Temat: energy dispersive X-ray spectroscopy - Katalog OPAC zbiorów

Skocz do pozycji: 1.

Tytuł:: Advanced microstructure diagnostics and interface analysis of modern materials by high-resolution analytical transmission electron microscopy
Autorzy:: Neumann, W.
Kirmse, H.
Hausler, I.
Mogilatenko, A.
Zheng, C.
Hetaba, W.
Powiązania:: https://bibliotekanauki.pl/articles/199872.pdf
Data publikacji:: 2010
Wydawca:: Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:: electron microscopy
energy dispersive X-ray spectroscopy
electron energy loss spectroscopy
electron holography
Opis:: Transmission electron microscopy (TEM) is a powerful diagnostic tool for the determination of structure/property relationships of materials. A comprehensive analysis of materials requires a combined use of a variety of complementary electron microscopical techniques of imaging, diffraction and spectroscopy at an atomic level of magnitude. The possibilities and limitations of quantitative TEM analysis will be demonstrated for interface studies of the following materials and materials systems: Nickel-based superalloy CMSX-10, (Zn,Cd)O/ZnO/Al2O3, (Al,Ga)N/AlN/Al2O3, GaN/LiAlO2 and FeCo-based nanocrystalline alloys.
Źródło:: Bulletin of the Polish Academy of Sciences. Technical Sciences; 2010, 58, 2; 237-253
0239-7528
Pojawia się w:: Bulletin of the Polish Academy of Sciences. Technical Sciences
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 2.

Tytuł:: Determination of elements by atomic absorption spectrometry and energy dispersive X-ray spectroscopy in humic acids and soil samples
Oznaczanie pierwiastków za pomocą atomowej spektrometrii absorpcyjnej i spektrometrii rentgenowskiej energii rozproszonej w próbkach kwasów huminowych oraz gleby
Autorzy:: Konečná, M.
Pospíšilová, L.
Škarpa, P.
Powiązania:: https://bibliotekanauki.pl/articles/125973.pdf
Data publikacji:: 2011
Wydawca:: Towarzystwo Chemii i Inżynierii Ekologicznej
Tematy:: humic acids
labile forms
atomic absorption spectrometry
energy dispersive X-ray spectroscopy
kwasy huminowe
formy labilne
spektrometria absorpcji atomowej
spektroskopia z dyspersją energii promieniowania X
Opis:: Determination of various elements in humic acids and soil samples is important with regard to their biological availability. This work was focused on the identification of trace elements presented in soil samples and humic acids preparates. The object of our study was the samples of grassland soil classified according to FAO as Eutric Cambisol (locality Vatín, Czech-Moravian Upland). Labile and total several element contents in the studied samples were determined. The labile forms were measured in the 0.01 M CaCl2 extract by using high resolution continuum source atomic absorption spectrometer. Total element contents were determined after extraction in aqua regia. Basic soil properties were measured by commonly used methods - soil reaction and conductivity by potentiometric method, texture by pipette method, CEC according to Kappen method and Cox by titrimetric oxidation. Soil humic acids (HA) were isolated according to standard IHSS method. Elemental composition of HA was determined by CHSN/O analyzer. Energy dispersive X-ray spectroscopy allowed us to detect elements in situ in HA molecule and following elements were found: Fe, Cu, Zn, Ti, Ca, K, S, P, Si and Br. The presence of mentioned elements in humic acids preparates was compared with the determined amounts of labile forms and total contents in the soil samples.
Źródło:: Proceedings of ECOpole; 2011, 5, 2; 377-381
1898-617X
2084-4557
Pojawia się w:: Proceedings of ECOpole
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 3.

Tytuł:: Biosynthesis, characterisation, free radical scavenging activity and anti-bacterial effect of plant-mediated zinc oxide nanoparticles using Pithecellobium dulce and Lagenaria siceraria Leaf Extract
Autorzy:: Prakash, M. Jeevan
Kalyanasundharam, S.
Powiązania:: https://bibliotekanauki.pl/articles/1193960.pdf
Data publikacji:: 2015
Wydawca:: Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:: 2-2-diphenyl-1-picrylhydrazyl
DPPH
Energy Dispersive Xray
Lagenaria siceraria
Pithecellobium dulce
Scanning Electron Microscopy
Transmission Electron Microscope
X-Ray
ZnO
by FTIR Spectroscopy
gram-positive and gram negative bacterial
Opis:: The study involved synthesis of Zinc Oxide nanoparticles using biological and chemical reducing agents. The aim was to compare the yield, nature and antimicrobial activity of nanoparticles. Nanoparticles synthesized by the two methods were characterized by FTIR Spectroscopy, Scanning Electron Microscopy (SEM), Energy Dispersive Xray (EDAX), Transmission Electron Microscope (TEM) and X-ray diffraction (XRD). In biological method, Pithecellobium dulce and Lagenaria siceraria leaf extract; and in chemical method, sodium hydroxide was used as reducing agents. Antibacterial study was carried out on gram-positive and gram negative bacterial strains by disc diffusion method. The biologically synthesized ZnO Nanoparticles showed better antimicrobial activities with respect to the activities of synthetic drugs than chemical method. Antioxidant potential of synthesized nanoparticles was assessed through 2,2–diphenyl-1-picrylhydrazyl (DPPH) method.
Źródło:: World Scientific News; 2015, 18; 60-77
2392-2192
Pojawia się w:: World Scientific News
Dostawca treści:: Biblioteka Nauki

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