş.
Şen, U. - Powiązania:
- https://bibliotekanauki.pl/articles/1401289.pdf
- Data publikacji:
- 2015-04
- Wydawca:
- Polska Akademia Nauk. Instytut Fizyki PAN
- Tematy:
-
77.84.Cg
77.84.-s - Opis:
- In this study, the effect of B₂O₃ addition on the sintering behavior of 0-5-10% ZrO₂ doped barium titanate based microwave dielectric ceramics were investigated. For this purpose, the powder mixtures consisting of BaCO₃, TiO₂ and ZrO₂ were prepared by ball milling technique in alcohol using ZrO₂ balls at 200 cycle/min for 20 h. The prepared powders were calcined at 900°C for 2 h. Produced powders were mixed 0.5% B₂O₃ and 5% PVA and pressed as green body under the pressure of 100 MPa. The disc-shaped die-pressed samples were sintered at 1250°C, 1350°C and 1450°C for 4 h. X-ray diffraction analysis showed that the main phases formed in the sintered samples are BaTiO₃ and $Ba(Ti_{1-x}Zr_{x})O_3$. The scanning electron microscope (SEM) and energy-dispersive X-ray spectroscopy (EDS) were used to investigate microstructure of the sintered samples. The bulk densities of the sintered samples increased with the addition of B₂O₃ content due to the low number of pores trapped between the grains.
- Źródło:
-
Acta Physica Polonica A; 2015, 127, 4; 1086-1089
0587-4246
1898-794X - Pojawia się w:
- Acta Physica Polonica A
- Dostawca treści:
- Biblioteka Nauki
Artykuł